NBN EN 13925-3 : 2005
Current
The latest, up-to-date edition.
NON DESTRUCTIVE TESTING - X RAY DIFFRACTION FROM POLYCRYSTALLINE AND AMORPHOUS MATERIALS - PART 3: INSTRUMENTS
12-01-2013
Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Description of equipment
4.1 General
4.2 X-ray sources
4.2.1 General
4.2.2 Conventional X-ray sources (sealed tubes and
rotating anode sources)
4.2.3 Synchrotron radiation sources
4.3 Incident and diffracted X-ray beam optics
4.3.1 General
4.3.2 Monochromators
4.3.3 Beam dimensions and geometry
4.4 Detectors
4.4.1 Types of detector
4.4.2 Spatial resolution of detectors
4.4.3 Energy resolution of detectors
4.5 Goniometers
4.5.1 General
4.5.2 Specimen positioning
4.6 Specimen stage
4.7 Data collection system
5 Characterisation of equipment components
6 Equipment alignment and calibration
6.1 General
6.2 Alignment
6.3 Calibration
7 Performance testing and monitoring
Annex A (informative) Relationship between the XRPD standards
Annex B (informative) Alignment of Bragg-Brentano diffractometers
Annex C (informative) Procedures for instrument performance
characterisation
C.1 General
C.2 Position, intensity and breadth of a limited number of
diffraction lines
C.3 Angular Deviation Curve
C.4 Line breadth
C.5 Intensity diagrams
C.6 Shape Analysis Curve
C.7 Lattice parameters
C.8 The use of the Fundamental Parameter Approach
C.9 Whole pattern fitting
Annex D (informative) Sample report forms for characterisation of
instruments
Bibliography
Defines the characteristics of instruments used for X-ray powder diffraction as a basis for their control and hence quality assurance of the measurements made by this technique.
DocumentType |
Standard
|
PublisherName |
Belgian Standards
|
Status |
Current
|
Standards | Relationship |
UNI EN 13925-3 : 2005 | Identical |
BS EN 13925-3:2005 | Identical |
DIN EN 13925-3:2005-07 | Identical |
EN 13925-3:2005 | Identical |
UNE-EN 13925-3:2006 | Identical |
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