PREN 16167 : DRAFT 2017
Current
The latest, up-to-date edition.
SOIL, TREATED BIOWASTE AND SLUDGE - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)
12-01-2013
European foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Interferences
6 Safety remarks
7 Reagents
8 Apparatus
9 Sample storage and preservation
10 Procedure
11 Performance characteristics
12 Precision
13 Test report
Annex A (informative) - Repeatability and
reproducibility data
Annex B (informative) - Examples for
retention times of PCBs
Annex C (informative) - Calculation method for
the estimation of total PCB content
Bibliography
Defines the method for quantitative determination of seven selected polychlorinated biphenyls (PCB28, PCB52, PCB101, PCB118, PCB138, PCB153 and PCB180) in sludge, treated biowaste and soil using GC-MS and GC-ECD.
| Committee |
TC 444
|
| DocumentType |
Draft
|
| PublisherName |
Comite Europeen de Normalisation
|
| Status |
Current
|
| Standards | Relationship |
| NEN EN 16167 : 2018 | Identical |
| 17/30364002 DC : DRAFT OCT 2017 | Identical |
| DIN EN 16167:2012-11 | Identical |
| NEN EN 16167 : 2012 | Identical |
| 17/30364002 DC : 0 | Identical |
| 10/30147454 DC : 0 | Identical |
| EN ISO 6468:1996 | Water quality - Determination of certain organochlorine insecticides, polychlorinated biphenyls and chlorobenzenes - Gas chromatographic method after liquid-liquid extraction (ISO 6468:1996) |
| EN 12766-1:2000 | Petroleum products and used oils - Determination of PCBs and related products - Part 1: Separation and determination of selected PCB congeners by gas chromatography (GC) using an electron capture detector (ECD) |
| ISO 22892:2006 | Soil quality Guidelines for the identification of target compounds by gas chromatography and mass spectrometry |
| EN 61619:1997 | Insulating liquids - Contamination by polychlorinated biphenyls (PCBs) - Method of determination by capillary column gas chromatography |
| EN 15308:2016 | Characterization of waste - Determination of selected polychlorinated biphenyls (PCB) in solid waste by gas chromatography with electron capture or mass spectrometric detection |
| ISO 5667-15:2009 | Water quality — Sampling — Part 15: Guidance on the preservation and handling of sludge and sediment samples |
| EN ISO 16720:2007 | Soil quality - Pretreatment of samples by freeze-drying for subsequent analysis (ISO 16720:2005) |
| EN 12766-2:2001 | Petroleum products and used oils - Determination of PCBs and related products - Part 2: Calculation of polychlorinated biphenyl (PCB) content |
| ISO 5725-2:1994 | Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method |
| ISO 8466-1:1990 | Water quality Calibration and evaluation of analytical methods and estimation of performance characteristics Part 1: Statistical evaluation of the linear calibration function |
| EN ISO 22892:2011 | Soil quality - Guidelines for the identification of target compounds by gas chromatography and mass spectrometry (ISO 22892:2006) |
| EN ISO 5667-15:2009 | Water quality - Sampling - Part 15: Guidance on the preservation and handling of sludge and sediment samples (ISO 5667-15:2009) |
| EN 15934:2012 | Sludge, treated biowaste, soil and waste - Calculation of dry matter fraction after determination of dry residue or water content |
| EN 16179:2012 | Sludge, treated biowaste and soil - Guidance for sample pretreatment |
| CEN/TS 16181:2013 | Sludge, treated biowaste and soil - Determination of polycyclic aromatic hydrocarbons (PAH) by gas chromatography (GC) and high performance liquid chromatography (HPLC) |
| ISO 18512:2007 | Soil quality Guidance on long and short term storage of soil samples |
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