UNE-EN 15308:2017
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
Characterization of waste - Determination of selected polychlorinated biphenyls (PCB) in solid waste by gas chromatography with electron capture or mass spectrometric detection
Hardcopy , PDF
Spanish, Castilian, English
08-02-2017
01-09-2020
This draft European Standard specifies a method for quantitative determination of seven polychlorinated biphenyl congeners (PCB-28, PCB-52, PCB-101, PCB-118, PCB-138, PCB-153 and PCB-180) in solid waste using high-resolution gas chromatography with electron capture or mass spectrometric detection. The basic content of this standard is identical to that of the Horizontal PCB-standard and is therefore also applicable to soil, sludge and treated bio-waste. The detection and the quantification limits in this method are dependent on sample intake, the level of interferences as well as instrumental limitations. Under the conditions specified in this standard, minimum amounts of individual PCB congeners equal or above 0,01 mg/kg dry matter can typically be determined with no interferences present.
NOTEFor the analysis of PCB in insulating liquids, petroleum products, used oils and aqueous samples is referred to EN 61619, EN 12766 1 and EN ISO 6468 respectively.
The method may be applied to the analysis of other PCB congeners not specified in the scope, but its suitability should be proven by proper in-house validation experiments.
| Committee |
CTN 77/SC 5
|
| DocumentType |
Standard
|
| Pages |
56
|
| PublisherName |
Asociación Española de Normalización
|
| Status |
Superseded
|
| Standards | Relationship |
| EN 15308:2016 | Identical |
| EN ISO 6468:1996 | Water quality - Determination of certain organochlorine insecticides, polychlorinated biphenyls and chlorobenzenes - Gas chromatographic method after liquid-liquid extraction (ISO 6468:1996) |
| EN 12766-1:2000 | Petroleum products and used oils - Determination of PCBs and related products - Part 1: Separation and determination of selected PCB congeners by gas chromatography (GC) using an electron capture detector (ECD) |
| ISO 11464:2006 | Soil quality — Pretreatment of samples for physico-chemical analysis |
| ISO 22892:2006 | Soil quality — Guidelines for the identification of target compounds by gas chromatography and mass spectrometry |
| EN 61619:1997 | Insulating liquids - Contamination by polychlorinated biphenyls (PCBs) - Method of determination by capillary column gas chromatography |
| EN 14346:2006 | Characterization of waste - Calculation of dry matter by determination of dry residue or water content |
| ISO 14507:2003 | Soil quality — Pretreatment of samples for determination of organic contaminants |
| EN 12766-2:2001 | Petroleum products and used oils - Determination of PCBs and related products - Part 2: Calculation of polychlorinated biphenyl (PCB) content |
| EN 15002:2015 | Characterization of waste - Preparation of test portions from the laboratory sample |
| EN ISO 22892:2011 | Soil quality - Guidelines for the identification of target compounds by gas chromatography and mass spectrometry (ISO 22892:2006) |
| ISO 6468:1996 | Water quality — Determination of certain organochlorine insecticides, polychlorinated biphenyls and chlorobenzenes — Gas chromatographic method after liquid-liquid extraction |
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