Skip to content
Please enter a keyword to search

  • ASTM D 6750 : 2019

    View superseded by
    Superseded A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
    View superseded by

    Standard Test Methods for Evaluation of Engine Oils in a High-Speed, Single-Cylinder Diesel Engine—1K Procedure (0.4 % Fuel Sulfur) and 1N Procedure (0.04 % Fuel Sulfur)

    Available format(s):  Hardcopy, PDF

    Superseded date:  14-07-2023

    Language(s):  English

    Published date:  06-06-2019

    Publisher:  American Society for Testing and Materials

    Add To Cart

    Abstract - (Show below) - (Hide below)

    These test methods cover the performance of engine oils intended for use in certain diesel engines.

    Scope - (Show below) - (Hide below)

    1.1These test methods cover the performance of engine oils intended for use in certain diesel engines. They are performed in a standardized high-speed, single-cylinder diesel engine by either the 1K (0.4 % mass fuel sulfur) or 1N (0.04 % mass fuel sulfur) procedure.3 The only difference in the two test methods is the fuel used. Piston and ring groove deposit-forming tendency and oil consumption are measured. Also, the piston, the rings, and the liner are examined for distress and the rings for mobility. These test methods are required to evaluate oils intended to satisfy API service categories CF-4 and CH-4 for 1K, and CG-4 for 1N of Specification D4485.

    1.2These test methods, although based on the original Caterpillar 1K/1N procedures,3 also embody TMC information letters issued before these test methods were first published. These test methods are subject to frequent change. Until the next revision of these test methods, TMC will update changes in these test methods by the issuance of information letters which shall be obtained from TMC (see Annex A1 – Annex A4).

    1.3The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

    1.3.1Exception—Where there is no direct SI equivalent such as screw threads, national pipe threads/diameters, tubing size, or single source equipment specified. Also Brake Specific Fuel Consumption is measured in kilograms per kilowatthour.

    1.4The following is the Table of Contents:

    Section

    Introduction

    Scope

    1

    Referenced documents

    2

    Terminology

    3

    Summary of Test Methods

    4

    Significance and Use

    5

    Apparatus

    6

    General Laboratory Requirements

    6.1

    Test Engine

    6.2

    Test Engine Accessories and Parts

    6.3

    Reagents and Materials

    7

    Test Oil Sample Requirements

    8

    Preparation of Apparatus

    9

    Engine Inspection

    9.1

    Engine Pre-Test Lubrication System Flush

    9.2

    Engine Pre-Test Measurements and Inspections

    9.3

    Engine Assembly

    9.4

    Pressure Testing of Fuel System Assembly

    9.5

    Calibration of Engine Test Stand

    10

    General Requirements and Frequency of Calibration

    10.1

    Runs

    10.2

    Specified Test Parameters

    10.3

    Calibration Test Acceptance Criteria

    10.4

    Action on Rejection of Calibration Test

    10.5

    Test Numbering

    10.6

    Reference Oils

    10.7

    Severity Adjustments

    10.8

    Engine Operating Procedure

    11

    Engine Run-In

    11.1

    Cool-Down Procedure

    11.2

    Warm-Up Procedure

    11.3

    Operating Conditions and Oil Additions

    11.4

    Measurement of Oil Consumption

    11.5

    Sampling Used Oil

    11.6

    Shutdowns, Lost Time and Off Tolerance Conditions

    11.7

    Recording of Exhaust Temperature

    11.8

    Air-Fuel Ratio Measurement

    11.9

    Recording of Engine Conditions

    11.10

    Humidity Requirements/Calibration/Measurement

    11.11

    Inspections, Photographs and Measurements

    12

    Reference to Reporting Form

    12.1

    Pre-Test Measurements of Engine Parts

    12.2

    Post-Test Information

    12.3

    Oil Inspections

    12.4

    Report

    13

    General Directions

    13.1

    Electronic Transmission of Test Results (Optional)

