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  • EN 1948-1:2006

    Current The latest, up-to-date edition.

    Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 1: Sampling of PCDDs/PCDFs

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    Published date:  15-03-2006

    Publisher:  Comite Europeen de Normalisation

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    Table of Contents - (Show below) - (Hide below)

    Foreword
    Introduction
    1 Scope
    2 Normative references
    3 Terms and definitions
    4 Symbols and abbreviations
    5 Principle of the complete PCDD/PCDF measurement procedure
    6 Sampling device and materials
    7 Minimum requirements for sampling
    8 Safety measures and transport
    9 Preparations and sampling
    Annex A (informative) Toxicity and toxic equivalency
    Annex B (informative) Examples of operation
    Annex C (informative) Examples of adsorbents and their preparations
                          and cleaning
    Annex D (informative) Sampling measurement record
    Annex E (informative) Relations to EU Directives
    Bibliography

    Abstract - (Show below) - (Hide below)

    This European Standard specifies the sampling of PCDDs/PCDFs. It is an integral part of the complete measurement procedure. The use of the other two parts prEN 1948-2:2005 and prEN 1948-3:2005 describing extraction and clean-up and identification and quantification, respectively, is necessary for the determination of the PCDDs/PCDFs.This European Standard has been developed to measure PCDD/PCDF concentrations at about 0,1 ng I TEQ/m3 in stationary source emissions.This European Standard specifies both method validation and a framework of quality control requirements which shall be fulfilled by any PCDD/PCDF sampling.The user has the possibility to choose between three different methods:-"filter/condenser method"-"dilution method"-"cooled probe method"Each sampling method is illustrated by some sampling systems described in detail in Annex B as examples of proven procedures.During comparison measurements of the three sampling methods on municipal waste incinerators at the level of about 0,1 ng I-TEQ/m3 these methods have been deemed comparable within the expected range of uncertainty. Validation trials were performed on the flue gas of municipal waste incinerators at the level of about 0,1 ng I-TEQ/m3 and a dust loading of from 1 mg/m3 to 15 mg/m3. Although this European Standard is primarily developed and validated for gaseous streams emitted by waste incinerators, the practical experience shows that it can be applied for wide concentration ranges and various emission sources.The procedure described in the three parts of prEN 1948:2005 specifies requirements which shall be met in order to measure the 17 congeners necessary to calculate the total I-TEQ (see Table A.1).Besides the determination of PCDDs/PCDFs the described measurement methods are suitable for determination of other low-volatile substances, e.g. of dioxin-like PCBs (details for sampling and analyses see CEN/TS 1948-4), although no validated performance characteristics are avail

    General Product Information - (Show below) - (Hide below)

    Committee CEN/TC 264
    Development Note Supersedes PREN 1948-1. (06/2006)
    Document Type Standard
    Publisher Comite Europeen de Normalisation
    Status Current

    Standards Referenced By This Book - (Show below) - (Hide below)

