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BS EN ISO 16931:2009

Current

Current

The latest, up-to-date edition.

Animal and vegetable fats and oils. Determination of polymerized triacylglycerols by high-performance size- exclusion chromatography (HPSEC)

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

31-05-2009

€156.59
Excluding VAT

Foreword
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Reagents
6 Apparatus
7 Sampling
8 Preparation of test sample
9 Procedure
10 Expression of results
11 Precision
12 Test report
Annex A (informative) - Chromatograms
Annex B (informative) - Results of interlaboratory
        tests
Bibliography

Describes a method using high-performance size-exclusion chromatography (HPSEC) to determine the contents, as mass fractions, of polymerized triacylglycerols (PTAGs) in oils and fats which contain at least 3% (from peak areas) of these polymers.

Committee
AW/307
DevelopmentNote
Supersedes 00/705062 DC. (12/2001) Supersedes 08/30176577 DC. (05/2009)
DocumentType
Standard
Pages
16
PublisherName
British Standards Institution
Status
Current
Supersedes

This International Standard specifies a method using high-performance size-exclusion chromatography (HPSEC) to determine the contents, as mass fractions, of polymerized triacylglycerols (PTAGs) in oils and fats which contain at least 3%(from peak areas) of these polymers. PTAGs (strictly speaking dimeric and oligomeric triacylglycerols) are formed during the heating of fats and oils, and thus, the method serves to assess the thermal deterioration of frying fats after use.

This method is applicable to frying fats and fats and oils that have been thermally treated, provided that the content of PTAGs is at least 3%. It can also be applied to the determination of polymers in fats for animal feedstuffs, although in this case, the extraction method used can have an influence on the result.

NOTE For further details, see ISO6492[4].

ISO 6492:1999 Animal feeding stuffs — Determination of fat content
ISO 5725-1:1994 Accuracy (trueness and precision) of measurement methods and results — Part 1: General principles and definitions
ISO 5555:2001 Animal and vegetable fats and oils — Sampling
ISO 5725-2:1994 Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
ISO 661:2003 Animal and vegetable fats and oils — Preparation of test sample

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