    13.12

    Reporting Calibration Test Results

    13.13

    Precision and Bias

    14

    Keywords

    15

    ANNEXES

    ASTM Test Monitoring Center Organization

    Annex A1

    ASTM Test Monitoring Center: Calibration Procedures

    Annex A2

    ASTM Test Monitoring Center: Maintenance Activities

    Annex A3

    ASTM Test Monitoring Center: Related Information

    Annex A4

    Specifications for Test Engine and Engine Build

    Annex A5

    Intake Air System Details

    Annex A6

    Exhaust System Details

    Annex A7

    Cooling System Details

    Annex A8

    Oil System Modifications and Instrument Locations

    Annex A9

    Other Pressure and Temperature Measurement Locations

    Annex A10

    Oil Consumption Linear Regression Method

    Annex A11

    Test Fuel Specifications

    Annex A12

    Lubrication System, Flush Apparatus and Procedure

    Annex A13

    Engine Operating Conditions

    Annex A14

    Procedure for Rating Piston and Liner

    Annex A15

    Calculation of Percent Offset and Percent Deviation

    Annex A16

    1K/1N Test Reporting

    Annex A17

    Parts List by Part Number (P/N) and Warranty

    Annex A18

    Safety Precautions

    Annex A19

    APPENDIXES

    Humidity Data

    Appendix X1

    Statistical Equations for Mean and Standard Deviation

    Appendix X2

    Examples of Forms for Reporting

    Appendix X3

    Optional Recording of Oil Pass Limits

    Appendix X4

    1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements appear throughout the text. Being engine tests, these test methods do have definite hazards that shall be met by safe practices (see Annex A19 on Safety Precautions).

    1.6This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

    General Product Information - (Show below) - (Hide below)

    Committee D 02
    Document Type Test Method
    Product Note THIS STANDARD ALSO REFERS TO ASTM D 2709
    Publisher American Society for Testing and Materials
    Status Superseded
    Superseded By
    Supersedes

    Standards Referenced By This Book - (Show below) - (Hide below)

    ASTM D 7589 : 2016 Standard Test Method for Measurement of Effects of Automotive Engine Oils on Fuel Economy of Passenger Cars and Light-Duty Trucks in Sequence VID Spark Ignition Engine
    ASTM D 4485 : 2020 Standard Specification for Performance of Active API Service Category Engine Oils
    ASTM D 6837 : 2013 Standard Test Method for Measurement of Effects of Automotive Engine Oils on Fuel Economy of Passenger Cars and Light-Duty Trucks in Sequence VIB Spark Ignition Engine (Withdrawn 2022)
    ASTM D 6984 : 2018 Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIF, Spark-Ignition Engine
    ASTM D 7320 : 2018 Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine

    Standards Referencing This Book - (Show below) - (Hide below)

