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ASTM D 6984 : 2018

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIF, Spark-Ignition Engine

Available format(s)

Hardcopy , PDF

Superseded date

28-06-2022

Language(s)

English

Published date

19-04-2018

€104.99
Excluding VAT

Committee
D 02
DocumentType
Test Method
Pages
54
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

1.1This test method covers an engine test procedure for evaluating automotive engine oils for certain high-temperature performance characteristics, including oil thickening, varnish deposition, oil consumption, as well as engine wear. Such oils include both single viscosity grade and multiviscosity grade oils that are used in both spark-ignition, gasoline-fueled engines, as well as in diesel engines.

Note 1:Companion test methods used to evaluate engine oil performance for specification requirements are discussed in SAE J304.

1.2The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.2.1Exceptions—The values stated in inches for ring gap measurements are to be regarded as standard, and where there is no direct SI equivalent such as screw threads, National Pipe Threads/diameters, tubing size, or single source supply equipment specifications.

1.3This test method is arranged as follows:

Subject

Section

Scope

1

Referenced Documents

2

Terminology

3

Summary of Test Method

4

Significance and Use

5

Apparatus

6

 Laboratory

6.1

 Drawings

6.2

 Specified Equipment

6.3

 Test Engine

6.4

  Engine Parts

6.4.1

 Engine Speed and Torque Control

6.5

 Sequence IIIF Fluid Conditioning Module

6.6

  Engine Cooling System

6.6.1

 Flushing Tank

6.7

 Coolant Mixing Tank

6.8

 Condenser Cooling Systems

6.9

 Engine Oil-Cooling System

6.10

 Fuel System

6.11

 Induction Air Supply Humidity, Temperature, and Pressure

6.12

 Temperature Measurement

6.13

  Thermocouple Location

6.13.1

 Air-to-Fuel Ratio Determination

6.14

  Injector Flow Testing

6.14.1

 Exhaust and Exhaust Back Pressure Systems

6.15

 Blowby Flow Rate Measurement

6.16

 Pressure Measurement and Pressure Sensor Location

6.17

Reagents and Materials

7

 Test Fuel

7.1

 Engine and Condenser Coolant

7.2

 Coolant Additive

7.3

 Coolant Preparation

7.4

 Pre-Test Cleaning Materials

7.5

 Sealing and Anti-seize Compounds

7.6

Test Oil Sample Requirements

8

Preparation of Apparatus

9

 Condenser Cleaning

9.1

 Intake Manifold Cleaning

9.3

 Cleaning of Engine Parts (other than the block and heads)

