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  • ASTM D 7591 : 2012 : R2017

    Current The latest, up-to-date edition.

    Standard Test Method for Determination of Free and Total Glycerin in Biodiesel Blends by Anion Exchange Chromatography

    Available format(s):  Hardcopy, PDF

    Language(s):  English

    Published date:  01-05-2017

    Publisher:  American Society for Testing and Materials

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    Abstract - (Show below) - (Hide below)

    CONTAINED IN VOL. 05.04, 2017 Defines an anion exchange chromatography procedure for determining free and total glycerin content of biodiesel (B100) and blends (B0 to B20) with diesel fuel oils defined by Specification D 975 Grades 1-D, 2-D, and low sulfur 1-D and 2-D and Specification D 6751 (for B100 feedstocks).

    Scope - (Show below) - (Hide below)

    1.1This test method covers and describes an anion exchange chromatography procedure for determining free and total glycerin content of biodiesel (B100) and blends (B0 to B20) with diesel fuel oils defined by Specification D975 Grades 1-D, 2-D, and low sulfur 1-D and 2-D and Specification D6751 (for B100 feedstocks). It is intended for the analysis of biodiesel and blend samples containing between 0.5 mg/kg to 50 mg/kg glycerin.

    1.2The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

    1.3This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

    1.4This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

    General Product Information - (Show below) - (Hide below)

    Committee D 02
    Document Type Test Method
    Product Note Reconfirmed 2017
    Publisher American Society for Testing and Materials
    Status Current

    Standards Referenced By This Book - (Show below) - (Hide below)

    ASTM D 8149 : 2017 Standard Practice for Optimization, Calibration, and Validation of Ion Chromatographic Determination of Heteroatoms and Anions in Petroleum Products and Lubricants

    Standards Referencing This Book - (Show below) - (Hide below)

