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ASTM D 4972 : 2019

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by

Standard Test Methods for pH of Soils

Available format(s)

Hardcopy , PDF

Superseded date

10-08-2024

Language(s)

English

Published date

01-05-2019

€67.30
Excluding VAT

1.1 These test methods cover the measurement of the pH of soils that will pass the 2.00 mm (No. 10) sieve.

Committee
D 18
DocumentType
Test Method
Pages
6
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

1.1These test methods cover the measurement of the pH of soils that will pass the 2.00 mm (No. 10) sieve. Such measurements are used in the agricultural, environmental, geotechnical, and natural resources fields. This measurement determines the degree of acidity or alkalinity in soil materials suspended in water and a 0.01 M calcium chloride solution. Measurements in both liquids are necessary to fully define the soil's pH. This variable is useful in determining the solubility of soil minerals and the mobility of ions in the soil and assessing the viability of the soil-plant environment. A more detailed discussion of the usefulness of this parameter is given in Refs (1-6)2.

1.2Two methods for measuring the pH of soils are provided. The method to be used shall be specified by the requesting authority. When no method is specified, Method A shall be used. The pH is determined in test water and a calcium chloride solution for both methods.

1.2.1Method A—The pH is measured using a potentiometer having a pH sensitive electrode system. This method can be used for any application and must be used when the application warrants a higher level of resolution.

1.2.2Method B—The pH is measured using pH sensitive paper. This method can be used for any application, however, because paper typically has a lower resolution, it provides an approximate estimate of the pH of the soil and should not be used when the application requires a higher level of resolution (Note 1).

Note 1:For example, paper with a sensitivity to the nearest 1 pH unit placed into a buffer solution of 4 should indicate a pH of 4, however, it would not indicate if the pH is 4.449 or 3.449.

1.3Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.4All measured and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026.

1.4.1The procedures used to specify how data are collected/recorded and calculated in the standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of these test methods to consider significant digits used in analysis methods for engineering data.

1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.6This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D 2976 : 2015 Standard Test Method for pH of Peat Materials
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ASTM D 5988 : 2018 Standard Test Method for Determining Aerobic Biodegradation of Plastic Materials in Soil
ASTM F 3339 : 2020 Standard Guide for Construction or Renovation of Native-soil Athletic Fields
ASTM D 2976 : 2022 : REV A Standard Test Method for pH of Peat Materials
ASTM D 8151 : 2019 : EDT 1 Standard Practice for Obtaining Rainfall Runoff from Unvegetated Rolled and Hydraulic Erosion Control Products (RECPs and HECPs) for Acute Ecotoxicity Testing
ASTM D 7294 : 2013 : R2021 Standard Guide for Collecting Treatment Process Design Data at a Contaminated Site—A Site Contaminated with Chemicals of Interest
ASTM F 2396 : 2011 : R2019 Standard Guide for Construction of High Performance Sand-Based Rootzones for Athletic Fields
ASTM E 2277 : 2014(R2019) Standard Guide for Design and Construction of Coal Ash Structural Fills
ASTM E 2243 : 2013 : R2019 Standard Guide for Use of Coal Combustion Products (CCPs) for Surface Mine Reclamation: Re-contouring and Highwall Reclamation
ASTM D 7100 : 2011 : R2020 Standard Test Method for Hydraulic Conductivity Compatibility Testing of Soils with Aqueous Solutions
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ASTM E 2278 : 2013 : R2019 Standard Guide for Use of Coal Combustion Products (CCPs) for Surface Mine Reclamation: Revegetation and Mitigation of Acid Mine Drainage
ASTM D 5268 : 2023 Standard Specification for Topsoil Used for Landscaping and Construction Purposes
ASTM F 2747 : 2019 Standard Guide for Construction of Sand-based Rootzones for Golf Putting Greens and Tees
ASTM E 2060 : 2022 Standard Guide for Use of Coal Combustion Products for Solidification/Stabilization of Inorganic Wastes

