PD CEN/TS 1948-5:2015
Current
The latest, up-to-date edition.
Stationary source emissions. Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs Long-term sampling of PCDDs/PCDFs and PCBs
Hardcopy , PDF
English
30-04-2015
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Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Symbols and abbreviations
5 Principle of long-term PCDD/PCDF/PCB sampling
6 Sampling device and materials
7 Minimum requirements for long-term PCDD/PCDF/PCB
sampling methods
8 Quality assurance
9 Analytical procedure
10 Estimation of uncertainty of the method
11 Reporting
Annex A (normative) - Overview of minimum requirements
Annex B (informative) - Cleaning of the probe
Annex C (normative) - Performance criteria and test procedure
for certification
Annex D (informative) - Examples of devices and operation for
long-term sampling systems
Annex E (informative) - Fundamentals of isokinetic sampling
Annex F (informative) - Example for the determination of the
representative sampling point
Annex G (informative) - Estimation of the uncertainty of
measured PCDD/PCDF of the long-term sampling
system
Annex H (informative) - Example for calculation of measurement
results for standard conditions
Annex I (normative) - Adaption of the maximum deviation in
relation to the PCDD/PCDF/PCB concentration
Bibliography
Describes the long-term sampling of PCDDs, PCDFs and PCBs.
| Committee |
EH/2/1
|
| DocumentType |
Standard
|
| Pages |
84
|
| PublisherName |
British Standards Institution
|
| Status |
Current
|
This Technical Specification specifies the long-term sampling of PCDDs, PCDFs and PCBs. There are three different sampling methods, which use the three different principles described in EN1948‑1 modified for long-term sampling requirements: filter/condenser method; dilution method; cooled probe method. Each sampling method is illustrated in detail in AnnexD. The sampling methods described in this document are designed for a sampling duration of typically four weeks. Additionally this document specifies a framework of quality control requirements for any long-term sampling method to be applied (see AnnexC and AnnexF). With the methods described experiences were gained for a concentration range from typically 0,003ng I-TEQ/m 3 up to 4,0ng I-TEQ/m 3 and 0,003ng WHO-TEQ/m 3 up to 4,0ng WHO-TEQ/m 3 respectively at different stationary sources (e.g. waste incinerators, sinter plants, cement kilns). For the complete measurement method the use of EN1948‑2 and EN1948‑3 describing extraction and cleanup and identification and quantification, respectively, is necessary in order to determine PCDDs/PCDFs. Also EN1948‑4 is necessary for the analyses of dioxin-like PCBs.
| Standards | Relationship |
| CEN/TS 1948-5:2015 | Identical |
| ISO/IEC 17025:2005 | General requirements for the competence of testing and calibration laboratories |
| EN 15267-3:2007 | Air quality - Certification of automated measuring systems - Part 3: Performance criteria and test procedures for automated measuring systems for monitoring emissions from stationary sources |
| EN 1948-2:2006 | Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 2: Extraction and clean-up of PCDDs/PCDFs |
| ISO 14956:2002 | Air quality — Evaluation of the suitability of a measurement procedure by comparison with a required measurement uncertainty |
| EN ISO 16911-1:2013 | Stationary source emissions - Manual and automatic determination of velocity and volume flow rate in ducts - Part 1: Manual reference method (ISO 16911-1:2013) |
| EN 15267-2:2009 | Air quality - Certification of automated measuring systems - Part 2: Initial assessment of the AMS manufacturer’s quality management system and post certification surveillance for the manufacturing process |
| EN 15259:2007 | Air quality - Measurement of stationary source emissions - Requirements for measurement sections and sites and for the measurement objective, plan and report |
| ISO/IEC Guide 99:2007 | International vocabulary of metrology Basic and general concepts and associated terms (VIM) |
| EN 13284-1:2017 | Stationary source emissions - Determination of low range mass concentration of dust - Part 1: Manual gravimetric method |
| ISO 16911-1:2013 | Stationary source emissions — Manual and automatic determination of velocity and volume flow rate in ducts — Part 1: Manual reference method |
| EN 14181:2014 | Stationary source emissions - Quality assurance of automated measuring systems |
| EN 1948-1:2006 | Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 1: Sampling of PCDDs/PCDFs |
| EN 1948-3:2006 | Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 3: Identification and quantification of PCDDs/PCDFs |
| EN ISO 14956:2002 | Air quality - Evaluation of the suitability of a measurement procedure by comparison with a required measurement uncertainty (ISO 14956:2002) |
| ENV 13005 : DRAFT 1999 | GUIDE TO THE EXPRESSION OF UNCERTAINTY IN MEASUREMENT |
| EN 1948-4:2010+A1:2013 | Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 4: Sampling and analysis of dioxin-like PCBs |
| EN 15267-1:2009 | Air quality - Certification of automated measuring systems - Part 1: General principles |
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