    ASTM D 5862 : 2009 Standard Test Method for Evaluation of Engine Oils in Two-Stroke Cycle Turbo-Supercharged 6V92TA Diesel Engine (Withdrawn 2009)
    ASTM D 2425 : 2019 Standard Test Method for Hydrocarbon Types in Middle Distillates by Mass Spectrometry
    ASTM D 4485 : 2003 : REV A Standard Specification for Performance of Engine Oils
    ASTM D 2622 : 1992 : EDT 1 Standard Test Method for Sulfur in Petroleum Products by X-Ray Spectrometry
    ASTM D 7422 : 2012 Standard Test Method for Evaluation of Diesel Engine Oils in T-12 Exhaust Gas Recirculation Diesel Engine
    ASTM D 5844 : 1998 Standard Test Method for Evaluation of Automotive Engine Oils for Inhibition of Rusting (Sequence IID) (Withdrawn 2003)
    ASTM D 4485 : 2006 Standard Specification for Performance of Engine Oils
    ASTM D 2622 : 1987 : EDT 1 Standard Test Method for Sulfur in Petroleum Products by X-Ray Spectrometry
    ASTM D 2709 : 1996 : R2011 : EDT 1 Standard Test Method for Water and Sediment in Middle Distillate Fuels by Centrifuge
    ASTM D 3524 : 2004 Standard Test Method for Diesel Fuel Diluent in Used Diesel Engine Oils by Gas Chromatography (Withdrawn 2013)
    ASTM D 2709 : 1996 : EDT 2 Standard Test Method for Water and Sediment in Middle Distillate Fuels by Centrifuge
    ASTM D 4485 : 2011 : REV C Standard Specification for Performance of Active API Service Category Engine Oils
    ASTM D 1319 : 1989 Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Absorption
    ASTM D 1319 : 2008 Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption
    ASTM D 1298 : 2012 : REV A Standard Test Method for Density, Relative Density (Specific Gravity), or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
    ASTM D 4485 : 2001 Standard Specification for Performance of Engine Oils
    ASTM D 1796 : 2011 Standard Test Method for Water and Sediment in Fuel Oils by the Centrifuge Method (Laboratory Procedure)
    ASTM D 7422 : 2009 Standard Test Method for Evaluation of Diesel Engine Oils in T-12 Exhaust Gas Recirculation Diesel Engine
    ASTM D 6202 : 2001 Standard Test Method for Automotive Engine Oils on the Fuel Economy of Passenger Cars and Light-Duty Trucks in the Sequence VIA Spark Ignition Engine
    ASTM D 5185 : 1997 Standard Test Method for Determination of Additive Elements, Wear Metals, and Contaminants in Used Lubricating Oils and Determination of Selected Elements in Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
    ASTM E 29 : 2013 : R2019 Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
    ASTM D 2425 : 2004 : R2009 Standard Test Method for Hydrocarbon Types in Middle Distillates by Mass Spectrometry
    ASTM D 4485 : 2003 Standard Specification for Performance of Engine Oils
    ASTM D 6202 : 2000 : REV A Standard Test Method for Automotive Engine Oils on the Fuel Economy of Passenger Cars and Light-Duty Trucks in the Sequence VIA Spark Ignition Engine
    ASTM D 4485 : 2008 Standard Specification for Performance of Engine Oils
    ASTM D 4739 : 2005 Standard Test Method for Base Number Determination by Potentiometric Titration
    ASTM D 2709 : 1996 : R2006 Standard Test Method for Water and Sediment in Middle Distillate Fuels by Centrifuge
    ASTM D 4485 : 2015 Standard Specification for Performance of Active API Service Category Engine Oils
    ASTM D 7422 : 2019 Standard Test Method for Evaluation of Diesel Engine Oils in T-12 Exhaust Gas Recirculation Diesel Engine
    ASTM D 1298 : 2012 : REV B Standard Test Method for Density, Relative Density, or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
    ASTM D 3117 : 1996 : EDT 1 Standard Test Method for Wax Appearance Point of Distillate Fuels
    ASTM D 1319 : 2018 Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption
