ASTM E 112 : 2013 : R2021
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
View Superseded by
Standard Test Methods for Determining Average Grain Size
Hardcopy , PDF
04-07-2024
English
01-09-2021
Committee |
E 04
|
DocumentType |
Test Method
|
Pages |
28
|
PublisherName |
American Society for Testing and Materials
|
Status |
Superseded
|
SupersededBy | |
Supersedes |
1.1These test methods cover the measurement of average grain size and include the comparison procedure, the planimetric (or Jeffries) procedure, and the intercept procedures. These test methods may also be applied to nonmetallic materials with structures having appearances similar to those of the metallic structures shown in the comparison charts. These test methods apply chiefly to single phase grain structures but they can be applied to determine the average size of a particular type of grain structure in a multiphase or multiconstituent specimen.
1.2These test methods are used to determine the average grain size of specimens with a unimodal distribution of grain areas, diameters, or intercept lengths. These distributions are approximately log normal. These test methods do not cover methods to characterize the nature of these distributions. Characterization of grain size in specimens with duplex grain size distributions is described in Test Methods E1181. Measurement of individual, very coarse grains in a fine grained matrix is described in Test Methods E930.
1.3These test methods deal only with determination of planar grain size, that is, characterization of the two-dimensional grain sections revealed by the sectioning plane. Determination of spatial grain size, that is, measurement of the size of the three-dimensional grains in the specimen volume, is beyond the scope of these test methods.
1.4These test methods describe techniques performed manually using either a standard series of graded chart images for the comparison method or simple templates for the manual counting methods. Utilization of semi-automatic digitizing tablets or automatic image analyzers to measure grain size is described in Test Methods E1382.
1.5These test methods deal only with the recommended test methods and nothing in them should be construed as defining or establishing limits of acceptability or fitness of purpose of the materials tested.
1.6The measured values are stated in SI units, which are regarded as standard. Equivalent inch-pound values, when listed, are in parentheses and may be approximate.
1.7This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.8The paragraphs appear in the following order:
Section | Number |
Scope | 1 |
Referenced Documents | 2 |
Terminology | 3 |
Significance and Use | 4 |
Generalities of Application | 5 |
Sampling | 6 |
Test Specimens | 7 |
Calibration | 8 |
Preparation of Photomicrographs | 9 |
Comparison Procedure | 10 |
Planimetric (Jeffries) Procedure | 11 |
General Intercept Procedures | 12 |
Heyn Linear Intercept Procedure | 13 |
Circular Intercept Procedures | 14 |
Hilliard Single-Circle Procedure | 14.2 |
Abrams Three-Circle Procedure | 14.3 |
Statistical Analysis | 15 |
Specimens with Non-equiaxed Grain Shapes | 16 |
Specimens Containing Two or More Phases or Constituents | 17 |
Report | 18 |
Precision and Bias | 19 |
Keywords | 20 |
Annexes: | |
Basis of ASTM Grain Size Numbers | Annex A1 |
Equations for Conversions Among Various Grain Size Measurements | Annex A2 |
Austenite Grain Size, Ferritic and Austenitic Steels | Annex A3 |
Fracture Grain Size Method | Annex A4 |