ASTM D 2487 : 2017 : EDT 1 Standard Practice for Classification of Soils for Engineering Purposes (Unified Soil Classification System)
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ASTM G 51 : 2018 Standard Test Method for Measuring pH of Soil for Use in Corrosion Testing
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ASTM D 653 : 2007 Standard Terminology Relating to Soil, Rock, and Contained Fluids
ASTM D 4753 : 2015 Standard Guide for Evaluating, Selecting, and Specifying Balances and Standard Masses for Use in Soil, Rock, and Construction Materials Testing
ASTM D 3740 : 2012 Standard Practice for Minimum Requirements for Agencies Engaged in Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
ASTM C 670 : 2024 Standard Practice for Preparing Precision and Bias Statements for Test Methods for Construction Materials
ASTM D 3740 : 2023 Standard Practice for Minimum Requirements for Agencies Engaged in Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
ASTM D 3740 : 2019 Standard Practice for Minimum Requirements for Agencies Engaged in Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
ASTM D 3740 : 2004 : REV A : EDT 1 Standard Practice for Minimum Requirements for Agencies Engaged in the Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
ASTM D 2488 : 1969 : R1975 Recommended Practice for Description Of Soils (Visual-Manual Procedure)
ASTM D 3740 : 2008 Standard Practice for Minimum Requirements for Agencies Engaged in Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
ASTM D 4753 : 2024 Standard Guide for Evaluating, Selecting, and Specifying Balances and Standard Masses for Use in Soil, Rock, and Construction Materials Testing
ASTM D 1193 : 1977 : R1983 : EDT 1 Standard Specification for Reagent Water
ASTM D 6026 : 2013 Standard Practice for Using Significant Digits in Geotechnical Data
ASTM D 6026 : 2006 Standard Practice for Using Significant Digits in Geotechnical Data
ASTM D 2488 : 2017 Standard Practice for Description and Identification of Soils (Visual-Manual Procedures)
ASTM D 3740 : 1999 : REV C Standard Practice for Minimum Requirements for Agencies Engaged in the Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
ASTM D 653 : 2024 Standard Terminology Relating to Soil, Rock, and Contained Fluids
ASTM D 1193 : 2006 : R2011 Standard Specification for Reagent Water
ASTM D 6913 : 2004 Standard Test Methods for Particle-Size Distribution (Gradation) of Soils Using Sieve Analysis
ASTM D 653 : 2022 Standard Terminology Relating to Soil, Rock, and Contained Fluids
ASTM D 4753 : 1995 Standard Specification for Evaluating, Selecting, and Specifying Balances and Scales for Use in Soil, Rock, and Construction Materials Testing
ASTM D 653 : 2020 : EDT 1 Standard Terminology Relating to Soil, Rock, and Contained Fluids
ASTM D 6026 : 1999 Standard Practice for Using Significant Digits in Geotechnical Data
ASTM D 3740 : 2011 Standard Practice for Minimum Requirements for Agencies Engaged in Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
ASTM D 2488 : 2009 Standard Practice for Description and Identification of Soils (Visual-Manual Procedure)
ASTM D 6026 : 2001 : EDT 1 Standard Practice for Using Significant Digits in Geotechnical Data
ASTM D 1193 : 1991 Standard Specification for Reagent Water
ASTM D 3740 : 2010 Standard Practice for Minimum Requirements for Agencies Engaged in Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
ASTM D 653 : 2021 : REV A Standard Terminology Relating to Soil, Rock, and Contained Fluids
ASTM D 6913 : 2004 : R2009 : EDT 1 Standard Test Methods for Particle-Size Distribution (Gradation) of Soils Using Sieve Analysis
ASTM D 6026 : 1996 Standard Practice for Using Significant Digits in Geotechnical Data
ASTM D 3740 : 2004 : REV A Standard Practice for Minimum Requirements for Agencies Engaged in the Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
ASTM D 4753 : 2007 Standard Guide for Evaluating, Selecting, and Specifying Balances and Standard Masses for Use in Soil, Rock, and Construction Materials Testing
ASTM D 3740 : 2001 Standard Practice for Minimum Requirements for Agencies Engaged in the Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
ASTM D 2488 : 2000 Standard Practice for Description and Identification of Soils (Visual-Manual Procedure)
ASTM D 2487 : 2006 : EDT 1 Standard Practice for Classification of Soils for Engineering Purposes (Unified Soil Classification System)
ASTM C 670 : 2024 : REV A Standard Practice for Preparing Precision and Bias Statements for Test Methods for Construction Materials
ASTM D 653 : 2021 Standard Terminology Relating to Soil, Rock, and Contained Fluids
ASTM D 653 : 2021 : REV B Standard Terminology Relating to Soil, Rock, and Contained Fluids
ASTM D 6026 : 1996 : EDT 1 Standard Practice for Using Significant Digits in Geotechnical Data
ASTM D 3740 : 2012 : REV A Standard Practice for Minimum Requirements for Agencies Engaged in Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
ASTM D 3740 : 2003 Standard Practice for Minimum Requirements for Agencies Engaged in the Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
ASTM D 2487 : 2010 Standard Practice for Classification of Soils for Engineering Purposes (Unified Soil Classification System)
ASTM D 1193 : 1970 Standard Specification For Reagent Water
ASTM D 2487 : 2000 Standard Classification of Soils for Engineering Purposes (Unified Soil Classification System)
ASTM D 1193 : 2006 Standard Specification for Reagent Water
ASTM D 2487 : 2006 Standard Practice for Classification of Soils for Engineering Purposes (Unified Soil Classification System)
ASTM D 4220/D4220M : 2014 Standard Practices for Preserving and Transporting Soil Samples (Withdrawn 2023)
ASTM D 6026 : 2021 Standard Practice for Using Significant Digits and Data Records in Geotechnical Data
ASTM D 1193 : 1999 Standard Specification for Reagent Water
ASTM D 6026 : 2001 Standard Practice for Using Significant Digits in Geotechnical Data
ASTM D 2487 : 2011 Standard Practice for Classification of Soils for Engineering Purposes (Unified Soil Classification System)
ASTM D 6913 : 2004 : R2009 Standard Test Methods for Particle-Size Distribution (Gradation) of Soils Using Sieve Analysis
ASTM D 1193 : 2006 : R2018 Standard Specification for Reagent Water
ASTM C 670 : 2015 Standard Practice for Preparing Precision and Bias Statements for Test Methods for Construction Materials
ASTM D 2487 : 2017 Standard Practice for Classification of Soils for Engineering Purposes (Unified Soil Classification System)
ASTM D 2488 : 2009 : REV A Standard Practice for Description and Identification of Soils (Visual-Manual Procedure)
ASTM D 2488 : 2017 : EDT 1 Standard Practice for Description and Identification of Soils (Visual-Manual Procedures)
ASTM D 2488 : 2006 Standard Practice for Description and Identification of Soils (Visual-Manual Procedure)
ASTM D 6913 : 2004 : EDT 1 Standard Test Methods for Particle-Size Distribution (Gradation) of Soils Using Sieve Analysis
ASTM D 6913 : 2004 : EDT 2 Standard Test Methods for Particle-Size Distribution (Gradation) of Soils Using Sieve Analysis
ASTM D 3740 : 2004 Standard Practice for Minimum Requirements for Agencies Engaged in the Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
ASTM D 2487 : 1969 : R1975 Standard Test Method for Classification Of Soils For Engineering Purposes

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