9.4

 Engine Block Cleaning

9.5

 Cylinder Head Cleaning

9.6

 Engine Build-up Procedure

9.7

  General Information

9.7.1

  Special Parts

9.7.2

  Hardware Information

9.7.3

  Fastener Torque Specifications and Torquing Procedures

9.7.4

 Parts Replacement

9.8

 Engine Block Preparation

9.9

 Piston Fitting and Numbering

9.10

  Piston Ring Fitting

9.10.1

 Pre-Test Camshaft and Lifter Measurements

9.11

 Camshaft Bearing Installation

9.12

 Camshaft Installation

9.13

 Main Bearings

9.14

  Crankshaft Installation

9.14.1

  Main Bearing Cap Installation

9.14.2

 Crankshaft Sprocket

9.15

 Camshaft Sprocket and Timing Chain

9.16

 Crankshaft End Play

9.17

 Piston Pin Installation

9.18

  Piston Installation

9.18.1

 Harmonic Balancer

9.19

 Connecting Rod Bearings

9.20

 Engine Front Cover

9.21

 Coolant Inlet Adapter

9.22

 Oil Dipstick Hole

9.23

 Oil Pan

9.24

 Cylinder Head Assembly

9.25

 Adjustment of Valve Spring Forces

9.26

 Cylinder Head Installation

9.27

 Hydraulic Valve Lifters

9.28

 Pushrods

9.29

 Valve Train Loading

9.30

 Intake Manifold

9.31

 Rocker Covers

9.32

 Water Inlet Adapter

9.33

 Condenser

9.34

 Coolant Outlet Adapter

9.35

 External Oil Cooling System

9.36

 Oil Sample Valve

9.37

 Ignition System

9.38

 Throttle Body

9.39

 Accessory Drive Units

9.40

 Exhaust Manifolds, Water-Cooled

9.41

 Engine Flywheel

9.42

 Pressure Checking of Engine Coolant System

9.43

 Lifting of Assembled Engines

9.44

 Mounting the Engine on the Test Stand

9.45

 External Cooling System Cleaning

9.46

 Engine Coolant Jacket Cleaning (Flushing)

9.47

 Coolant Charging

9.48

 Test Oil Charging

9.49

 Engine Oil Pump Priming

9.50

Calibration

10

 Laboratory and Engine Test Stand Calibration

10.1

 Testing of Reference Oils

10.2

 Reference Oil Test Frequency

10.3

 Evaluation of Reference Oil Test Results

10.4

 Status of Non-Reference Oil Tests Relative to Reference
  Oil Test

10.5

 Status of Test Stands Used for Non-Standard Tests

10.6

 Data Acquisition and Control

10.7

  Sample Rate

10.7.1

  Measurement Accuracy

10.7.2

  Temperature

10.7.3

  Pressure

10.7.4

  Flow

10.7.5

  Speed

10.7.6

  Mass

10.7.7

  Measurement Resolution

10.7.8

  System Time Response

10.7.9

  Quality Index

10.7.10

Engine Operating Procedure

11

 Dipstick and Hole Plug

11.1

 Dipstick Hole O-ring

11.2

 Engine Start-up and Shutdown Procedures

11.3

 Start-up

11.4

 Scheduled Shutdown

11.5

 Non-Scheduled Shutdowns

11.6

 Oil Sampling

11.7

 Oil Leveling

11.8

 Air-to-Fuel-Ratio Measurement and Control

11.9

 Air-to-Fuel Ratio Verification

11.10

 Blowby Flow Rate Measurement

11.11

 NOx Determinations

11.12

 Data Recording

11.13

 Initial Run (10 min)

11.14

 Engine Oil Quality Testing (80 h)