Requirements for Wrought Copper and Copper-Base Alloys | Annex A5 |
Application to Special Situations | Annex A6 |
Appendixes: | |
Results of Interlaboratory Grain Size Determinations | Appendix X1 |
Referenced Adjuncts | Appendix X2 |
1.9This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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ASTM A 510/A510M : 2020 | Standard Specification for General Requirements for Wire Rods and Coarse Round Wire, Carbon Steel, and Alloy Steel |
ASTM A 765/A765M : 2007 : R2017 | Standard Specification for Carbon Steel and Low-Alloy Steel Pressure-Vessel-Component Forgings with Mandatory Toughness Requirements |
ASTM F 912 : 2011 : R2017 | Standard Specification for Alloy Steel Socket Set Screws |
ASTM A 788/A788M : 2019 : REV A | Standard Specification for Steel Forgings, General Requirements |
ASTM A 988/A988M : 2017 | Standard Specification for Hot Isostatically-Pressed Stainless Steel Flanges, Fittings, Valves, and Parts for High Temperature Service |
ASTM B 811 : 2013 : R2017 | Standard Specification for Wrought Zirconium Alloy Seamless Tubes for Nuclear Reactor Fuel Cladding |
ASTM F 1586 : 2021 | Standard Specification for Wrought Nitrogen Strengthened 21Chromium—10Nickel—3Manganese—2.5Molybdenum Stainless Steel Alloy Bar for Surgical Implants (UNS S31675) |
ASTM B 865 : 2020 | Standard Specification for Precipitation Hardening Nickel-Copper-Aluminum Alloy<brk/> Bar, Rod, Wire, Forgings, and Forging Stock |
ASTM B 587 : 2019 | Standard Specification for Welded Brass Tube |
ASTM F 1376 : 1992 : R2020 | Standard Guide for Metallurgical Analysis for Gas Distribution System Components (Withdrawn 2023) |
ASTM B 163 : 2019 | Standard Specification for Seamless Nickel and Nickel Alloy Condenser and Heat-Exchanger Tubes |
ASTM A 194/A194M : 2020 : REV A | Standard Specification for Carbon Steel, Alloy Steel, and Stainless Steel Nuts for Bolts for High Pressure or High Temperature Service, or Both |
ASTM B 152/B152M : 2019 | Standard Specification for Copper Sheet, Strip, Plate, and Rolled Bar |
ASTM B 101 : 2012 : R2019 | Standard Specification for Lead-Coated Copper Sheet and Strip for Building Construction |
ASTM E 1181 : 2002 : R2015 | Standard Test Methods for Characterizing Duplex Grain Sizes |
ASTM B 829 : 2019 : REV A | Standard Specification for General Requirements for Nickel and Nickel Alloys Seamless Pipe and Tube |
ASTM B 248 : 2017 | Standard Specification for General Requirements for Wrought Copper and Copper-Alloy Plate, Sheet, Strip, and Rolled Bar |
ASTM A 623M : 2016 | Standard Specification for Tin Mill Products, General Requirements [Metric] |
ASTM B 251/B251M : 2017 | Standard Specification for General Requirements for Wrought Seamless Copper and Copper-Alloy Tube |
ASTM F 2229 : 2021 | Standard Specification for Wrought, Nitrogen Strengthened 23Manganese-21Chromium-1Molybdenum Low-Nickel Stainless Steel Alloy Bar and Wire for Surgical Implants (UNS S29108) |
ASTM B 694 : 2019 | Standard Specification for Copper, Copper-Alloy, Copper-Clad Bronze (CCB), Copper-Clad Stainless Steel (CCS), and Copper-Clad Alloy Steel (CAS) Sheet and Strip for Electrical Cable Shielding |
ASTM B 592 : 2020 | Standard Specification for Copper-Zinc-Aluminum-Cobalt Alloy, Copper-Zinc-Tin-Iron Alloy Plate, Sheet, Strip, and Rolled Bar |
ASTM B 447 : 2012 : REV A : R2021 | Standard Specification for Welded Copper Tube |