    ASTM D 4057 : 2019 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 6792 : 2021 : REV A Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
    ASTM D 4057 : 1995 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 6299 : 2010 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6299 : 2013 : EDT 1 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM E 177 : 1990 : REV A : R1996 Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods
    ASTM D 4177 : 2016 : EDT 1 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM E 177 : 2014 : REDLINE Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods
    ASTM D 6299 : 2017 : REV A Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6299 : 2017 : REV B Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6299 : 2009 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 975 : 2022 Standard Specification for Diesel Fuel
    ASTM D 4177 : 1995 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 6751 : 2006 : REV A Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 4057 : 2012 : R2018 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 6751 : 2007 : REV B Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 6751 : 2006 : EDT 1 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 6299 : 2013 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6792 : 2006 Standard Guide for Quality System in Petroleum Products and Lubricants Testing Laboratories
    ASTM D 6299 : 2021 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6792 : 2017 : REDLINE Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
    ASTM D 6751 : 2018 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 6751 : 2009 : REV A Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 6792 : 2004 Standard Guide for Quality System in Petroleum Products and Lubricants Testing Laboratories
    ASTM D 6751 : 2007 : REV B : EDT 1 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 975 : 2019 : REV B Standard Specification for Diesel Fuel
    ASTM D 1193 : 1977 : R1983 : EDT 1 Standard Specification for Reagent Water
    ASTM D 6299 : 2010 : EDT 1 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6299 : 2022 : EDT 1 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6751 : 2007 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 4057 : 1981 : EDT 2 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 6751 : 2012 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 975 : 2021 Standard Specification for Diesel Fuel
    ASTM D 975 : 2023 : REV A Standard Specification for Diesel Fuel
    ASTM D 6792 : 2021 : REV B Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
    ASTM D 6792 : 2023 : REV C Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
    ASTM E 691 : 2020 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
    ASTM D 6299 : 2023 : REV A Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6751 : 2014 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 6792 : 2004 : REV A Standard Guide for Quality System in Petroleum Products and Lubricants Testing Laboratories
    ASTM D 6792 : 2005 Standard Guide for Quality System in Petroleum Products and Lubricants Testing Laboratories
    ASTM D 6299 : 2000 Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6299 : 2010 : EDT 2 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6751 : 2011 : REV B Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 975 : 2020 : REV C Standard Specification for Diesel Fuel
    ASTM D 6299 : 2016 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM E 691 : 2019 : EDT 1 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
    ASTM D 6792 : 2023 : REV B Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
    ASTM D 6751 : 2015 : REV B Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 4057 : 2006 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM E 691 : 2023 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
    ASTM D 1193 : 2006 : R2011 Standard Specification for Reagent Water
    ASTM D 4177 : 2015 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 6792 : 2020 Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
    ASTM D 6751 : 2015 : REV C Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 6299 : 2019 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6792 : 2021 Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
    ASTM D 6751 : 2015 : REV A Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 4057 : 2012 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 6299 : 2023 : EDT 1 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6299 : 2000 : REV A Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6792 : 2013 Standard Practice for Quality System in Petroleum Products and Lubricants Testing Laboratories
    ASTM D 6792 : 2017 Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
    ASTM E 691 : 2022 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
    ASTM D 6751 : 2002 Standard Specification for Biodiesel Fuel (B100) Blend Stock for Distillate Fuels
    ASTM D 6751 : 2003 : REV A Standard Specification for Biodiesel Fuel (B100) Blend Stock for Distillate Fuels
    ASTM D 6792 : 2007 Standard Practice for Quality System in Petroleum Products and Lubricants Testing Laboratories
    ASTM E 691 : 2009 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
    ASTM D 4177 : 2022 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 1193 : 1991 Standard Specification for Reagent Water
    ASTM D 6751 : 2023 : REV A Standard Specification for Biodiesel Fuel Blendstock (B100) for Middle Distillate Fuels
    ASTM D 6792 : 2021 : REV C Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
    ASTM D 6751 : 2020 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 6299 : 2023 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6299 : 2020 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6751 : 2020 : REV A Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 4177 : 1995 : R2010 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 6299 : 2008 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6751 : 2003 Standard Specification for Biodiesel Fuel (B100) Blend Stock for Distillate Fuels
    ASTM D 6751 : 2008 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 6751 : 2019 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 6792 : 2023 : REV A Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
    ASTM D 4177 : 1995 : R2000 Standard Practice for Automatic Sampling of Peroleum and Petroleum Products
    ASTM D 6299 : 2002 : EDT 1 Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance
    ASTM E 691 : 2021 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
    ASTM D 6751 : 2015 : REV C : EDT 1 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 975 : 2022 : REV A Standard Specification for Diesel Fuel
    ASTM D 6751 : 2023 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 6299 : 2022 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6751 : 2007 : REV A Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 6792 : 2022 Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
    ASTM D 4057 : 2022 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 975 : 2023 Standard Specification for Diesel Fuel
    ASTM D 6751 : 2011 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 4177 : 2016 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 1193 : 1970 Standard Specification For Reagent Water
    ASTM D 6792 : 2003 Standard Guide for Quality System in Petroleum Products and Lubricants Testing Laboratories
    ASTM D 4177 : 2020 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 4177 : 1995 : R2005 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 1193 : 2006 Standard Specification for Reagent Water
    ASTM D 6751 : 2011 : REV A Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 6751 : 2015 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 1193 : 1999 Standard Specification for Reagent Water
    ASTM D 6792 : 2002 Standard Guide for A Quality System in Petroleum Products and Lubricants Testing Laboratories
    ASTM D 6299 : 2007 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6792 : 2023 Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
    ASTM D 6299 : 2007 : EDT 1 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 4057 : 1995 : R2000 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 6299 : 2020 : REV A Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 4177 : 2022 : EDT 1 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 6299 : 2017 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
    ASTM D 6751 : 2009 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 1193 : 2006 : R2018 Standard Specification for Reagent Water
    ASTM D 4177 : 2015 : REV A Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 6792 : 2022 : REV A Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
    ASTM D 4057 : 2006 : R2011 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 6751 : 2010 Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
    ASTM D 6751 : 2002 : REV A Standard Specification for Biodiesel Fuel (B100) Blend Stock for Distillate Fuels
    ASTM D 6299 : 2002 Standard Practice for Applying Statistical Quality Assurance Techniques to Evaluate Analytical Measurement System Performance
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