• EN 61619:1997

    Current The latest, up-to-date edition.

    Insulating liquids - Contamination by polychlorinated biphenyls (PCBs) - Method of determination by capillary column gas chromatography

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    Published date:  23-04-1997

    Publisher:  European Committee for Standards - Electrical

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    Table of Contents - (Show below) - (Hide below)

    1 Scope and object
    2 Normative reference
    3 Definitions
    4 Principle
    5 Reagents and auxiliary materials
    6 Apparatus
    7 Sample
    8 Chromatograph operating conditions
    9 Data-processing system
    10 Checks of instrumental performance
    11 Procedure
    12 Test report
    13 Detection limit
    14 Precision
    Annexes
    A Test mixtures
    B General informations
    C Bibliography
    ZA Normative references to international publications
        with their corresponding European publications

    Abstract - (Show below) - (Hide below)

    Specifies a method for the determination of polychlorinated biphenyl (PCB) concentration in non-halogenated insulating liquids by high-resolution capillary column gas chromatography using an electron capture detector (ECD). Gives total PCB content; especially useful when a detailed analysis of PCB congeners is necessary.

    General Product Information - (Show below) - (Hide below)

    Committee CLC/SR 10
    Document Type Standard
    Publisher European Committee for Standards - Electrical
    Status Current

    Standards Referenced By This Book - (Show below) - (Hide below)