    ASTM D 4485 : 2005 : REV A Standard Specification for Performance of Engine Oils
    ASTM D 7422 : 2016 : REV A Standard Test Method for Evaluation of Diesel Engine Oils in T-12 Exhaust Gas Recirculation Diesel Engine
    ASTM D 6594 : 2013 Standard Test Method for Evaluation of Corrosiveness of Diesel Engine Oil at 135  °C
    ASTM D 2500 : 2016 : REV B Standard Test Method for Cloud Point of Petroleum Products and Liquid Fuels
    ASTM D 1319 : 2014 Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption
    ASTM D 4485 : 2011 : REV A Standard Specification for Performance of Active API Service Category Engine Oils
    ASTM E 29 : 2002 Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
    ASTM D 2622 : 1998 Standard Test Method for Sulfur in Petroleum Products by Wavelength Dispersive X-ray Fluorescence Spectrometry
    ASTM D 2500 : 2016 : REV A Standard Test Method for Cloud Point of Petroleum Products and Liquid Fuels
    ASTM D 2500 : 2016 Standard Test Method for Cloud Point of Petroleum Products
    ASTM D 1319 : 1999 Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption
    ASTM D 7422 : 2015 Standard Test Method for Evaluation of Diesel Engine Oils in T-12 Exhaust Gas Recirculation Diesel Engine
    ASTM D 4485 : 2018 Standard Specification for Performance of Active API Service Category Engine Oils
    ASTM D 5185 : 2005 Standard Test Method for Determination of Additive Elements, Wear Metals, and Contaminants in Used Lubricating Oils and Determination of Selected Elements in Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
    ASTM D 4737 : 2009 Standard Test Method for Calculated Cetane Index by Four Variable Equation
    ASTM D 1298 : 1999 : R2005 Standard Test Method for Density, Relative Density (Specific Gravity), or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
    ASTM D 235 : 2022 Standard Specification for Mineral Spirits (Petroleum Spirits) (Hydrocarbon Dry Cleaning Solvent)
    ASTM D 5185 : 2002 Standard Test Method for Determination of Additive Elements, Wear Metals, and Contaminants in Used Lubricating Oils and Determination of Selected Elements in Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
    ASTM D 1298 : 2012 : REV B : R2017 Standard Test Method for Density, Relative Density, or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
    ASTM D 1298 : 2012 Standard Test Method for Density, Relative Density (Specific Gravity), or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
    ASTM D 4485 : 2011 : REV B Standard Specification for Performance of Active API Service Category Engine Oils
    ASTM D 2622 : 2008 Standard Test Method for Sulfur in Petroleum Products by Wavelength Dispersive X-ray Fluorescence Spectrometry
    ASTM D 4485 : 2016 Standard Specification for Performance of Active API Service Category Engine Oils
    ASTM D 4485 : 2007 Standard Specification for Performance of Engine Oils
    ASTM D 7422 : 2014 : REV A Standard Test Method for Evaluation of Diesel Engine Oils in T-12 Exhaust Gas Recirculation Diesel Engine
    ASTM D 4485 : 2010 Standard Specification for Performance of Engine Oils
    ASTM D 1298 : 1999 : EDT 2 Standard Test Method for Density, Relative Density (Specific Gravity), or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
    ASTM D 5185 : 2018 Standard Test Method for Multielement Determination of Used and Unused Lubricating Oils and Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
    ASTM D 4485 : 2001 : REV A Standard Specification for Performance of Engine Oils
    ASTM D 7422 : 2010 : REV A Standard Test Method for Evaluation of Diesel Engine Oils in T-12 Exhaust Gas Recirculation Diesel Engine
    ASTM D 5186 : 2019 Standard Test Method for Determination of the Aromatic Content and Polynuclear Aromatic Content of Diesel Fuels By Supercritical Fluid Chromatography
