• ASTM D 923 : 2015

    Superseded A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

    Standard Practices for Sampling Electrical Insulating Liquids

    Available format(s):  Hardcopy, PDF

    Superseded date:  04-01-2024

    Language(s):  English

    Published date:  20-10-2015

    Publisher:  American Society for Testing and Materials

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    Abstract - (Show below) - (Hide below)

    These practices cover sampling of new electrical insulating liquids including oils, askarels, silicones, synthetic liquids, and natural ester insulating liquids as well as those insulating liquids in service or subsequent to service in cables, transformers, circuit breakers, and other electrical apparatus.

    Scope - (Show below) - (Hide below)

    1.1These practices cover sampling of new electrical insulating liquids including oils, askarels, silicones, synthetic liquids, and natural ester insulating liquids as well as those insulating liquids in service or subsequent to service in cables, transformers, circuit breakers, and other electrical apparatus. These practices apply to liquids having a viscosity of less than 6.476 × 10-4 m2/s (540 cSt) at 40°C (104°F).

    1.2Representative samples of electrical insulating liquids are taken for test specimens so that the quality pertinent to their use may be determined. The quality in different portions of a given container, or the average quality of the whole bulk may be ascertained if desired.

    1.3The values stated in SI units are regarded as the standard where applicable. Inch pound units are used where there is no SI equivalent.

    1.4These practices also include special techniques and devices for sampling for dissolved gases-in-oil (DGA) (D3612), water (D1533) and particles (D6786).

    1.5For ease of use, this document has been indexed as follows:

    Section Title

    Section/Paragraph

    Mandatory Conditions and General Information

    Section 5

    Description of Sampling Devices and Containers

    Section 6, Annex A1, Appendix X2

    Most Frequently Used Sampling Techniques for Electrical Apparatus

    Collecting Samples from Electrical Equipment Using Bottles  and Cans

    Section 7, Appendix X1, Appendix X2

    Collecting Samples from Electrical Equipment Using Glass  Syringes (DGA and Water Analysis)

    Section 8

    Collecting Samples from Electrical Equipment Using  Stainless Steel Cylinders (DGA and Water Analysis)

    Section 9

    Sampling of Cans, Drums, Tank Cars, Tank Trucks and  Small Electrical Equipment

    Sampling Using the Dip-Type Device (drum thief)

    Section 10

    Sampling Using the Pressure-Type Device

    Section 11, Annex A1.1

    Sampling Using the Tank Car-Type Device

    Section 12, Annex A1.2

    Sampling Cable Feeders

     Mandatory Conditions

    Section 13

     General Considerations

    Section 14

     Sampling Using the Manifold-Type Device

    Section 15, Annex A1.3

    Cleaning, Preparation, Storage, and Handling of Sampling  Containers

    Section 16

    Storage, Packaging and Shipping of Samples

    Section 17

    Cleaning and Storage of Sampling Devices

    Section 18

    Sample Information

    Section 19

    Mandatory Information—Construction of Sampling Devices

    Annex A1

    Determination of Electrical Apparatus Temperature

    Appendix X1

    Sample Container Types

    Appendix X2

    1.6Handle askarels containing polychlorinated biphenyls (PCBs) according to federal and local regulations existing for that country. For example, the federal regulations concerning PCBs in the United States can be found in 40 CFR Part 761.

    1.7Properly contain, package and dispose of any liquid or material resulting from the use of these practices in a manner that is in accordance with local and state regulations specific to the country in which the samples are taken.

    1.8This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific warning statements are given in 1.6, 1.7, Section 5, 10.1, 13.2, 15.2.3, Section 16, and 18.2. These practices involve close contact with the electrical insulating liquids being sampled as well as liquids and other materials used to clean the sampling tools and devices. When required, or as a matter of diligence to personal safety, use personal protective equipment (PPE).

    General Product Information - (Show below) - (Hide below)

    Committee D 27
    Document Type Standard Practice
    Publisher American Society for Testing and Materials
    Status Superseded
    Superseded By
    Supersedes

    Standards Referenced By This Book - (Show below) - (Hide below)