ASTM F 562 : 2013 | Standard Specification for Wrought 35Cobalt-35Nickel-20Chromium-10Molybdenum Alloy for Surgical Implant Applications (UNS R30035) |
ASTM B 884 : 2011 : R2019 | Standard Specification for Niobium-Titanium Alloy Billets, Bar, and Rod for Superconducting Applications |
ASTM C 776 : 2017 | Standard Specification for Sintered Uranium Dioxide Pellets for Light Water Reactors |
ASTM C 1421 : 2018 | Standard Test Methods for Determination of Fracture Toughness of Advanced Ceramics at Ambient Temperature |
ASTM E 2821 : 2020 | Standard Specification for Compacted Mineral-Insulated, Metal-Sheathed Cable Used in Industrial Resistance Thermometers |
ASTM A 891/A891M : 2016 : R2021 | Standard Specification for Precipitation Hardening Iron Base Superalloy Forgings for Turbine Rotor Disks and Wheels |
ASTM E 585/E585M : 2018 | Standard Specification for Compacted Mineral-Insulated, Metal-Sheathed, Base Metal Thermocouple Cable |
ASTM B 543/B543M : 2018 | Standard Specification for Welded Copper and Copper-Alloy Heat Exchanger Tube |
ASTM A 592/A592M : 2010 : R2020 | Standard Specification for High-Strength Quenched and Tempered Low-Alloy Steel Forged Parts for Pressure Vessels |
ASTM B 101 : 2022 | Standard Specification for Lead-Coated Copper Sheet and Strip for Building Construction |
ASTM B 811 : 2013 : R2022 : EDT 1 | Standard Specification for Wrought Zirconium Alloy Seamless Tubes for Nuclear Reactor Fuel Cladding |
ASTM F 2066 : 2023 | Standard Specification for Wrought Titanium-15 Molybdenum Alloy for Surgical Implant Applications (UNS R58150) |
ASTM A 1033 : 2018 : R2023 | Standard Practice for Quantitative Measurement and Reporting of Hypoeutectoid Carbon and Low-Alloy Steel Phase Transformations |
ASTM A 941 : 2024 | Standard Terminology Relating to Steel, Stainless Steel, Related Alloys, and Ferroalloys |
ASTM B 280 : 2023 | Standard Specification for Seamless Copper Tube for Air Conditioning and Refrigeration Field Service |
ASTM B 511/B511M : 2021 | Standard Specification for Nickel-Iron-Chromium-Silicon Alloy Bars and Shapes |
ASTM A 182/A182M : 2024 : REV A | Standard Specification for Forged or Rolled Alloy and Stainless Steel Pipe Flanges, Forged Fittings, and Valves and Parts for High-Temperature Service |
ASTM A 965/A965M : 2024 | Standard Specification for Steel Forgings, Austenitic, for Pressure and High Temperature Parts |
ASTM B 370 : 2022 | Standard Specification for Copper Sheet and Strip for Building Construction |
ASTM B 249/B249M : 2023 | Standard Specification for General Requirements for Wrought Copper and Copper-Alloy Rod, Bar, Shapes and Forgings |
ASTM B 129 : 2022 | Standard Specification for Cartridge Brass Cartridge Case Cups |
ASTM B 131 : 2022 | Standard Specification for Copper Alloy Bullet Jacket Cups |
ASTM F 15 : 2004 : R2022 | Standard Specification for Iron-Nickel-Cobalt Sealing Alloy (Withdrawn 2024) |
ASTM A 555/A555M : 2023 | Standard Specification for General Requirements for Stainless Steel Wire and Wire Rods |
ASTM A 29/A29M : 2023 | Standard Specification for General Requirements for Steel Bars, Carbon and Alloy, Hot-Wrought |
ASTM A 574 : 2021 | Standard Specification for Alloy Steel Socket-Head Cap Screws |
ASTM B 743 : 2023 | Standard Specification for Seamless Copper Tube in Coils |
ASTM F 31 : 2021 | Standard Specification for Nickel-Chromium-Iron Sealing Alloys (Withdrawn 2024) |
ASTM A 213/A213M : 2024 | Standard Specification for Seamless Ferritic and Austenitic Alloy-Steel Boiler, Superheater, and Heat-Exchanger Tubes |
