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EN 15863:2015

Current

Current

The latest, up-to-date edition.

Characterization of waste - Leaching behaviour test for basic characterization - Dynamic monolithic leaching test with periodic leachant renewal, under fixed conditions

Published date

01-04-2015

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This European Standard is applicable for determining the leaching behaviour of monolithic wastes under dynamic conditions. The test is performed under fixed experimental conditions in this document. This test is aimed at determining the release as a function of time of inorganic constituents from a monolithic waste, when it is put into contact with an aqueous solution (leachant).This dynamic monolithic leaching test (DMLT) is a parameter specific test as specified in EN 12920 and is therefore not aimed at simulating real situations. The application of this test method alone is not sufficient for the determination of the detailed leaching behaviour of a monolithic waste under specified conditions.In the framework of EN 12920 and in combination with additional chemical information, the test results are used to identify the leaching mechanisms and their relative importance. The intrinsic properties can be used to predict the release of constituents at a given time frame, in order to assess the leaching behaviour of monolithic waste materials, placed in different situations or scenarios (including disposal and recycling scenarios).The test method applies to regularly shaped test portions of monolithic wastes with minimum dimensions of 40 mm in all directions that are assumed to maintain their integrity over a time frame relevant for the considered scenario. The test method applies to test portions for which the geometric surface area can be determined with the help of simple geometric equations. The test method applies to low permeable monolithic materials.Within the reproducibility ranges, the leaching results obtained with EN 15863 are expected to be equivalent to those obtained with CEN/TS 16637-2 (DMLT for construction products), because the main testing conditions are equalized in both standards. As shown in the results obtained with EN 15863 (see Annex E), they are also demonstrated to be comparable with EPA method 1315 (SW846). These observations imply that a monolithic waste tested with this European Standard, does not need to be tested a second time, when the material proves suitable for beneficial use in construction and provided it has not undergone a treatment or other changes modifying its leaching behaviour.NOTE 1If, in order to comply with the requirements of regular shape, the test portion is prepared by cutting or coring, then new surfaces are exposed which can lead to change(s) in leaching properties. On the other hand if the test portion is prepared by moulding, the surface will be dependent to the type of mould and the conditions of storage. If the intention is to evaluate the behaviour of the material core, the specimen needs to be stored without any contact with air to avoid carbonation.NOTE 2For monolithic waste materials with a saturated hydraulic conductivity higher than 10−8 m/s water is likely to percolate through the monolith rather than flow around. In such cases relating the release to the geometric surface can lead to misinterpretation. A percolation test is more appropriate then (e.g. CEN/TS 14405).This procedure may not be applicable to materials reacting with the leachant, leading for example to excessive gas emission or an excessive heat release.This document has been developed to determine the release of mainly inorganic constituents from wastes. It does not take into account the particular characteristics of organic constituents, nor the consequences of microbiological processes in organic degradable wastes.

Committee
CEN/TC 444
DevelopmentNote
Supersedes CEN/TS 15863 & PREN 15863. (04/2015)
DocumentType
Standard
PublisherName
Comite Europeen de Normalisation
Status
Current
Supersedes

Standards Relationship
I.S. EN 15863:2015 Identical
PN EN 15863 : 2015 Identical
BS EN 15863:2015 Identical
UNE-EN 15863:2015 Identical
NBN EN 15863 : 2015 Identical
NF EN 15863 : 2015 Identical
NEN EN 15863 : 2015 Identical
DIN EN 15863:2015-06 Identical
SN EN 15863:2015 Identical
NS EN 15863 : 2015 Identical
UNI EN 15863 : 2015 Identical
UNE-EN 15863:2015 Identical