11.15

 Test Termination

11.16

Determination of Test Results

12

 Engine Disassembly

12.2

 Preparation of Parts for Rating of Sticking, Deposits,
  and Plugging

12.3

 Piston Deposit Ratings

12.4

 Post-Test Camshaft and Lifter Wear Measurements

12.5

 End-of Test Used Oil Sample Testing

12.6

 Viscosity Test

12.7

 Testing Oil Samples for Wear Metals

12.8

 Blowby Flow Rate Measurements

12.9

 Oil Consumption Computation

12.10

 Photographs of Test Parts

12.11

 Retention of Representative Test Parts

12.12

 Severity Adjustments

12.13

 Determination of Operational Validity

12.14

Report

13

 Report Forms

13.1

 Precision of Reported Units

13.4

 Deviations from Test Operational Limits

13.3

Precision and Bias

14

Keywords

15

Annexes

ASTM Test Monitoring Center – Organization

Annex A1

ASTM Test Monitoring Center – Calibration Procedures

Annex A2

ASTM Test Monitoring Center – Maintenance Activities

Annex A3

ASTM Test Monitoring Center – Related Information

Annex A4

Sequence IIIF Test Parts Replacement Guidelines

Annex A5

Sequence IIIF Determination Volume of Engine Oil in Pan

Annex A6

Sequence IIIF Test Fuel Analysis

Annex A7

Sequence IIIF Test Report Forms and Data Dictionary

Annex A8

Sequence IIIF Test Air-to-Fuel Ratio Control Flow Chart

Annex A9

Sequence IIIF Test Set Points and Control States

Annex A10

Sequence IIIF Quality Index Upper and Lower Values

Annex A11

Sequence IIIF Engine Oil Level Worksheet

Annex A12

Engine Build Worksheets

Annex A13

Blowby Flow Rate Determination

Annex A14

Safety Precautions

Annex A15

Sequence IIIF Blueprint Listing

Annex A16

Fluid Conditioning Module Components

Annex A17

Engine Oil Cooling System Configuration

Annex A18

Guidelines For Hardware Subject To First-In/First-Out Criteria

Annex A19

Appendixes

Sequence IIIFHD Test Procedure

Appendix X1

Sequence IIIFVIS Test Procedure

Appendix X2

1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.5This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D 2699 : 1992 Standard Test Method for Knock Characteristics of Motor Fuels by the Research Method
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ASTM D 6750 : 2019 Standard Test Methods for Evaluation of Engine Oils in a High-Speed, Single-Cylinder Diesel Engine—1K Procedure (0.4 % Fuel Sulfur) and 1N Procedure (0.04 % Fuel Sulfur)
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ASTM D 4815 : 2022 Standard Test Method for Determination of MTBE, ETBE, TAME, DIPE, tertiary-Amyl Alcohol and C<inf>1</inf> to C<inf>4</inf> Alcohols in Gasoline by Gas Chromatography
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ASTM D 6750 : 2018 Standard Test Methods for Evaluation of Engine Oils in a High-Speed, Single-Cylinder Diesel Engine—1K Procedure (0.4 % Fuel Sulfur) and 1N Procedure (0.04 % Fuel Sulfur)
ASTM E 1119 : 1997 Standard Specification for Industrial Grade Ethylene Glycol
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ASTM D 7422 : 2010 : REV A Standard Test Method for Evaluation of Diesel Engine Oils in T-12 Exhaust Gas Recirculation Diesel Engine
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ASTM D 4175 : 2001 : EDT 1 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
ASTM D 4175 : 2020 : REV B : EDT 1 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
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ASTM D 7422 : 2017 : REV A Standard Test Method for Evaluation of Diesel Engine Oils in T-12 Exhaust Gas Recirculation Diesel Engine
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ASTM D 3343 : 2005 : R2015 Standard Test Method for Estimation of Hydrogen Content of Aviation Fuels
ASTM D 7422 : 2022 Standard Test Method for Evaluation of Diesel Engine Oils in T-12 Exhaust Gas Recirculation Diesel Engine
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ASTM D 3343 : 1990 Standard Test Method for Estimation of Hydrogen Content of Aviation Fuels
ASTM D 2699 : 2019 : EDT 1 Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
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ASTM D 5453 : 2016 Standard Test Method for Determination of Total Sulfur in Light Hydrocarbons, Spark Ignition Engine Fuel, Diesel Engine Fuel, and Engine Oil by Ultraviolet Fluorescence
ASTM D 5191 : 1999 Standard Test Method for Vapor Pressure of Petroleum Products (Mini Method)
ASTM D 7422 : 2015 : REV A Standard Test Method for Evaluation of Diesel Engine Oils in T-12 Exhaust Gas Recirculation Diesel Engine