    DD CEN/TS 1948-4:2007 Stationary source emissions. Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs Sampling and analysis of dioxin-like PCBs
    PD CEN/TS 1948-5:2015 Stationary source emissions. Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs Long-term sampling of PCDDs/PCDFs and PCBs
    S.R. CEN TS 1948-4:2007 STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 4: SAMPLING AND ANALYSIS OF DIOXIN-LIKE PCBS
    UNI CEN/TS 16190 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF DIOXINS AND FURANS AND DIOXIN-LIKE POLYCHLORINATED BIPHENYLS BY GAS CHROMATOGRAPHY WITH HIGH RESOLUTION MASS SELECTIVE DETECTION (HR GC-MS)
    CEN/TS 1948-5:2015 Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 5: Long-term sampling of PCDDs/PCDFs and PCBs
    EN 1948-4:2010+A1:2013 STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 4: SAMPLING AND ANALYSIS OF DIOXIN-LIKE PCBS
    CEN/TS 15675:2007 Air quality - Measurement of stationary source emissions - Application of EN ISO/IEC 17025:2005 to periodic measurements
    I.S. EN 1948-4:2010 STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 4: SAMPLING AND ANALYSIS OF DIOXIN-LIKE PCBS
    BS ISO 13914:2013 Soil quality. Determination of dioxins and furans and dioxin-like polychlorinated biphenyls by gas chromatography with high-resolution mass selective detection (GC/HRMS)
    03/320962 DC : DRAFT DEC 2003 EN 1948-3 - STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 3: IDENTIFICATION AND QUANTIFICATION OF PCDDS/PCDFS
    S.R. CEN TS 15675:2007 AIR QUALITY - MEASUREMENT OF STATIONARY SOURCE EMISSIONS - APPLICATION OF EN ISO/IEC 17025:2005 TO PERIODIC MEASUREMENTS
    PREN 16190 : DRAFT 2017 SOIL, TREATED BIOWASTE AND SLUDGE - DETERMINATION OF DIOXINS AND FURANS AND DIOXIN-LIKE POLYCHLORINATED BIPHENYLS BY GAS CHROMATOGRAPHY WITH HIGH RESOLUTION MASS SELECTIVE DETECTION (HR GC-MS)
    DIN EN 1948-2:2006-06 Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 2: Extraction and clean-up of PCDDs/PCDFs
    I.S. EN 1948-2:2006 STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 2: EXTRACTION AND CLEAN-UP OF PCDDS/PCDFS
    DIN EN 1948-3:2006-06 Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 3: Identification and quantification of PCDDs/PCDFs
    I.S. EN 1948-3:2006 STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 3: IDENTIFICATION AND QUANTIFICATION OF PCDDS/PCDFS
    VDI 3927 Blatt 2:2015-05 Waste gas cleaning - Reduction of inorganic and organic trace species in combustion flue gases
    VDI 3890:2016-03 Emission control - Pet cremation facilities
    VDI 3874:2006-12 Stationary source emissions - Determination of polycyclic aromatic hydrocarbons (PAH) - GC/MC method
    VDI 2597:2004-07 Emission control - Plants for the production of lead and lead alloys
    VDI 3462 Blatt 6:2009-03 Emission control - Wood machining and processing - Facility-specific measuring instructions
    VDI 3476 Blatt 1:2015-06 Waste gas cleaning - Methods of catalytic waste gas cleaning - Fundamentals
    VDI 3891:2015-07 Emission control - Human cremation facilities
    VDI 3498 Blatt 2:2002-07 Ambient air measurement - Indoor air measurement - Measurement of polychlorinated dibenzo-p-dioxins and dibenzofurans; Method using small filters
    VDI 3899 Blatt 1:2016-05 Emission control - Landfill gas - Utilisation and treatment of landfill gas
    VDI 2576:2010-01 Emission control - Carbothermic and metallothermic production of ferroalloys and silicon metal
    VDI 3498 Blatt 1:2002-07 Ambient air measurement - Indoor air measurement - Measurement of polychlorinated dibenzo-p-dioxins and dibenzofurans; Method using large filters
    VDI 3475-3 : 2006 COR 2007 Emission control - Mechnical-biological treatment facilities for municipal solid waste - Corrigendum concerning guideline VDI 3475 Part 3:2006-12
    VDI 2578:2017-05 Emission control - Glassworks
    VDI 2262 Blatt 1:2013-06 Workplace air - Reduction of exposure to air pollutants - Legal principles, terms and definitions, basic organisational measures for industrial safety and environmental protection
    VDI 3898:2013-01 Emission control - Plants for dry mechanical, physio-chemical, thermal and biological soil treatment
    VDI 2102 Blatt 1:2007-04 (Draft) Emission control - Secondary copper smelting and refining plants
