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  • ASTM D 482 : 2013

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    Superseded A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
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    Standard Test Method for Ash from Petroleum Products

    Available format(s):  Hardcopy, PDF

    Superseded date:  05-12-2019

    Language(s):  English

    Published date:  29-08-2013

    Publisher:  American Society for Testing and Materials

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    Abstract - (Show below) - (Hide below)

    1.1 This test method covers the determination of ash in the range 0.001–0.180 mass %, from distillate and residual fuels, gas turbine fuels, crude oils, lubricating oils, waxes, and other petroleum products, in which any ash-forming materials present are normally considered to be undesirable impurities or contaminants (Note 1).

    Scope - (Show below) - (Hide below)

    1.1This test method covers the determination of ash in the range 0.001–0.180 mass %, from distillate and residual fuels, gas turbine fuels, crude oils, lubricating oils, waxes, and other petroleum products, in which any ash-forming materials present are normally considered to be undesirable impurities or contaminants (Note 1). The test method is limited to petroleum products which are free from added ash-forming additives, including certain phosphorus compounds (Note 2).

    Note 1—In certain types of samples, all of the ash-forming metals are not retained quantitatively in the ash. This is particularly true of distillate oils, which require a special ash procedure in order to retain metals quantitatively.
    Note 2—This test method is not intended for the analysis of unused lubricating oils containing additives; for such samples use Test Method D874. Neither is it intended for the analysis of lubricating oils containing lead nor for used engine crankcase oils.

    1.2The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only. The preferred expression of the property is mass %.

    1.3This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

    General Product Information - (Show below) - (Hide below)

    Committee D 02
    Document Type Test Method
    Publisher American Society for Testing and Materials
    Status Superseded
    Superseded By
    Supersedes

    Standards Referenced By This Book - (Show below) - (Hide below)

    ASTM D 7666 : 2012 : R2019 Standard Specification for Triglyceride Burner Fuel
    ASTM D 4530 : 2015 : R2020 Standard Test Method for Determination of Carbon Residue (Micro Method)
    ASTM D 8048 : 2021 : REV A : EDT 1 Standard Test Method for Evaluation of Diesel Engine Oils in T-13 Diesel Engine
    ASTM D 7156 : 2019 Standard Test Method for Evaluation of Diesel Engine Oils in the T-11 Exhaust Gas Recirculation Diesel Engine
    ASTM E 2470 : 2022 Standard Specification for Polyester Grade Ethylene Glycol
    ASTM D 4042 : 1993 : R2019 Standard Test Method for Sampling and Testing for Ash and Total Iron in Steel Mill Dispersions of Rolling Oils
    ASTM D 7578 : 2020 Standard Guide for Calibration Requirements for Elemental Analysis of Petroleum Products and Lubricants
    ASTM D 7422 : 2022 Standard Test Method for Evaluation of Diesel Engine Oils in T-12 Exhaust Gas Recirculation Diesel Engine
    ASTM D 8074 : 2022 Standard Test Method for Evaluation of Diesel Engine Oils in DD13 Diesel Engine
    ASTM D 7876 : 2013 : R2018 Standard Practice for Practice for Sample Decomposition Using Microwave Heating (With or Without Prior Ashing) for Atomic Spectroscopic Elemental Determination in Petroleum Products and Lubricants
    ASTM F 715 : 2007 : R2018 Standard Test Methods for Coated Fabrics Used for Oil Spill Control and Storage
    ASTM D 6618 : 2016 Standard Test Method for Evaluation of Engine Oils in Diesel Four-Stroke Cycle Supercharged 1M-PC Single Cylinder Oil Test Engine
    ASTM D 7467 : 2020 : REV A Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 5967 : 2021 Standard Test Method for Evaluation of Diesel Engine Oils in T-8 Diesel Engine
    ASTM D 7455 : 2019 Standard Practice for Sample Preparation of Petroleum and Lubricant Products for Elemental Analysis
    ASTM D 7544 : 2012 : R2017 Standard Specification for Pyrolysis Liquid Biofuel
    ASTM D 6448 : 2016 : R2022 Standard Specification for Industrial Burner Fuels from Used Lubricating Oils
    ASTM C 726 : 2017 Standard Specification for Mineral Wool Roof Insulation Board
    ASTM D 396 : 2021 Standard Specification for Fuel Oils
    ASTM D 4868 : 2017 Standard Test Method for Estimation of Net and Gross Heat of Combustion of Hydrocarbon Burner and Diesel Fuels
    ASTM D 7583 : 2016 Standard Test Method for John Deere Coolant Cavitation Test
    ASTM D 4730 : 2013 : R2020 Standard Specification for Flooding Compounds for Telecommunications Wire and Cable
    ASTM D 524 : 2015 : R2019 Standard Test Method for Ramsbottom Carbon Residue of Petroleum Products
    ASTM D 874 : 2023 Standard Test Method for Sulfated Ash from Lubricating Oils and Additives
    ASTM D 189 : 2006 : R2019 Standard Test Method for Conradson Carbon Residue of Petroleum Products
    ASTM D 5966 : 2022 Standard Test Method for Evaluation of Engine Oils for Roller Follower Wear in Light-Duty Diesel Engine
    ASTM D 7549 : 2021 Standard Test Method for Evaluation of Heavy-Duty Engine Oils under High Output Conditions—Caterpillar C13 Test Procedure
    ASTM D 6681 : 2017 Standard Test Method for Evaluation of Engine Oils in a High Speed, Single-Cylinder Diesel Engine—Caterpillar 1P Test Procedure
    ASTM D 4252 : 1989 : R2017 Standard Test Methods for Chemical Analysis of Alcohol Ethoxylates and Alkylphenol Ethoxylates
    ASTM E 1119 : 2023 Standard Specification for Industrial Grade Ethylene Glycol
    ASTM D 7468 : 2022 Standard Test Method for Cummins ISM Test
    ASTM D 7484 : 2023 Standard Test Method for Evaluation of Automotive Engine Oils for Valve-Train Wear Performance in Cummins ISB Medium-Duty Diesel Engine
    ASTM D 975 : 2022 : REV A Standard Specification for Diesel Fuel
    ASTM D 8056 : 2018 Standard Guide for Elemental Analysis of Crude Oil
    ASTM D 6823 : 2008 : R2021 Standard Specification for Commercial Boiler Fuels With Used Lubricating Oils
    ASTM D 6750 : 2019 : EDT 1 Standard Test Methods for Evaluation of Engine Oils in a High-Speed, Single-Cylinder Diesel Engine—1K Procedure (0.4 % Fuel Sulfur) and 1N Procedure (0.04 % Fuel Sulfur)
    ASTM D 6710 : 2021 Standard Guide for Evaluation of Hydrocarbon-Based Quench Oil