UNE-EN 15002:2015 Characterization of waste - Preparation of test portions from the laboratory sample
I.S. EN 15002:2015 CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
PD CEN/TS 16660:2015 Characterization of waste. Leaching behaviour test. Determination of the reducing character and the reducing capacity
PD CEN/TS 15864:2012 Characterisation of waste. Leaching behaviour test for basic characterisation. Dynamic monolithic leaching test with continuous leachant renewal under conditions relevant for specified scenario(s)
S.R. CEN/TS 15864:2015 CHARACTERISATION OF WASTE - LEACHING BEHAVIOUR TEST FOR BASIC CHARACTERIZATION - DYNAMIC MONOLITHIC LEACHING TEST WITH CONTINUOUS LEACHANT RENEWAL UNDER CONDITIONS RELEVANT FOR SPECIFIED SCENARIO(S)
DIN EN 15002:2015-07 CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
EN 15002:2015 Characterization of waste - Preparation of test portions from the laboratory sample
S.R. CEN/TS 16660:2015 CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TEST - DETERMINATION OF THE REDUCING CHARACTER AND THE REDUCING CAPACITY
BS EN 15002:2015 Characterization of waste. Preparation of test portions from the laboratory sample
CEN/TS 15864:2015 Characterization of waste - Leaching behaviour test for basic characterization - Dynamic monolithic leaching test with continuous leachant renewal under conditions relevant for specified scenario(s)
CEN/TS 16660:2015 Characterization of waste - Leaching behaviour test - Determination of the reducing character and the reducing capacity

EN 12457-2:2002 Characterisation of waste - Leaching - Compliance test for leaching of granular waste materials and sludges - Part 2: One stage batch test at a liquid to solid ratio of 10 l/kg for materials with particle size below 4 mm (without or with size reduction)
CEN/TS 16637-2:2014 Construction products - Assessment of release of dangerous substances - Part 2: Horizontal dynamic surface leaching test
ENV 12920 : 1997 CHARACTERIZATION OF WASTE - METHODOLOGY FOR THE DETERMINATION OF THE LEACHING BEHAVIOUR OF WASTE UNDER SPECIFIED CONDITIONS
EN 14997:2015 Characterization of waste - Leaching behaviour test - Influence of pH on leaching with continuous pH control
NEN 7345 : 1995 LEACHING CHARACTERISTICS OF SOLID EARTHY AND STONY BUILDING AND WASTE MATERIALS - LEACHING TESTS - DETERMINATION OF THE LEACHING OF INORGANIC COMPONENTS FROM BUILDINGS AND MONOLITIC WASTE MATERIALS WITH THE DIFFUSION TEST
EN 12457-4:2002 Characterisation of waste - Leaching - Compliance test for leaching of granular waste materials and sludges - Part 4: One stage batch test at a liquid to solid ratio of 10 l/kg for materials with particle size below 10 mm (without or with size reduction)
EN 14346:2006 Characterization of waste - Calculation of dry matter by determination of dry residue or water content
ISO 5667-3:2012 Water quality Sampling Part 3: Preservation and handling of water samples
CEN/TS 15864:2015 Characterization of waste - Leaching behaviour test for basic characterization - Dynamic monolithic leaching test with continuous leachant renewal under conditions relevant for specified scenario(s)
EN 12457-1:2002 Characterisation of waste - Leaching - Compliance test for leaching of granular waste materials and sludges - Part 1: One stage batch test at a liquid to solid ratio of 2 l/kg for materials with high solid content and with particle size below 4 mm (without or with size reduction)
ISO 5725-2:1994 Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
EN 16192:2011 Characterization of waste - Analysis of eluates
EN ISO 5667-3:2012 Water quality - Sampling - Part 3: Preservation and handling of water samples (ISO 5667-3:2012)
ISO 3696:1987 Water for analytical laboratory use — Specification and test methods
EN 12920:2006+A1:2008 Characterization of waste - Methodology for the determination of the leaching behaviour of waste under specified conditions
EN ISO 3696:1995 Water for analytical laboratory use - Specification and test methods (ISO 3696:1987)
EN 15002:2015 Characterization of waste - Preparation of test portions from the laboratory sample
EN 12457-3:2002 Characterisation of waste - Leaching - Compliance test for leaching of granular waste materials and sludges - Part 3: Two stage batch test at a liquid to solid ratio of 2 l/kg and 8 l/kg for materials with high solid content and with particle size below 4 mm (without or with size reduction)
CEN/TS 14405 : 2004 CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TESTS - UP-FLOW PERCOLATION TEST (UNDER SPECIFIED CONDITIONS)
CEN/TS 15862:2012 Characterisation of waste - Compliance leaching test - One stage batch leaching test for monoliths at fixed liquid to surface area ratio (L/A) for test portions with fixed minimum dimensions
EN 14899:2005 Characterization of waste - Sampling of waste materials - Framework for the preparation and application of a Sampling Plan
EN 14429:2015 Characterization of waste - Leaching behaviour test - Influence of pH on leaching with initial acid/base addition

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