    NFPA 70B:2023 Standard for Electrical Equipment Maintenance
    ASTM D 4059 : 2000 : R2018 Standard Test Method for Analysis of Polychlorinated Biphenyls in Insulating Liquids by Gas Chromatography
    ASTM D 971 : 2020 Standard Test Method for Interfacial Tension of Insulating Liquids Against Water by the Ring Method
    ASTM D 8180 : 2023 Standard Specification for Rerefined Mineral Insulating Liquid Used in Electrical Apparatus
    ASTM D 4652 : 2020 Standard Specification for Silicone Liquid Used for Electrical Insulation
    ASTM D 2668 : 2007 : R2021 Standard Test Method for 2,6-di-tert-Butyl- p-Cresol and 2,6-di-tert-Butyl Phenol in Electrical Insulating Oil by Infrared Absorption
    ASTM D 6871 : 2017 Standard Specification for Natural (Vegetable Oil) Ester Fluids Used in Electrical Apparatus
    ASTM D 1816 : 2012(R2019) Standard Test Method for Dielectric Breakdown Voltage of Insulating Liquids Using VDE Electrodes
    ASTM D 1934 : 2020 Standard Test Method for Oxidative Aging of Electrical Insulating Liquids by Open-Beaker Method
    ASTM D 2140 : 2023 Standard Practice for Calculating Carbon-Type Composition of Insulating Oils of Petroleum Origin
    ASTM D 2225 : 2020 Standard Test Methods for Silicone Liquids Used for Electrical Insulation
    ASTM D 117 : 2022 Standard Guide for Sampling, Test Methods, and Specifications for Electrical Insulating Liquids
    ASTM D 1275 : 2015 Standard Test Method for Corrosive Sulfur in Electrical Insulating Liquids
    ASTM D 5837 : 2015 Standard Test Method for Furanic Compounds in Electrical Insulating Liquids by High-Performance Liquid Chromatography (HPLC)
    ASTM D 1533 : 2020 Standard Test Method for Water in Insulating Liquids by Coulometric Karl Fischer Titration
    ASTM D 7151 : 2015 Standard Test Method for Determination of Elements in Insulating Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
    ASTM D 8086 : 2020 Standard Test Method for Determination of Methanol and Ethanol in Electrical Insulating Liquids of Petroleum Origin by Headspace (HS)-Gas Chromatography (GC) Using Mass Spectrometry (MS) or Flame Ionization Detection (FID)
    ASTM D 8112 : 2022 Standard Guide for Obtaining In-Service Samples of Turbine Operation Related Lubricating Fluid
    ASTM D 3487 : 2016 : EDT 1 Standard Specification for Mineral Insulating Oil Used in Electrical Apparatus
    ASTM D 877/D877M : 2019 Standard Test Method for Dielectric Breakdown Voltage of Insulating Liquids Using Disk Electrodes
    ASTM D 924 : 2023 Standard Test Method for Dissipation Factor (or Power Factor) and Relative Permittivity (Dielectric Constant) of Electrical Insulating Liquids
    ASTM D 4768 : 2011 : R2019 Standard Test Method for Analysis of 2,6-Ditertiary-Butyl Para-Cresol and 2,6-Ditertiary-Butyl Phenol in Insulating Liquids by Gas Chromatography
    ASTM D 5222 : 2023 Standard Specification for Less Flammable High Molecular Weight Hydrocarbon Mineral Electrical Insulating Liquids
    ASTM D 4733 : 2017 Standard Test Methods for Solventless Electrical Insulating Varnishes
    ASTM D 8240 : 2022 : EDT 1 Standard Specification for Less-Flammable Synthetic Ester Liquids Used in Electrical Apparatus
    ASTM D 2144 : 2007 : R2021 Standard Practices for Examination of Electrical Insulating Oils by Infrared Absorption
    ASTM D 3300 : 2020 Standard Test Method for Dielectric Breakdown Voltage of Insulating Liquids Under Impulse Conditions
    ASTM D 1169 : 2019 : REV A Standard Test Method for Specific Resistance (Resistivity) of Electrical Insulating Liquids

    Standards Referencing This Book - (Show below) - (Hide below)

    ASTM D 4057 : 2019 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 4057 : 1995 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 1933 : 2003 : R2008 Standard Specification for Nitrogen Gas as an Electrical Insulating Material
    ASTM D 1533 : 2012 Standard Test Method for Water in Insulating Liquids by Coulometric Karl Fischer Titration
    ASTM D 4057 : 2012 : R2018 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 1933 : 1997 Standard Specification for Nitrogen Gas as an Electrical Insulating Material
    ASTM D 3612 : 2002 : R2017 Standard Test Method for Analysis of Gases Dissolved in Electrical Insulating Oil by Gas Chromatography
    ASTM D 4057 : 1981 : EDT 2 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 3612 : 2002 : EDT 1 Standard Test Method for Analysis of Gases Dissolved in Electrical Insulating Oil by Gas Chromatography
    ASTM D 1933 : 2003 : R2017 Standard Specification for Nitrogen Gas as an Electrical Insulating Material
    ASTM D 3612 : 2002 Standard Test Method for Analysis of Gases Dissolved in Electrical Insulating Oil by Gas Chromatography
    ASTM D 4057 : 2006 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 1533 : 2000 : R2005 Standard Test Method for Water in Insulating Liquids by Coulometric Karl Fischer Titration
    ASTM D 1933 : 2003 Standard Specification for Nitrogen Gas as an Electrical Insulating Material
    ASTM D 4057 : 2012 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 6786 : 2015 Standard Test Method for Particle Count in Mineral Insulating Oil Using Automatic Optical Particle Counters
    ASTM D 3612 : 1996 Standard Test Method for Analysis of Gases Dissolved in Electrical Insulating Oil by Gas Chromatography
    ASTM D 3612 : 2001 Standard Test Method for Analysis of Gases Dissolved in Electrical Insulating Oil by Gas Chromatography
    ASTM D 6786 : 2008 Standard Test Method for Particle Count in Mineral Insulating Oil Using Automatic Optical Particle Counters
    ASTM D 4057 : 2022 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 6786 : 2002 Standard Test Method for Particle Count in Mineral Insulating Oil Using Automatic Optical Particle Counters
    ASTM D 6786 : 2007 Standard Test Method for Particle Count in Mineral Insulating Oil Using Automatic Optical Particle Counters
    ASTM D 4057 : 1995 : R2000 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 4057 : 2006 : R2011 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 1533 : 2000 Standard Test Method for Water in Insulating Liquids by Coulometric Karl Fischer Titration
    ASTM D 3612 : 2002 : R2009 Standard Test Method for Analysis of Gases Dissolved in Electrical Insulating Oil by Gas Chromatography
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