ASTM A 193/A193M : 2024 | Standard Specification for Alloy-Steel and Stainless Steel Bolting for High Temperature or High Pressure Service and Other Special Purpose Applications |
ASTM A 988/A988M : 2023 | Standard Specification for Hot Isostatically-Pressed Stainless Steel Flanges, Fittings, Valves, and Parts for High Temperature Service |
ASTM A 688/A688M : 2024 | Standard Specification for Seamless and Welded Austenitic Stainless Steel Feedwater Heater Tubes |
ASTM F 1314 : 2024 | Standard Specification for Wrought Nitrogen Strengthened 22Chromium-13Nickel-5Manganese-2.5Molybdenum Stainless Steel Alloy Bar and Wire for Surgical Implants (UNS S20910) |
ASTM E 839 : 2023 | Standard Test Methods for Sheathed Thermocouples and Sheathed Thermocouple Cable |
ASTM B 36/B36M : 2023 | Standard Specification for Brass Plate, Sheet, Strip, And Rolled Bar |
ASTM F 2282 : 2023 | Standard Specification for Quality Assurance Requirements for Carbon and Alloy Steel Wire, Rods, and Bars for Mechanical Fasteners |
ASTM B 476 : 2021 | Standard Specification for General Requirements for Wrought Precious Metal Electrical Contact Materials |
ASTM A 194/A194M : 2024 | Standard Specification for Carbon Steel, Alloy Steel, and Stainless Steel Nuts for Bolts for High Pressure or High Temperature Service, or Both |
ASTM A 484/A484M : 2024 | Standard Specification for General Requirements for Stainless Steel Bars, Billets, Shapes, and Forgings |
ASTM B 564 : 2022 | Standard Specification for Nickel Alloy Forgings |
ASTM A 1090/A1090M : 2019 : R2024 | Standard Specification for Forged Rings and Hollows for Use as Base Plates in Power Transmission Structures |
ASTM A 788/A788M : 2023 | Standard Specification for Steel Forgings, General Requirements |
ASTM A 623M : 2022 | Standard Specification for Tin Mill Products, General Requirements [Metric] |
ASTM B 167 : 2023 | Standard Specification for Nickel-Chromium-Aluminum Alloys, Nickel-Chromium-Iron Alloys, Nickel-Chromium-Cobalt-Molybdenum Alloy, Nickel-Iron-Chromium-Tungsten Alloy, and Nickel-Chromium-Molybdenum-Copper Alloy Seamless Pipe and Tube |
ASTM A 240/A240M : 2024 | Standard Specification for Chromium and Chromium-Nickel Stainless Steel Plate, Sheet, and Strip for Pressure Vessels and for General Applications |
ASTM C 833 : 2023 | Standard Specification for Sintered (Uranium-Plutonium) Dioxide Pellets for Light Water Reactors |
ASTM B 359/B359M : 2023 | Standard Specification for Copper and Copper-Alloy Seamless Condenser and Heat Exchanger Tubes With Integral Fins |
ASTM E 531 : 2024 | Standard Practice for Surveillance Testing of High-Temperature Nuclear Component Materials |
ASTM B 197/B197M : 2020 : EDT 1 | Standard Specification for Copper-Beryllium Alloy Wire |
ASTM B 408 : 2022 | Standard Specification for Nickel-Iron-Chromium Alloy Rod and Bar |
ASTM B 903 : 2015 : R2022 | Standard Specification for Seamless Copper Heat Exchanger Tubes With Internal Enhancement |
ASTM A 376/A376M : 2022 | Standard Specification for Seamless Austenitic Steel Pipe for High-Temperature Service |
ASTM B 775/B775M : 2022 | Standard Specification for General Requirements for Nickel and Nickel Alloy Welded Pipe |
ASTM B 166 : 2024 | Standard Specification for Nickel-Chromium-Aluminum Alloy, Nickel-Chromium-Iron Alloys, Nickel-Chromium-Cobalt-Molybdenum Alloy, Nickel-Iron-Chromium-Tungsten Alloy, and Nickel-Chromium-Molybdenum-Copper Alloy Rod, Bar, and Wire |