    ASTM D 7422 : 2008 Standard Test Method for Evaluation of Diesel Engine Oils in T-12 Exhaust Gas Recirculation Diesel Engine
    ASTM D 1796 : 2004 : R2009 Standard Test Method for Water and Sediment in Fuel Oils by the Centrifuge Method (Laboratory Procedure)
    ASTM D 1319 : 2002 : REV A Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption
    ASTM D 7422 : 2017 : REV A Standard Test Method for Evaluation of Diesel Engine Oils in T-12 Exhaust Gas Recirculation Diesel Engine
    ASTM D 2709 : 2016 Standard Test Method for Water and Sediment in Middle Distillate Fuels by Centrifuge
    ASTM D 2500 : 1999 Standard Test Method for Cloud Point of Petroleum Products
    ASTM D 2500 : 2002 : EDT 1 Standard Test Method for Cloud Point of Petroleum Products
    ASTM D 4739 : 2008 Standard Test Method for Base Number Determination by Potentiometric Hydrochloric Acid Titration
    ASTM D 2500 : 2005 Standard Test Method for Cloud Point of Petroleum Products
    ASTM D 5185 : 2013 : EDT 1 Standard Test Method for Multielement Determination of Used and Unused Lubricating Oils and Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
    ASTM D 93 : 1990 : EDT 1 Standard Test Methods for Flash Point by Pensky-Martens Closed Tester
    ASTM D 5186 : 1999 Standard Test Method for Determination of Aromatic Content and Polynuclear Aromatic Content of Diesel Fuels and Aviation Turbine Fuels by Supercritical Fluid Chromatography
    ASTM D 4485 : 2004 Standard Specification for Performance of Engine Oils
    ASTM D 445 : 1988 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and the Calculation of Dynamic Viscosity)
    ASTM D 1298 : 1999 Standard Test Method for Density, Relative Density (Specific Gravity), or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
    ASTM D 2500 : 2002 Standard Test Method for Cloud Point of Petroleum Products
    ASTM D 2500 : 2011 Standard Test Method for Cloud Point of Petroleum Products
    ASTM D 4739 : 2017 Standard Test Method for Base Number Determination by Potentiometric Hydrochloric Acid Titration
    ASTM D 2500 : 2009 Standard Test Method for Cloud Point of Petroleum Products
    ASTM D 6594 : 2020 Standard Test Method for Evaluation of Corrosiveness of Diesel Engine Oil at 135 °C
    ASTM D 3524 : 2014 Standard Test Method for Diesel Fuel Diluent in Used Diesel Engine Oils by Gas Chromatography
    ASTM D 4739 : 2006 Standard Test Method for Base Number Determination by Potentiometric Titration
    ASTM D 1796 : 1997 Standard Test Method for Water and Sediment in Fuel Oils by the Centrifuge Method (Laboratory Procedure)
    ASTM D 4485 : 2000 Standard Specification for Performance of Engine Oils
    ASTM D 4739 : 1996 Standard Test Method for Base Number Determination by Potentiometric Titration
    ASTM D 2500 : 2017 Standard Test Method for Cloud Point of Petroleum Products and Liquid Fuels
    ASTM D 5186 : 2003 : R2009 Standard Test Method for Determination of Aromatic Content and Polynuclear Aromatic Content of Diesel Fuels and Aviation Turbine Fuels by Supercritical Fluid Chromatography
    ASTM D 7422 : 2022 Standard Test Method for Evaluation of Diesel Engine Oils in T-12 Exhaust Gas Recirculation Diesel Engine
    ASTM D 1319 : 2003 Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption
    ASTM D 7422 : 2013 Standard Test Method for Evaluation of Diesel Engine Oils in T-12 Exhaust Gas Recirculation Diesel Engine
    ASTM D 4485 : 2015 : REV A Standard Specification for Performance of Active API Service Category Engine Oils
    ASTM D 6594 : 2019 : REV A Standard Test Method for Evaluation of Corrosiveness of Diesel Engine Oil at 135 °C
