UNE-EN ISO 15753:2016
Current
The latest, up-to-date edition.
Animal and vegetable fats and oils - Determination of polycyclic aromatic hydrocarbons (ISO 15753:2016)
Hardcopy , PDF
Spanish, Castilian, English
13-07-2016
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Foreword
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Reagents and materials
6 Apparatus
7 Sampling
8 Sample preparation
9 Procedure for determination of PAHs from fats and oils:
General method
9.1 Preliminary remarks
9.2 Blank
9.3 Determination of recovery values (without matrix)
9.4 Extraction (liquid/liquid extraction)
9.5 Purification on C18-bonded phase cartridge
(solid/liquid extraction)
9.6 Purification on Florisil-bonded phase cartridge
(solid/liquid extraction)
10 Procedure for determination of PAHs from fats and
oils: Method specific for coconut oil
10.1 First extraction (liquid/liquid extraction)
10.2 Second extraction (liquid/liquid extraction)
10.3 Purification on C18-bonded phase cartridge
(solid/liquid extraction)
10.4 Purification on Florisil-bonded phase cartridge
(solid/liquid extraction)
11 High-performance liquid chromatography (HPLC)
11.1 Operating conditions
11.2 Detection parameters
11.3 Analysis of samples and standards
11.4 Confirmation of the presence of PAHs
12 Expression of results
13 Precision
13.1 Interlaboratory test
13.2 Repeatability
13.3 Reproducibility
14 Test report
Annex A (informative) Recovery values, flow charts,
chromatograms and injection sequences
Annex B (informative) Results of the interlaboratory test
Bibliography
States two methods for the determination of 15 polycyclic aromatic hydrocarbons (PAHs) in animal and vegetable fats and oils: - a general method, and - a method specific for coconut oil and vegetable oils with short-chain fatty acids.
| Committee |
CTN 34/SC 6
|
| DocumentType |
Standard
|
| Pages |
30
|
| PublisherName |
Asociacion Espanola de Normalizacion
|
| Status |
Current
|
| Supersedes |
| Standards | Relationship |
| ISO 15753:2016 | Identical |
| NBN EN ISO 15753 : 2016 | Identical |
| NF EN ISO 15753 : 2016 | Identical |
| NEN EN ISO 15753 : 2016 | Identical |
| NS EN ISO 15753 : 2016 | Identical |
| I.S. EN ISO 15753:2016 | Identical |
| SN EN ISO 15753 : 2006 AMD 1 2011 | Identical |
| UNI EN ISO 15753 : 2011 | Identical |
| BS EN ISO 15753:2016 | Identical |
| EN ISO 15753:2016 | Identical |
| DIN EN ISO 15753:2016-11 | Identical |
| ISO 5725-1:1994 | Accuracy (trueness and precision) of measurement methods and results — Part 1: General principles and definitions |
| ISO 5555:2001 | Animal and vegetable fats and oils — Sampling |
| ISO 1042:1998 | Laboratory glassware — One-mark volumetric flasks |
| ISO 835:2007 | Laboratory glassware — Graduated pipettes |
| ISO 4788:2005 | Laboratory glassware — Graduated measuring cylinders |
| ISO 7712:1983 | Laboratory glassware — Disposable Pasteur pipettes |
| ISO 5725-2:1994 | Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method |
| ISO 661:2003 | Animal and vegetable fats and oils — Preparation of test sample |
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