ASTM B 575 : 2017 : R2023 | Standard Specification for Low-Carbon Nickel-Chromium-Molybdenum, Low-Carbon Nickel-Chromium-Molybdenum-Copper, Low-Carbon Nickel-Chromium-Molybdenum-Tantalum, Low-Carbon Nickel-Chromium-Molybdenum-Tungsten, and Low-Carbon Nickel-Molybdenum-Chromium Alloy Plate, Sheet, and Strip |
ASTM A 312/A312M : 2024 : REV A | Standard Specification for Seamless, Welded, and Heavily Cold Worked Austenitic Stainless Steel Pipes |
ASTM A 711/A711M : 2017 : R2022 | Standard Specification for Steel Forging Stock |
ASTM B 88 : 2022 | Standard Specification for Seamless Copper Water Tube |
ASTM A 729/A729M : 2017 : R2022 | Standard Specification for Carbon and Alloy Steel Axles, Heat-Treated, for Mass Transit and Electric Railway Service |
ASTM A 534 : 2017 : R2022 | Standard Specification for Carburizing Steels for Anti-Friction Bearings |
ASTM A 623 : 2022 | Standard Specification for Tin Mill Products, General Requirements |
ASTM F 3554 : 2022 | Standard Specification for Additive Manufacturing – Finished Part Properties – Grade 4340 (UNS G43400) via Laser Beam Powder Bed Fusion for Transportation Applications |
ASTM A 479/A479M : 2024 | Standard Specification for Stainless Steel Bars and Shapes for Use in Boilers and Other Pressure Vessels |
ASTM B 248M : 2022 | Standard Specification for General Requirements for Wrought Copper and Copper-Alloy Plate, Sheet, Strip, and Rolled Bar (Metric) |
ASTM A 6/A6M : 2024 : REV A | Standard Specification for General Requirements for Rolled Structural Steel Bars, Plates, Shapes, and Sheet Piling |
ASTM A 249/A249M : 2024 : REV A | Standard Specification for Welded Austenitic Steel Boiler, Superheater, Heat-Exchanger, and Condenser Tubes |
ASTM C 776 : 2017 : R2022 | Standard Specification for Sintered Uranium Dioxide Pellets for Light Water Reactors |
ASTM F 562 : 2022 | Standard Specification for Wrought 35Cobalt-35Nickel-20Chromium-10Molybdenum Alloy for Surgical Implant Applications (UNS R30035) |
ASTM B 444 : 2023 | Standard Specification for Nickel-Chromium-Molybdenum-Niobium Alloys<brk/> and Nickel-Chromium-Molybdenum-Silicon Alloy Pipe and Tube |
ASTM B 506 : 2022 | Standard Specification for Copper-Clad Stainless Steel Sheet and Strip for Building Construction |
ASTM B 570 : 2022 | Standard Specification for Copper-Beryllium Alloy Forgings and Extrusions (UNS Nos. C17000 and C17200) |
ASTM F 2527 : 2024 | Standard Specification for Wrought Seamless and Welded and Drawn Cobalt Alloy Small Diameter Tubing for Surgical Implants (UNS R30003, UNS R30008, UNS R30035, UNS R30605, and UNS R31537) |
ASTM B 508 : 2022 | Standard Specification for Copper Alloy Strip for Flexible Metal Hose |
ASTM B 950 : 2023 | Standard Guide for Editorial Procedures and Form of Product Specifications for Copper and Copper Alloys |
ASTM A 765/A765M : 2007 : R2022 | Standard Specification for Carbon Steel and Low-Alloy Steel Pressure-Vessel-Component Forgings with Mandatory Toughness Requirements |
ASTM F 2257 : 2022 | Standard Specification for Wrought Seamless or Welded and Drawn 18Chromium-14Nickel-2.5Molybdenum Stainless Steel Small Diameter Tubing for Surgical Implants (UNS S31673) |
ASTM B 1020/B1020M : 2022 | Standard Specification for Seamless Nickel Alloy Mechanical Tubing and Hollow Bar |
ASTM B 906 : 2022 | Standard Specification for General Requirements for Flat-Rolled Nickel and Nickel Alloys Plate, Sheet, and Strip |
ASTM E 235/E235M : 2023 | Standard Specification for Type K and Type N Mineral-Insulated, Metal-Sheathed Thermocouples for Nuclear or for Other High-Reliability Applications |
