UNI CEN/TS 16181 : 2013
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
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SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCYCLIC AROMATIC HYDROCARBONS (PAH) BY GAS CHROMATOGRAPHY (GC) AND HIGH PERFORMANCE LIQUID CHROMATOGRAPHY (HPLC)
27-07-2022
16-05-2013
Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Interferences
6 Safety remarks
7 Reagents
8 Apparatus
9 Sample storage and preservation
10 Procedure
11 Performance characteristics
12 Precision
13 Test report
Annex A (informative) - Repeatability and
reproducibility data
Annex B (informative) - Examples of instrumental
conditions and chromatograms
Bibliography
Defines the quantitative determination of 16 polycyclic aromatic hydrocarbons (PAH) (see Table 2) in sludge, soil and treated biowaste using GC/MS and HPLC-UV-DAD/FLD covering a wide range of PAH contamination levels.
| DocumentType |
Technical Specification
|
| PublisherName |
Ente Nazionale Italiano di Unificazione (UNI)
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| Status |
Superseded
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| SupersededBy |
| Standards | Relationship |
| CEN/TS 16181:2013 | Identical |
| EN ISO 17993:2003 | Water quality - Determination of 15 polycyclic aromatic hydrocarbons (PAH) in water by HPLC with fluorescence detection after liquid-liquid extraction (ISO 17993:2002) |
| DIN 38414-23:2002-02 | GERMAN STANDARD METHODS FOR THE EXAMINATION OF WATER, WASTE WATER AND SLUDGE - SLUDGE AND SEDIMENTS (GROUP S) - PART 23: DETERMINATION OF 15 POLYCYCLIC AROMATIC HYDROCARBONS (PAH) BY HIGH PERFORMANCE LIQUID CHROMATOGRAPHY (HPLC) AND FLUORESCENCE DETECTION (S 23) |
| ISO 22892:2006 | Soil quality Guidelines for the identification of target compounds by gas chromatography and mass spectrometry |
| ISO 18287:2006 | Soil quality Determination of polycyclic aromatic hydrocarbons (PAH) Gas chromatographic method with mass spectrometric detection (GC-MS) |
| EN 15308:2016 | Characterization of waste - Determination of selected polychlorinated biphenyls (PCB) in solid waste by gas chromatography with electron capture or mass spectrometric detection |
| ISO 5667-15:2009 | Water quality — Sampling — Part 15: Guidance on the preservation and handling of sludge and sediment samples |
| ISO 17993:2002 | Water quality — Determination of 15 polycyclic aromatic hydrocarbons (PAH) in water by HPLC with fluorescence detection after liquid-liquid extraction |
| ISO 16720:2005 | Soil quality Pretreatment of samples by freeze-drying for subsequent analysis |
| ISO 28540:2011 | Water quality — Determination of 16 polycyclic aromatic hydrocarbons (PAH) in water — Method using gas chromatography with mass spectrometric detection (GC-MS) |
| EN ISO 16720:2007 | Soil quality - Pretreatment of samples by freeze-drying for subsequent analysis (ISO 16720:2005) |
| ISO 5725-2:1994 | Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method |
| ISO 8466-1:1990 | Water quality Calibration and evaluation of analytical methods and estimation of performance characteristics Part 1: Statistical evaluation of the linear calibration function |
| EN ISO 22892:2011 | Soil quality - Guidelines for the identification of target compounds by gas chromatography and mass spectrometry (ISO 22892:2006) |
| EN 15527:2008 | Characterization of waste - Determination of polycyclic aromatic hydrocarbons (PAH) in waste using gas chromatography mass spectrometry (GC/MS) |
| EN ISO 5667-15:2009 | Water quality - Sampling - Part 15: Guidance on the preservation and handling of sludge and sediment samples (ISO 5667-15:2009) |
| EN 15934:2012 | Sludge, treated biowaste, soil and waste - Calculation of dry matter fraction after determination of dry residue or water content |
| EN 16179:2012 | Sludge, treated biowaste and soil - Guidance for sample pretreatment |
| ISO 18512:2007 | Soil quality Guidance on long and short term storage of soil samples |
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