    ASTM D 5185 : 2013 Standard Test Method for Multielement Determination of Used and Unused Lubricating Oils and Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
    ASTM D 6594 : 2014 Standard Test Method for Evaluation of Corrosiveness of Diesel Engine Oil at 135°C
    ASTM D 1796 : 1997 : EDT 1 Standard Test Method for Water and Sediment in Fuel Oils by the Centrifuge Method (Laboratory Procedure)
    ASTM D 664 : 1995 Standard Test Method for Acid Number of Petroleum Products by Potentiometric Titration
    ASTM D 2622 : 2003 Standard Test Method for Sulfur in Petroleum Products by Wavelength Dispersive X-ray Fluorescence Spectrometry
    ASTM D 2425 : 1999 Standard Test Method for Hydrocarbon Types in Middle Distillates by Mass Spectrometry
    ASTM D 1319 : 2010 Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption
    ASTM D 4737 : 2009 : REV A Standard Test Method for Calculated Cetane Index by Four Variable Equation
    ASTM D 4737 : 2021 Standard Test Method for Calculated Cetane Index by Four Variable Equation
    ASTM D 5186 : 2015 Standard Test Method for Determination of the Aromatic Content and Polynuclear Aromatic Content of Diesel Fuels and Aviation Turbine Fuels By Supercritical Fluid Chromatography
    ASTM D 2425 : 2021 Standard Test Method for Hydrocarbon Types in Middle Distillates by Mass Spectrometry
    ASTM D 7422 : 2015 : REV A Standard Test Method for Evaluation of Diesel Engine Oils in T-12 Exhaust Gas Recirculation Diesel Engine
    ASTM D 1298 : 1999 : EDT 1 Standard Test Method for Density, Relative Density (Specific Gravity), or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
    ASTM D 4485 : 2006 : REV A Standard Specification for Performance of Engine Oils
    ASTM D 4739 : 2011 : R2017 Standard Test Method for Base Number Determination by Potentiometric Hydrochloric Acid Titration
    ASTM D 4737 : 2010 : R2016 Standard Test Method for Calculated Cetane Index by Four Variable Equation
    ASTM D 6594 : 2004 Standard Test Method for Evaluation of Corrosiveness of Diesel Engine Oil at 135°C
    ASTM D 2425 : 2004 Standard Test Method for Hydrocarbon Types in Middle Distillates by Mass Spectrometry
    ASTM D 445 : 2019 : REV A Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
    ASTM D 7422 : 2016 Standard Test Method for Evaluation of Diesel Engine Oils in T-12 Exhaust Gas Recirculation Diesel Engine
    ASTM D 2500 : 2017 : REV A Standard Test Method for Cloud Point of Petroleum Products and Liquid Fuels
    ASTM D 7422 : 2011 Standard Test Method for Evaluation of Diesel Engine Oils in T-12 Exhaust Gas Recirculation Diesel Engine
    ASTM D 7422 : 2010 Standard Test Method for Evaluation of Diesel Engine Oils in T-12 Exhaust Gas Recirculation Diesel Engine
    ASTM D 4737 : 2003 Standard Test Method for Calculated Cetane Index by Four Variable Equation
    ASTM D 3524 : 1990 : R1999 Standard Test Method for Diesel Fuel Diluent in Used Diesel Engine Oils by Gas Chromatography
    ASTM D 4739 : 2008 : EDT 1 Standard Test Method for Base Number Determination by Potentiometric Hydrochloric Acid Titration
    ASTM D 235 : 2002 : R2012 Standard Specification for Mineral Spirits (Petroleum Spirits) (Hydrocarbon Dry Cleaning Solvent) (Withdrawn 2021)
    ASTM D 6594 : 2004 : REV A Standard Test Method for Evaluation of Corrosiveness of Diesel Engine Oil at 135°C
    ASTM D 4485 : 2018 : REV A Standard Specification for Performance of Active API Service Category Engine Oils
    ASTM D 3117 : 2003 Standard Test Method for Wax Appearance Point of Distillate Fuels (Withdrawn 2010)
    ASTM D 2622 : 2010 Standard Test Method for Sulfur in Petroleum Products by Wavelength Dispersive X-ray Fluorescence Spectrometry
    ASTM D 6594 : 2006 Standard Test Method for Evaluation of Corrosiveness of Diesel Engine Oil at 135°C