ASTM D 7320 : 2006 Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
ASTM D 7320 : 2017 Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
ASTM G 40 : 2021 : REV A Standard Terminology Relating to Wear and Erosion
ASTM D 7320 : 2008 Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
ASTM D 445 : 2019 : REV A Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM E 608/E608M : 2013 : R2019 Standard Specification for Mineral-Insulated, Metal-Sheathed Base Metal Thermocouples
ASTM D 7422 : 2016 Standard Test Method for Evaluation of Diesel Engine Oils in T-12 Exhaust Gas Recirculation Diesel Engine
ASTM D 2700 : 2021 Standard Test Method for Motor Octane Number of Spark-Ignition Engine Fuel
ASTM D 4815 : 1999 Standard Test Method for Determination of MTBE, ETBE, TAME, DIPE, <I>tertiary</I>-Amyl Alcohol and C<sub>1</sub> to C<sub>4</sub> Alcohols in Gasoline by Gas Chromatography
ASTM D 2700 : 2019 : EDT 1 Standard Test Method for Motor Octane Number of Spark-Ignition Engine Fuel
ASTM D 4052 : 1996 Standard Test Method for Density and Relative Density of Liquids by Digital Density Meter
ASTM D 2699 : 2015 Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
ASTM D 235 : 2002 : R2012 Standard Specification for Mineral Spirits (Petroleum Spirits) (Hydrocarbon Dry Cleaning Solvent) (Withdrawn 2021)
ASTM D 4485 : 2018 : REV A Standard Specification for Performance of Active API Service Category Engine Oils
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ASTM D 445 : 2001 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (the Calculation of Dynamic Viscosity)
ASTM D 6593 : 2016 : REV A Standard Test Method for Evaluation of Automotive Engine Oils for Inhibition of Deposit Formation in a Spark-Ignition Internal Combustion Engine Fueled with Gasoline and Operated Under Low-Temperature, Light-Duty Conditions
ASTM D 2699 : 2021 Standard Test Method for Research Octane Number of Spark-Ignition Engine Fuel
ASTM D 445 : 2021 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM D 5293 : 2017 : EDT 1 Standard Test Method for Apparent Viscosity of Engine Oils and Base Stocks Between –10 °C and –35 °C Using Cold-Cranking Simulator
ASTM D 4485 : 2014 Standard Specification for Performance of Active API Service Category Engine Oils
ASTM D 5453 : 2019 : REV A Standard Test Method for Determination of Total Sulfur in Light Hydrocarbons, Spark Ignition Engine Fuel, Diesel Engine Fuel, and Engine Oil by Ultraviolet Fluorescence
ASTM D 6557 : 2018 Standard Test Method for Evaluation of Rust Preventive Characteristics of Automotive Engine Oils
ASTM D 6750 : 2015 Standard Test Methods for Evaluation of Engine Oils in a High-Speed, Single-Cylinder Diesel Engine—1K Procedure (0.4 % Fuel Sulfur) and 1N Procedure (0.04 % Fuel Sulfur)
ASTM D 5862 : 1999 : REV A Standard Test Method for Evaluation of Engine Oils in Two-Stroke Cycle Turbo-Supercharged 6V92TA Diesel Engine
ASTM D 7320 : 2017 : REV A Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
ASTM D 6593 : 2016 Standard Test Method for Evaluation of Automotive Engine Oils for Inhibition of Deposit Formation in a Spark-Ignition Internal Combustion Engine Fueled with Gasoline and Operated Under Low-Temperature, Light-Duty Conditions
ASTM D 4052 : 2022 Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter
ASTM E 1119 : 2009 : R2015 : EDT 1 Standard Specification for Industrial Grade Ethylene Glycol
ASTM D 7422 : 2017 Standard Test Method for Evaluation of Diesel Engine Oils in T-12 Exhaust Gas Recirculation Diesel Engine
ASTM D 3237 : 1997 Standard Test Method for Lead In Gasoline By Atomic Absorption Spectroscopy
ASTM D 3231 : 1989 Standard Test Method for Phosphorus in Gasoline
ASTM D 445 : 2021 : EDT 1 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM G 40 : 2017 Standard Terminology Relating to Wear and Erosion
ASTM D 7320 : 2016 : REV A Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
ASTM D 6750 : 2002 Standard Test Methods for Evaluation of Engine Oils in A High-Speed, Single-Cylinder Diesel Engine -1K Procedure (0.4 % Fuel Sulfur) and 1N Procedure (0.04 % Fuel Sulfur)
ASTM D 5293 : 2017 Standard Test Method for Apparent Viscosity of Engine Oils and Base Stocks Between –10 °C and –35 °C Using Cold-Cranking Simulator
ASTM E 1119 : 2009 : R2015 Standard Specification for Industrial Grade Ethylene Glycol
ASTM D 1319 : 2002 Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption
ASTM E 29 : 2022 Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications

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