ASTM B 353 : 2012 : R2022 : EDT 1 | Standard Specification for Wrought Zirconium and Zirconium Alloy Seamless and Welded Tubes for Nuclear Service (Except Nuclear Fuel Cladding) |
ASTM F 3635 : 2023 | Standard Specification for Additive Manufacturing – Finished Part Properties – Standard Specification for Niobium-Hafnium Alloy UNS R04295 via Laser Beam Powder Bed Fusion for Spaceflight Applications |
ASTM F 835 : 2023 | Standard Specification for Alloy Steel Socket Button, Low and Flat Countersunk Head Cap Screws |
ASTM G 108 : 2023 | Standard Test Methods for Electrochemical Reactivation (EPR) for Detecting Sensitization of AISI Type 304 and 304L Stainless Steels |
ASTM B 121/B121M : 2023 | Standard Specification for Leaded Brass Plate, Sheet, Strip, and Rolled Bar |
ASTM A 403/A403M : 2022 : REV B | Standard Specification for Wrought Austenitic Stainless Steel Piping Fittings |
ASTM A 1100 : 2016 : R2022 | Standard Guide for Qualification and Control of Induction Heat Treating |
ASTM G 133 : 2022 | Standard Test Method for Linearly Reciprocating Ball-on-Flat Sliding Wear |
ASTM B 163 : 2022 | Standard Specification for Seamless Nickel and Nickel Alloy Condenser and Heat-Exchanger Tubes |
ASTM B 194 : 2022 | Standard Specification for Copper-Beryllium Alloy Plate, Sheet, Strip, and Rolled Bar |
ASTM B 168 : 2019 : EDT 1 | Standard Specification for Nickel-Chromium-Aluminum Alloys (UNS N06699), Nickel-Chromium-Iron Alloys (UNS N06600, N06601, N06603, N06690, N06693, N06025, N06045, and N06696), Nickel-Chromium-Cobalt-Molybdenum Alloy (UNS N06617), Nickel-Iron-Chromium-Tungsten Alloy (UNS N06674), and Nickel-Chromium-Molybdenum-Copper Alloy (UNS N06235) Plate, Sheet, and Strip |
ASTM B 1003 : 2016 : R2023 | Standard Specification for Seamless Copper Tube for Linesets |
ASTM F 2384 : 2024 | Standard Specification for Wrought Zirconium-2.5Niobium Alloy for Surgical Implant Applications (UNS R60901) |
ASTM B 248 : 2022 | Standard Specification for General Requirements for Wrought Copper and Copper-Alloy Plate, Sheet, Strip, and Rolled Bar |
ASTM E 585/E585M : 2023 | Standard Specification for Compacted Mineral-Insulated, Metal-Sheathed, Base Metal Thermocouple Cable |
ASTM A 266/A266M : 2024 | Standard Specification for Carbon Steel Forgings for Pressure Vessel Components |
SAE AMS6448N | Steel, Bars, Forgings, Mechanical Tubing, and Forging Stock Aircraft Quality 0.95Cr - 0.22V (0.48 - 0.53C) (6150) |
ASTM E 7 : 2017 | Standard Terminology Relating to Metallography |
ASTM E 1181 : 2002 : R2023 | Standard Test Methods for Characterizing Duplex Grain Sizes |
ASTM E 883 : 2011 : R2017 | Standard Guide for Reflected–Light Photomicrography |
ASTM E 7 : 2022 | Standard Terminology Relating to Metallography |
ASTM E 3 : 2011 : R2017 | Standard Guide for Preparation of Metallographic Specimens |
ASTM E 691 : 2023 | Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method |
ASTM E 883 : 2011 : R2024 | Standard Guide for Reflected–Light Photomicrography |
ASTM E 691 : 2022 | Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method |
ASTM E 691 : 2021 | Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method |
ASTM E 1382 : 1997 : R2023 | Standard Test Methods for Determining Average Grain Size Using Semiautomatic and Automatic Image Analysis |
ASTM E 407 : 2007 : R2015 : EDT 1 | Standard Practice for Microetching Metals and Alloys |
ASTM E 407 : 2023 | Standard Practice for Microetching Metals and Alloys |
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