    ASTM D 2709 : 1988 Standard Test Method for Water and Sediment in Distillate Fuels by Centrifuge
    ASTM D 4485 : 2005 Standard Specification for Performance of Engine Oils
    ASTM D 5185 : 2009 Standard Test Method for Determination of Additive Elements, Wear Metals, and Contaminants in Used Lubricating Oils and Determination of Selected Elements in Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
    ASTM D 93 : 2000 Standard Test Methods for Flash-Point by Pensky-Martens Closed Cup Tester
    ASTM D 445 : 2001 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (the Calculation of Dynamic Viscosity)
    ASTM D 4737 : 1996 : REV A Standard Test Method for Calculated Cetane Index by Four Variable Equation
    ASTM D 6202 : 2002 Standard Test Method for Automotive Engine Oils on the Fuel Economy of Passenger Cars and Light-Duty Trucks in the Sequence VIA Spark Ignition Engine (Withdrawn 2009)
    ASTM D 2622 : 2021 Standard Test Method for Sulfur in Petroleum Products by Wavelength Dispersive X-ray Fluorescence Spectrometry
    ASTM D 445 : 2021 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
    ASTM D 7422 : 2009 : REV A Standard Test Method for Evaluation of Diesel Engine Oils in T-12 Exhaust Gas Recirculation Diesel Engine
    ASTM D 5186 : 2003 Standard Test Method for Determination of Aromatic Content and Polynuclear Aromatic Content of Diesel Fuels and Aviation Turbine Fuels by Supercritical Fluid Chromatography
    ASTM D 5862 : 2006 Standard Test Method for Evaluation of Engine Oils in Two-Stroke Cycle Turbo-Supercharged 6V92TA Diesel Engine
    ASTM D 6594 : 2001 Standard Test Method for Evaluation of Corrosiveness of Diesel Engine Oil at 135oC
    ASTM D 4485 : 2014 Standard Specification for Performance of Active API Service Category Engine Oils
    ASTM D 93 : 1985 Standard Test Method for Flash Point by Pensky-Martens Closed Tester
    ASTM D 1796 : 2011 : R2016 Standard Test Method for Water and Sediment in Fuel Oils by the Centrifuge Method (Laboratory Procedure)
    ASTM D 4485 : 2002 Standard Specification for Performance of Engine Oils
    ASTM D 5186 : 2022 Standard Test Method for Determination of the Aromatic Content and Polynuclear Aromatic Content of Diesel Fuels By Supercritical Fluid Chromatography
    ASTM D 2622 : 2007 Standard Test Method for Sulfur in Petroleum Products by Wavelength Dispersive X-ray Fluorescence Spectrometry
    ASTM D 4485 : 2005 : EDT 1 Standard Specification for Performance of Engine Oils
    ASTM D 2622 : 1994 Standard Test Method for Sulfur in Petroleum Products by X-Ray Spectrometry
    ASTM D 5862 : 1999 : REV A Standard Test Method for Evaluation of Engine Oils in Two-Stroke Cycle Turbo-Supercharged 6V92TA Diesel Engine
    ASTM D 2622 : 2005 Standard Test Method for Sulfur in Petroleum Products by Wavelength Dispersive X-ray Fluorescence Spectrometry
    ASTM D 5185 : 2002 : EDT 1 Standard Test Method for Determination of Additive Elements, Wear Metals, and Contaminants in Used Lubricating Oils and Determination of Selected Elements in Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
    ASTM D 5862 : 2003 Standard Test Method for Evaluation of Engine Oils in Two-Stroke Cycle Turbo-Supercharged 6V92TA Diesel Engine
    ASTM D 6594 : 2003 Standard Test Method for Evaluation of Corrosiveness of Diesel Engine Oil at 135oC
    ASTM D 6594 : 2000 Standard Test Method for Evaluation of Corrosiveness of Diesel Engine Oil at 135oC
    ASTM D 4737 : 2004 Standard Test Method for Calculated Cetane Index by Four Variable Equation
    ASTM D 1298 : 1985 : R1990 : EDT 1 Standard Practice for Density, Relative Density (Specific Gravity), or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
    ASTM D 1319 : 2015 Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption
