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ASTM D 5837 : 2015

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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Standard Test Method for Furanic Compounds in Electrical Insulating Liquids by High-Performance Liquid Chromatography (HPLC)

Available format(s)

Hardcopy , PDF

Superseded date

17-01-2024

Language(s)

English

Published date

20-10-2015

€67.30
Excluding VAT

This test method covers the determination in electrical insulating liquids of products of the degradation of cellulosic materials such as paper, pressboard, and cotton materials typically found as insulating materials in electrical equipment.

Committee
D 27
DocumentType
Test Method
Pages
9
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

1.1This test method covers the determination in electrical insulating liquids of products of the degradation of cellulosic materials such as paper, pressboard, and cotton materials typically found as insulating materials in electrical equipment. These degradation products are substituted furan derivatives, commonly referred to as furanic compounds or furans. This test method allows either liquid/liquid or solid phase extraction (SPE) of the furanic compounds from the sample matrix followed by analysis for specific furanic compounds by HPLC or direct injection for analysis of specific furanic compounds by HPLC.

1.2The individual furanic compounds that may be identified and quantified include the following:

5-hydroxymethyl-2-furaldehyde

furfuryl alcohol

2-furaldehyde

2-acetylfuran

5-methyl-2-furaldehyde

1.3The direct injection method generally has a higher limit of detection, especially for furfuryl alcohol. Greater interference for furfuryl alcohol may be expected when using the direct injection method as opposed to extraction methods.

1.4This test method has been used to successfully test for furanic compounds in mineral insulating oil, silicone fluid, high fire point electrical insulating oils of mineral origin, askarels, and perchloroethylene-based dielectric fluids.

1.5The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.6This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

NFPA 70B:2023 Standard for Electrical Equipment Maintenance
ASTM D 117 : 2018 Standard Guide for Sampling, Test Methods, and Specifications for Electrical Insulating Liquids
ASTM D 5282 : 2005 : R2012 Standard Test Methods for Compatibility of Construction Material with Silicone Fluid Used for Electrical Insulation
ASTM D 3487 : 2016 : EDT 1 Standard Specification for Mineral Insulating Oil Used in Electrical Apparatus
ANSI/NETA MTS:2023+ERR:2023 Standard for Maintenance Testing Specifications for Electrical Power Equipment and Systems
ASTM D 8086 : 2020 Standard Test Method for Determination of Methanol and Ethanol in Electrical Insulating Liquids of Petroleum Origin by Headspace (HS)-Gas Chromatography (GC) Using Mass Spectrometry (MS) or Flame Ionization Detection (FID)
ASTM D 8180 : 2023 Standard Specification for Rerefined Mineral Insulating Liquid Used in Electrical Apparatus
ASTM D 5282 : 2005 : R2020 Standard Test Methods for Compatibility of Construction Material with Silicone Fluid Used for Electrical Insulation
ASTM D 117 : 2022 Standard Guide for Sampling, Test Methods, and Specifications for Electrical Insulating Liquids

ASTM D 923 : 2015 : R2023 Standard Practices for Sampling Electrical Insulating Liquids
ASTM D 3487 : 2016 Standard Specification for Mineral Insulating Oil Used in Electrical Apparatus
ASTM D 3612 : 2002 : R2017 Standard Test Method for Analysis of Gases Dissolved in Electrical Insulating Oil by Gas Chromatography
ASTM D 3612 : 2002 : EDT 1 Standard Test Method for Analysis of Gases Dissolved in Electrical Insulating Oil by Gas Chromatography
ASTM D 3612 : 2002 Standard Test Method for Analysis of Gases Dissolved in Electrical Insulating Oil by Gas Chromatography
ASTM D 923 : 2015 Standard Practices for Sampling Electrical Insulating Liquids
ASTM D 3487 : 2000 Standard Specification for Mineral Insulating Oil Used in Electrical Apparatus
ASTM D 3487 : 2008 Standard Specification for Mineral Insulating Oil Used in Electrical Apparatus
ASTM D 3612 : 1996 Standard Test Method for Analysis of Gases Dissolved in Electrical Insulating Oil by Gas Chromatography
ASTM D 3487 : 2009 Standard Specification for Mineral Insulating Oil Used in Electrical Apparatus
ASTM D 3487 : 2000 : R2006 Standard Specification for Mineral Insulating Oil Used in Electrical Apparatus
ASTM D 3612 : 2001 Standard Test Method for Analysis of Gases Dissolved in Electrical Insulating Oil by Gas Chromatography
ASTM D 3487 : 1988 : R1993 Standard Specification for Mineral Insulating Oil Used in Electrical Apparatus
ASTM D 3487 : 2016 : EDT 1 Standard Specification for Mineral Insulating Oil Used in Electrical Apparatus
ASTM D 3612 : 2002 : R2009 Standard Test Method for Analysis of Gases Dissolved in Electrical Insulating Oil by Gas Chromatography

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