• PREN 15991 : DRAFT 2014

    Superseded A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

    TESTING OF CERAMIC AND BASIC MATERIALS - DIRECT DETERMINATION OF MASS FRACTIONS OF IMPURITIES IN POWDERS AND GRANULES OF SILICON CARBIDE BY INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRY (ICP OES) WITH ELECTROTHERMAL VAPORISATION (ETV)

    Available format(s): 

    Superseded date:  01-11-2015

    Language(s): 

    Published date:  12-01-2013

    Publisher:  Comite Europeen de Normalisation

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    Table of Contents - (Show below) - (Hide below)

    Foreword
    1 Scope
    2 Principle
    3 Spectrometry
    4 Apparatus
    5 Reagents and auxiliary material
    6 Sampling and sample preparation
    7 Calibration
    8 Procedure
    9 Wavelength and working range
    10 Calculation of the results and evaluation
    11 Reporting of results
    12 Precision
    13 Test report
    Annex A (informative) - Results of interlaboratory study
    Annex B (informative) - Wavelength and working range
    Annex C (informative) - Possible interferences and their elimination
    Annex D (informative) - Information regarding the evaluation of the
            uncertainty of the mean value
    Annex E (informative) - Commercial certified reference materials
    Annex F (informative) - Information regarding the validation of an
            analytical method based on liquid standards at the example
            of SiC and graphite
    Bibliography

    Abstract - (Show below) - (Hide below)

    Describes a method for the determination of the trace element concentrations of Al, Ca, Cr, Cu, Fe, Mg, Ni, Ti, V and Zr in powdered and granular silicon carbide.

    General Product Information - (Show below) - (Hide below)

    Comment Closes On
    Committee TC 187
    Document Type Draft
    Publisher Comite Europeen de Normalisation
    Status Superseded
    Superseded By

    Standards Referencing This Book - (Show below) - (Hide below)

    ISO 5022:1979 Shaped refractory products Sampling and acceptance testing
    EN ISO 21068-1:2008 Chemical analysis of silicon-carbide-containing raw materials and refractory products - Part 1: General information and sample preparation (ISO 21068-1:2008)
    ISO 5725-4:1994 Accuracy (trueness and precision) of measurement methods and results Part 4: Basic methods for the determination of the trueness of a standard measurement method
    ISO 21068-1:2008 Chemical analysis of silicon-carbide-containing raw materials and refractory products Part 1: General information and sample preparation
    ISO 5725-2:1994 Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
    ISO 8656-1:1988 Refractory products Sampling of raw materials and unshaped products Part 1: Sampling scheme
    ISO/IEC Guide 98-3:2008 Uncertainty of measurement — Part 3: Guide to the expression of uncertainty in measurement (GUM:1995)
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