    ASTM D 7422 : 2017 Standard Test Method for Evaluation of Diesel Engine Oils in T-12 Exhaust Gas Recirculation Diesel Engine
    ASTM D 1796 : 1997 : R2002 Standard Test Method for Water and Sediment in Fuel Oils by the Centrifuge Method (Laboratory Procedure)
    ASTM D 5185 : 2002 : EDT 2 Standard Test Method for Determination of Additive Elements, Wear Metals, and Contaminants in Used Lubricating Oils and Determination of Selected Elements in Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
    ASTM D 4739 : 2011 Standard Test Method for Base Number Determination by Potentiometric Hydrochloric Acid Titration
    ASTM D 4739 : 2002 Standard Test Method for Base Number Determination by Potentiometric Titration
    ASTM D 1319 : 2013 Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption
    ASTM D 5186 : 1991 Standard Test Method for Determination of Aromatic Content of Diesel Fuels by Supercritical Fluid Chromatography
    ASTM D 1796 : 2004 Standard Test Method for Water and Sediment in Fuel Oils by the Centrifuge Method (Laboratory Procedure)
    ASTM D 445 : 2021 : EDT 1 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
    ASTM D 4739 : 2006 : REV A Standard Test Method for Base Number Determination by Potentiometric Titration
    ASTM D 1796 : 2011 : EDT 1 Standard Test Method for Water and Sediment in Fuel Oils by the Centrifuge Method (Laboratory Procedure)
    ASTM D 1796 : 1983 : R1990 : EDT 1 Standard Test Method for Water and Sediment in Fuel Oils by the Centrifuge Method (Laboratory Procedure)
    ASTM D 2425 : 2017 Standard Test Method for Hydrocarbon Types in Middle Distillates by Mass Spectrometry
    ASTM D 93 : 1997 Standard Test Methods for Flash-Point by Pensky-Martens Closed Cup Tester
    ASTM D 4485 : 2009 Standard Specification for Performance of Engine Oils
    ASTM D 4485 : 2019 Standard Specification for Performance of Active API Service Category Engine Oils
    ASTM D 6594 : 2005 Standard Test Method for Evaluation of Corrosiveness of Diesel Engine Oil at 135°C
    ASTM D 6594 : 2019 Standard Test Method for Evaluation of Corrosiveness of Diesel Engine Oil at 135 °C
    ASTM D 4485 : 2010 : REV A Standard Specification for Performance of Engine Oils
    ASTM D 4485 : 2011 Standard Specification for Performance of Engine Oils
    ASTM D 1319 : 2019 Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption
    ASTM D 5186 : 2020 Standard Test Method for Determination of the Aromatic Content and Polynuclear Aromatic Content of Diesel Fuels By Supercritical Fluid Chromatography
    ASTM D 4737 : 2010 Standard Test Method for Calculated Cetane Index by Four Variable Equation
    ASTM D 6594 : 2008 Standard Test Method for Evaluation of Corrosiveness of Diesel Engine Oil at 135°C
    ASTM D 1319 : 2002 Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption
    ASTM D 2622 : 2016 Standard Test Method for Sulfur in Petroleum Products by Wavelength Dispersive X-ray Fluorescence Spectrometry
    ASTM D 2709 : 1996 : R2001 : EDT 1 Standard Test Method for Water and Sediment in Middle Distillate Fuels by Centrifuge
    ASTM D 7422 : 2014 Standard Test Method for Evaluation of Diesel Engine Oils in T-12 Exhaust Gas Recirculation Diesel Engine
    ASTM D 4485 : 2007 : REV A Standard Specification for Performance of Engine Oils
    ASTM E 29 : 2022 Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
    View more information

    • Access your standards online with a subscription

      Features

      • Simple online access to standards, technical information and regulations
      • Critical updates of standards and customisable alerts and notifications
      • Multi - user online standards collection: secure, flexibile and cost effective