    BS 2000-462.3(2004) : 2004 PETROLEUM PRODUCTS AND USED OILS - DETERMINATION OF PCBS AND RELATED PRODUCTS - PART 3: DETERMINATION AND QUANTIFICATION OF POLYCHLORINATED TERPHENYLS (PCT) AND POLYCHLORINATED BENZYL TOLUENES (PCBT) CONTENT BY GAS CHROMATOGRAPHY (GC) USING AN ELECTRON CAPTURE DETECTOR (ECD)
    BS EN 60422:2013 Mineral insulating oils in electrical equipment. Supervision and maintenance guidance
    BS EN 15308:2016 Characterization of waste. Determination of selected polychlorinated biphenyls (PCB) in solid waste by gas chromatography with electron capture or mass spectrometric detection
    S.R. CLC/TR 50503:2010 GUIDELINES FOR THE INVENTORY CONTROL, MANAGEMENT, DECONTAMINATION AND/OR DISPOSAL OF ELECTRICAL EQUIPMENT AND INSULATING LIQUIDS CONTAINING PCBS
    DIN EN 16167:2012-11 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)
    I.S. EN 12766-3:2005 PETROLEUM PRODUCTS AND USED OILS - DETERMINATION OF PCBS AND RELATED PRODUCTS - PART 3: DETERMINATION AND QUANTIFICATION OF POLYCHLORINATED TERPHENYLS (PCT) AND POLYCHLORINATED BENZYL TOLUENES (PCBT) CONTENT BY GAS CHROMATOGRAPHY (GC) USING AN ELECTRON CAPTURE DETECTOR (ECD)
    EN 62701:2014 Fluids for electrotechnical applications - Recycled mineral insulating oils for transformers and switchgears
    EN 12766-2:2001 Petroleum products and used oils - Determination of PCBs and related products - Part 2: Calculation of polychlorinated biphenyl (PCB) content
    I.S. EN 60422:2013 MINERAL INSULATING OILS IN ELECTRICAL EQUIPMENT - SUPERVISION AND MAINTENANCE GUIDANCE (IEC 60422:2013 (EQV))
    UNI EN 16167 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)
    BS EN 12766-3:2004 Petroleum products and used oils. Determination of PCBs and related products Determination and quantification of polychlorinated terphenyls (PCT) and polychlorinated benzyl toluenes (PCBT) content by gas chromatography (GC) using an electron capture detector (ECD)
    EN 15308:2016 Characterization of waste - Determination of selected polychlorinated biphenyls (PCB) in solid waste by gas chromatography with electron capture or mass spectrometric detection
    UNE-EN 15308:2017 Characterization of waste - Determination of selected polychlorinated biphenyls (PCB) in solid waste by gas chromatography with electron capture or mass spectrometric detection
    05/30133366 DC : DRAFT MAY 2005 EN 5XXXX BTTF 116-1 - STANDARD FOR THE INVENTORY, CONTROL, MANAGEMENT, DECONTAMINATION AND/OR DISPOSAL OF ELECTRICAL EQUIPMENT AND INSULATING LIQUIDS CONTAINING PCBS
    BS EN 16167:2012 Sludge, treated biowaste and soil. Determination of polychlorinated biphenyls (PCB) by gas chromatography with mass selective detection (GC-MS) and gas chromatography with electron-capture detection (GC-ECD)
    06/30159746 DC : 0 BS EN 50503 - FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - STANDARD FOR THE INVENTORY CONTROL, MANAGEMENT, DECONTAMINATION AND/OR DISPOSAL OF ELECTRICAL EQUIPMENT AND INSULATING LIQUIDS CONTAINING PCBS
    BS EN 60296:2012 Fluids for electrotechnical applications. Unused mineral insulating oils for transformers and switchgear
    12/30231385 DC BS ISO 13876. Soil quality. Determination of polychlorinated biphenyls (PCB) by gas chromatography with mass selective detection (GC-MS) and gas chromatography with electron-capture detection (GC-ECD)
    PREN 15308 : DRAFT 2015 CHARACTERIZATION OF WASTE - DETERMINATION OF SELECTED POLYCHLORINATED BIPHENYLS (PCB) IN SOLID WASTE BY GAS CHROMATOGRAPHY WITH ELECTRON CAPTURE OR MASS SPECTROMETRIC DETECTION
    17/30364002 DC : 0 BS EN 16167 - SOIL, TREATED BIOWASTE AND SLUDGE - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)
    I.S. EN 62701:2014 FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - RECYCLED MINERAL INSULATING OILS FOR TRANSFORMERS AND SWITCHGEARS
    BS 2000-462.2(2001) : 2001 METHODS OF TEST FOR PETROLEUM AND ITS PRODUCTS - PETROLEUM PRODUCTS AND USED OILS - DETERMINATION OF PCBS AND RELATED PRODUCTS - CALCULATION OF POLYCHLORINATED BIPHENYL (PCB) CONTENT
    ISO 13876:2013 Soil quality — Determination of polychlorinated biphenyls (PCB) by gas chromatography with mass selective detection (GC-MS) and gas chromatography with electron-capture detection (GC-ECD)
    I.S. EN 12766-2:2001 PETROLEUM PRODUCTS AND USED OILS - DETERMINATION OF PCBS AND RELATED PRODUCTS - PART 2: CALCULATION OF POLYCHLORINATED BIPHENYL (PCB) CONTENT
    CEI EN 60296 : 2013 FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED MINERAL INSULATING OILS FOR TRANSFORMERS AND SWITCHGEAR
    EN 60296:2012 Fluids for electrotechnical applications - Unused mineral insulating oils for transformers and switchgear
    CEI EN 62770 : 2014 FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED NATURAL ESTERS FOR TRANSFORMERS AND SIMILAR ELECTRICAL EQUIPMENT
    05/30136951 DC : 0 EN 15308 - CHARACTERIZATION OF WASTE - DETERMINATION OF SELECTED POLYCHLORINATED BIPHENYLS (PCB) IN SOLID WASTE, SOIL AND SLUDGE BY USING CAPILLARY GAS CHROMATOGRAPHY WITH ELECTRON CAPTURE OR MASS SPECTROMETRIC DETECTION
    BS EN 62770:2014 Fluids for electrotechnical applications. Unused natural esters for transformers and similar electrical equipment
    10/30147454 DC : 0 BS EN 16167 - SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)
    I.S. EN 16167:2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRONCAPTURE DETECTION (GC-ECD)
    I.S. EN 62770:2014 FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED NATURAL ESTERS FOR TRANSFORMERS AND SIMILAR ELECTRICAL EQUIPMENT
    PREN 16167 : DRAFT 2017 SOIL, TREATED BIOWASTE AND SLUDGE - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)
    UNE-EN 60296:2012 Fluids for electrotechnical applications - Unused mineral insulating oils for transformers and switchgear
    UNE-EN 60422:2013 Mineral insulating oils in electrical equipment - Supervision and maintenance guidance
    UNE-EN 62770:2014 Fluids for electrotechnical applications - Unused natural esters for transformers and similar electrical equipment
    15/30330799 DC : 0 BS EN 15308 - CHARACTERIZATION OF WASTE - DETERMINATION OF SELECTED POLYCHLORINATED BIPHENYLS (PCB) IN SOLID WASTE BY GAS CHROMATOGRAPHY WITH ELECTRON CAPTURE OR MASS SPECTROMETRIC DETECTION
    CLC/TR 50503 : 2010 Guidelines for the inventory control, management, decontamination and/or disposal of electrical equipment and insulating liquids containing PCBs
    I.S. EN 15308:2016 CHARACTERIZATION OF WASTE - DETERMINATION OF SELECTED POLYCHLORINATED BIPHENYLS (PCB) IN SOLID WASTE BY GAS CHROMATOGRAPHY WITH ELECTRON CAPTURE OR MASS SPECTROMETRIC DETECTION
    I.S. EN 60296:2012 FLUIDS FOR ELECTROTECHNICAL APPLICATIONS - UNUSED MINERAL INSULATING OILS FOR TRANSFORMERS AND SWITCHGEAR (IEC 60296:2012 (EQV))
    EN 16167:2012 Sludge, treated biowaste and soil - Determination of polychlorinated biphenyls (PCB) by gas chromatography with mass selective detection (GC-MS) and gas chromatography with electron-capture detection (GC-ECD)
    DIN EN 12766-3:2005-02 Petroleum products and used oils - Determination of PCBs and related products - Part 3: Determination and quantification of polychlorinated terphenyls (PCT) and polychlorinated benzyl toluenes (PCBT) content by gas chromatography (GC) using an electron capture detector (ECD)
    BS EN 12766-2:2001 Methods of test for petroleum and its products. Petroleum products and used oils. Determination of PCBs and related products Calculation of polychlorinated biphenyl (PCB) content
    EN 12766-3:2004/AC:2007 PETROLEUM PRODUCTS AND USED OILS - DETERMINATION OF PCBS AND RELATED PRODUCTS - PART 3: DETERMINATION AND QUANTIFICATION OF POLYCHLORINATED TERPHENYLS (PCT) AND POLYCHLORINATED BENZYL TOLUENES (PCBT) CONTENT BY GAS CHROMATOGRAPHY (GC) USING AN ELECTRON CAPTURE DETECTOR (ECD)
    EN 62770:2014 Fluids for electrotechnical applications - Unused natural esters for transformers and similar electrical equipment
    EN 60422:2013 Mineral insulating oils in electrical equipment - Supervision and maintenance guidance
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