    VDI 2102 Blatt 2:2013-04 Emission control - Copper and copper alloy melting plants
    VDI 3476 Blatt 2:2010-01 Waste gas cleaning - Catalytic waste gas cleaning methods - Oxidative processes
    09/30198710 DC : 0 BS EN 1948-4 - STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 4: SAMPLING AND ANALYSIS OF DIOXIN-LIKE PCBS
    12/30231398 DC : 0 BS ISO 13914 - SOIL QUALITY - DETERMINATION OF DIOXINS AND FURANS AND DIOXIN-LIKE POLYCHLORINATED BIPHENYLS BY GAS CHROMATOGRAPHY WITH HIGH-RESOLUTION MASS SELECTIVE DETECTION (HR GC/MS)
    DIN EN 1948-4:2014-03 STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 4: SAMPLING AND ANALYSIS OF DIOXIN-LIKE PCBS
    BS EN 1948-3:2006 Stationary source emissions. Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs Identification and quantification of PCDDs/PCDFs
    EN 1948-2:2006 Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 2: Extraction and clean-up of PCDDs/PCDFs
    UNI EN 1948-3 : 2006 STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 3: IDENTIFICATION AND QUANTIFICATION OF PCDDS/PCDFS
    UNI EN 1948-2 : 2006 STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 2: EXTRACTION AND CLEAN-UP OF PCDDS/PCDFS
    DD CEN/TS 15675:2007 Air quality. Measurement of stationary source emissions. Application of EN ISO/IEC 17025:2005 to periodic measurements
    UNE-EN 1948-4:2011 Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 4: Sampling and analysis of dioxin-like PCBs
    03/320961 DC : DRAFT NOV 2003 EN 1948-2 - STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 2: EXTRACTION AND CLEAN-UP OF PCDDS/PCDFS
    BS EN 1948-2:2006 Stationary source emissions. Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs Extraction and clean-up of PCDDs/PCDFs
    EN 1948-3:2006 Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 3: Identification and quantification of PCDDs/PCDFs
    BS EN 1948-4 : 2010 STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 4: SAMPLING AND ANALYSIS OF DIOXIN-LIKE PCBS
    S.R. CEN/TS 16190:2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF DIOXINS AND FURANS AND DIOXIN-LIKE POLYCHLORINATED BIPHENYLS BY GAS CHROMATOGRAPHY WITH HIGH RESOLUTION MASS SELECTIVE DETECTION (HR GC-MS)
    17/30363999 DC : 0 BS EN 16190 - SOIL, TREATED BIOWASTE AND SLUDGE - DETERMINATION OF DIOXINS AND FURANS AND DIOXIN-LIKE POLYCHLORINATED BIPHENYLS BY GAS CHROMATOGRAPHY WITH HIGH RESOLUTION MASS SELECTIVE DETECTION (HR GC-MS)
    S.R. CEN/TS 1948-5:2015 STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 5: LONG-TERM SAMPLING OF PCDDS/PCDFS AND PCBS
    UNI EN 1948-4 : 2014 STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE MASS CONCENTRATION OF PCDDS/PCDFS AND DIOXIN-LIKE PCBS - PART 4: SAMPLING AND ANALYSIS OF DIOXIN-LIKE PCBS
    ISO 13914:2013 Soil quality — Determination of dioxins and furans and dioxin-like polychlorinated biphenyls by gas chromatography with high-resolution mass selective detection (GC/HRMS)
    CEN/TS 16190:2012 Sludge, treated biowaste and soil - Determination of dioxins and furans and dioxin-like polychlorinated biphenyls by gas chromatography with high resolution mass selective detection (HR GC-MS)
    CEN/TS 1948-4:2007 Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 4: Sampling and analysis of dioxin-like PCBs

    Standards Referencing This Book - (Show below) - (Hide below)

    ISO/IEC 17025:2005 General requirements for the competence of testing and calibration laboratories
    ISO 845:2006 Cellular plastics and rubbers — Determination of apparent density
    EN 1948-2:2006 Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 2: Extraction and clean-up of PCDDs/PCDFs
    EN 14789:2017 Stationary source emissions - Determination of volume concentration of oxygen - Standard reference method: Paramagnetism
    EN ISO 845:2009 Cellular plastics and rubbers - Determination of apparent density (ISO 845:2006)
    EN 13284-1:2017 Stationary source emissions - Determination of low range mass concentration of dust - Part 1: Manual gravimetric method
    EN 1948-3:2006 Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 3: Identification and quantification of PCDDs/PCDFs
    EN 14790:2017 Stationary source emissions - Determination of the water vapour in ducts - Standard reference method
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