WATER QUALITY - DETERMINATION OF ORGANOCHLORINE PESTICIDES (OCP) IN WHOLE WATER SAMPLES - METHOD USING SOLID PHASE EXTRACTION (SPE) WITH SPE-DISKS COMBINED WITH GAS CHROMATOGRAPHY MASS SPECTROMETRY (GC-MS)

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

01-01-2015

Publisher

National Standards Authority of Ireland

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National Foreword
European foreword
Introduction
1 Scope
2 Normative references
3 Principle
4 Interferences
5 Reagents
6 Apparatus
7 Sampling
8 Procedure
9 Calibration
10 Calculation of the results
11 Expression of results
12 Test report
Annex A (informative) - Suitable gas chromatographic
        conditions and example chromatograms -
        GC-conditions of example chromatograms in
        Figure A.1
Annex B (informative) - Repeatability and reproducibility data
Annex C (informative) - Examples of suitable SPE-disks
Annex D (informative) - Examples of internal standards
Bibliography

Defines a method for the determination of selected organochlorine pesticides (OCP), in water samples.

DocumentType	Standard
Pages	34
PublisherName	National Standards Authority of Ireland
Status	Current

Standards	Relationship
EN 16693:2015	Identical

ISO 22892:2006	Soil quality Guidelines for the identification of target compounds by gas chromatography and mass spectrometry
ISO 5667-3:2012	Water quality Sampling Part 3: Preservation and handling of water samples
ISO 5667-1:2006	Water quality Sampling Part 1: Guidance on the design of sampling programmes and sampling techniques
ISO 5725-2:1994	Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
EN ISO 5667-3:2012	Water quality - Sampling - Part 3: Preservation and handling of water samples (ISO 5667-3:2012)
ISO 3696:1987	Water for analytical laboratory use — Specification and test methods
ISO 8466-1:1990	Water quality Calibration and evaluation of analytical methods and estimation of performance characteristics Part 1: Statistical evaluation of the linear calibration function
EN ISO 3696:1995	Water for analytical laboratory use - Specification and test methods (ISO 3696:1987)
EN ISO 22892:2011	Soil quality - Guidelines for the identification of target compounds by gas chromatography and mass spectrometry (ISO 22892:2006)
ISO/TS 28581:2012	Water quality — Determination of selected non-polar substances — Method using gas chromatography with mass spectrometric detection (GC-MS)
EN ISO 5667-1 : 2006 COR 2007	WATER QUALITY - SAMPLING - PART 1: GUIDANCE ON THE DESIGN OF SAMPLING PROGRAMMES AND SAMPLING TECHNIQUES

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I.S. EN 16693:2015

WATER QUALITY - DETERMINATION OF ORGANOCHLORINE PESTICIDES (OCP) IN WHOLE WATER SAMPLES - METHOD USING SOLID PHASE EXTRACTION (SPE) WITH SPE-DISKS COMBINED WITH GAS CHROMATOGRAPHY MASS SPECTROMETRY (GC-MS)

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Abstract

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