    Standards Referencing This Book - (Show below) - (Hide below)

    ASTM D 4057 : 2019 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 6299 : 2010 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6299 : 2013 : EDT 1 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 4928 : 2000 Standard Test Methods for Water in Crude Oils by Coulometric Karl Fischer Titration
    ASTM D 4177 : 2016 : EDT 1 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 6299 : 2017 : REV A Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6299 : 2017 : REV B Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6299 : 2009 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 4177 : 1995 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 4057 : 2012 : R2018 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 6299 : 2013 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6792 : 2006 Standard Guide for Quality System in Petroleum Products and Lubricants Testing Laboratories
    ASTM D 6792 : 2004 Standard Guide for Quality System in Petroleum Products and Lubricants Testing Laboratories
    ASTM D 6299 : 2010 : EDT 1 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 4057 : 1981 : EDT 2 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 6792 : 2004 : REV A Standard Guide for Quality System in Petroleum Products and Lubricants Testing Laboratories
    ASTM D 4928 : 2000 : EDT 1 Standard Test Methods for Water in Crude Oils by Coulometric Karl Fischer Titration
    ASTM D 6792 : 2005 Standard Guide for Quality System in Petroleum Products and Lubricants Testing Laboratories
    ASTM D 6299 : 2000 Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6299 : 2010 : EDT 2 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6299 : 2016 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 4057 : 2006 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 4177 : 2015 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 4057 : 2012 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 6299 : 2000 : REV A Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6792 : 2013 Standard Practice for Quality System in Petroleum Products and Lubricants Testing Laboratories
    ASTM D 6792 : 2017 Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
    ASTM D 4928 : 2000 : R2010 Standard Test Methods for Water in Crude Oils by Coulometric Karl Fischer Titration
    ASTM D 4928 : 2000 : R2005 Standard Test Methods for Water in Crude Oils by Coulometric Karl Fischer Titration
    ASTM D 6792 : 2007 Standard Practice for Quality System in Petroleum Products and Lubricants Testing Laboratories
    ASTM D 4177 : 1995 : R2010 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 6299 : 2008 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 4177 : 1995 : R2000 Standard Practice for Automatic Sampling of Peroleum and Petroleum Products
    ASTM D 6299 : 2002 : EDT 1 Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 4928 : 2011 Standard Test Method for Water in Crude Oils by Coulometric Karl Fischer Titration
    ASTM D 4928 : 2012 : R2018 Standard Test Method for Water in Crude Oils by Coulometric Karl Fischer Titration
    ASTM D 4177 : 2016 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 6792 : 2003 Standard Guide for Quality System in Petroleum Products and Lubricants Testing Laboratories
    ASTM D 4177 : 1995 : R2005 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 6792 : 2002 Standard Guide for A Quality System in Petroleum Products and Lubricants Testing Laboratories
    ASTM D 6299 : 2007 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 4928 : 2012 Standard Test Method for Water in Crude Oils by Coulometric Karl Fischer Titration
    ASTM D 6299 : 2007 : EDT 1 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 4057 : 1995 : R2000 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 6299 : 2017 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 4177 : 2015 : REV A Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 4057 : 2006 : R2011 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 6299 : 2002 Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance
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