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NFV 03 110 : 2010

Current

Current

The latest, up-to-date edition.

ANALYSIS OF AGRI-FOODSTUFFS - PROTOCOL OF CHARACTERIZATION FOR THE VALIDATION OF A QUANTITATIVE METHOD OF ANALYSIS BY CONSTRUCTION OF AN ACCURACY PROFILE

Published date

12-01-2013

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1 Domaine d'application
2 Références normatives
3 Définitions et symboles
  3.1 Vocabulaire général
  3.2 Vocabulaire propre au présent document
  3.3 symboles
4 Contenu du dossier de validation intra-laboratoire
  4.1 Texte ou référence précise de la méthode de
      référence
  4.2 Description détaillée de la méthode alternative
  4.3 Portée de la validation intra-laboratoire
  4.4 Organisation des protocoles de mesure
  4.5 Calculs et conclusions
5 Partie expérimentale
  5.1 Étalonnage de la méthode alternative (plan A)
  5.2 Spécificité de la méthode alternative (plan B)
  5.3 Évaluation de la fidélité (répétabilité) et de la
      justesse par rapport à la méthode de référence
      (plan C)
  5.4 Reproductibilité interne (plan D) (optionnel)
6 Résumé des expériences effectuées
Annexe A (informative) Exemples
Annexe B Tables statistiques
Annexe C Conduite des calculs avec un tableur
Bibliographie

Le présent document se propose de guider un laboratoire d'analyse agro-alimentaire dans la constitution d'un dossier de validation intralaboratoire d'une méthode d'analyse quantitative pratiquée en interne, par rapport à une méthode de référence. Cette validation doit permettre à tout analyste d'utiliser la méthode en connaissant ses performances.

DevelopmentNote
Indice de classement: V03-110. (02/2004) PR NFV 03 110 February 2009. (02/2009) PR NFV 03 110 November 2009. (11/2009)
DocumentType
Standard
PublisherName
Association Francaise de Normalisation
Status
Current

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NF ISO 5725-2 : 1994 APPLICATION OF STATISTICS - ACCURACY (TRUENESS AND PRECISION) OF MEASUREMENT METHODS AND RESULTS - PART 2: BASIC METHOD FOR THE DETERMINATION OF REPEATABILITY AND REPRODUCIBILITY OF A STANDARD MEASUREMENT METHOD
NF ISO 5725-1 : 1994 APPLICATION OF STATISTICS - ACCURACY (TRUENESS AND PRECISION) OF MEASUREMENT METHODS AND RESULTS - PART 1: GENERAL PRINCIPLES AND DEFINITIONS
NF ISO 5725-3 : 1994 APPLICATION OF STATISTICS - ACCURACY (TRUENESS AND PRECISION) OF MEASUREMENT METHODS AND RESULTS - PART 3: INTERMEDIATE MEASURES OF THE PRECISION OF A STANDARD MEASUREMENT METHOD
NF ISO 5725-4 : 1994 APPLICATION OF STATISTICS - ACCURACY (TRUENESS AND PRECISION) OF MEASUREMENT METHODS AND RESULTS - PART 4: BASIC METHODS FOR THE DETERMINATION OF THE TRUENESS OF A STANDARD MEASUREMENT METHOD
ISO/IEC Guide 99:2007 International vocabulary of metrology Basic and general concepts and associated terms (VIM)

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