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ASTM A 262 : 2015 : REDLINE

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Current

The latest, up-to-date edition.

Standard Practices for Detecting Susceptibility to Intergranular Attack in Austenitic Stainless Steels

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English

Published date

01-09-2015

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CONTAINED IN VOL. 01.03, 2017 Defines the following five tests: 1) Practice A - Oxalic Acid Etch Test for Classification of Etch Structures of Austenitic Stainless Steels, 2) Practice B - Ferric Sulfate-Sulfuric Acid Test for Detecting Susceptibility to Intergranular Attack in Austenitic Stainless Steels, 3) Practice C - Nitric Acid Test for Detecting Susceptibility to Intergranular Attack in Austenitic Stainless Steels, 4) Practice E - Copper-Copper Sulfate-Sulfuric Acid Test for Detecting Susceptibility to Intergranular Attack in Austenitic Stainless Steels, and 5) Practice F - Copper-Copper Sulfate-50% Sulfuric Acid Test for Detecting Susceptibility to Intergranular Attack in Molybdenum-Bearing Cast Austenitic Stainless Steels.

Committee
A 01
DevelopmentNote
Supersedes ASTM A 393. (04/2002)
DocumentType
Redline
Pages
27
PublisherName
American Society for Testing and Materials
Status
Current

1.1These practices cover the following five tests:

1.1.1Practice A—Oxalic Acid Etch Test for Classification of Etch Structures of Austenitic Stainless Steels (Sections 4 to 13, inclusive),

1.1.2Practice B—Ferric Sulfate-Sulfuric Acid Test for Detecting Susceptibility to Intergranular Attack in Austenitic Stainless Steels (Sections 14 to 25, inclusive),

1.1.3Practice C—Nitric Acid Test for Detecting Susceptibility to Intergranular Attack in Austenitic Stainless Steels (Sections 26 to 36, inclusive),

1.1.4Practice E—Copper–Copper Sulfate–Sulfuric Acid Test for Detecting Susceptibility to Intergranular Attack in Austenitic Stainless Steels (Sections 37 to 46, inclusive), and

1.1.5Practice F—Copper–Copper Sulfate–50 % Sulfuric Acid Test for Detecting Susceptibility to Intergranular Attack in Molybdenum-Bearing Austenitic Stainless Steels (Sections 47 to 58, inclusive).

1.2The Oxalic Acid Etch Test is a rapid method of identifying, by simple etching, those specimens of certain stainless steel grades that are essentially free of susceptibility to intergranular attack associated with chromium carbide precipitates. These specimens will have low corrosion rates in certain corrosion tests and therefore can be eliminated (screened) from testing as “acceptable.” The etch test is applicable only to those grades listed in the individual hot acid tests and classifies the specimens either as “acceptable” or as “suspect.”

1.3The ferric sulfate-sulfuric acid test, the copper–copper sulfate–50 % sulfuric acid test, and the nitric acid test are based on weight loss determinations and, thus, provide a quantitative measure of the relative performance of specimens evaluated. In contrast, the copper–copper sulfate–16 % sulfuric acid test is based on visual examination of bend specimens and, therefore, classifies the specimens only as acceptable or nonacceptable.

1.4The presence or absence of intergranular attack in these tests is not necessarily a measure of the performance of the material in other corrosive environments. These tests do not provide a basis for predicting resistance to forms of corrosion other than intergranular, such as general corrosion, pitting, or stress-corrosion cracking.

Note 1:See Appendix X1 for information regarding test selection.

1.5The values stated in SI units are to be regarded as standard. The inch-pound equivalents are in parentheses and may be approximate.

1.6This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Some specific hazards statements are given in 10.1, 20.1.1, 20.1.9, 31.3, 34.4, 53.1.1, and 53.1.10.

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PD 8010-2:2004 Code of practice for pipelines Subsea pipelines
ASTM F 1387 : 1999 : R2005 Standard Specification for Performance of Piping and Tubing Mechanically Attached Fittings
ASTM A 493 : 2016 : REDLINE Standard Specification for Stainless Steel Wire and Wire Rods for Cold Heading and Cold Forging
ASTM A 632 : 2004 : R2009 Standard Specification for Seamless and Welded Austenitic Stainless Steel Tubing (Small-Diameter) for General Service
ASTM G 31 : 2012 GUIDE FOR LABORATORY IMMERSION CORROSION TESTING OF METALS
ASTM F 2281 : 2004 : R2012 Standard Specification for Stainless Steel and Nickel Alloy Bolts, Hex Cap Screws, and Studs, for Heat Resistance and High Temperature Applications
SAE AMS5556J Steel, Corrosion and Heat-Resistant, Seamless or Welded Hydraulic Tubing 18Cr - 11Ni - 0.70Cb (347) Solution Heat Treated
ASTM B 853 : 2016 : REDLINE Standard Specification for Powder Metallurgy (PM) Boron Stainless Steel Structural Components
ASTM F 2229 : 2012 : REDLINE Standard Specification for Wrought, Nitrogen Strengthened 23Manganese-21Chromium-1Molybdenum Low-Nickel Stainless Steel Alloy Bar and Wire for Surgical Implants (UNS S29108)
SAE AMS5513J Steel, Corrosion-Resistant, Sheet, Strip, and Plate 19Cr – 9.2Ni (SAE 30304) Solution Heat Treated
SAE MA1339 Hose Assembly, Polytetrafluoroethylene, Metallic Reinforced, 21,000 kPa, 204 °C, Lightweight, Hydraulic and Pneumatic, Metric
SAE AS1339H Hose Assembly, Polytetrafluoroethylene, Metallic Reinforced, 3000 psi, 400 °F, Lightweight, Hydraulic and Pneumatic
SAE AMS6474B Forgings, Hardenable Steels and Corrosion-Resistant Steels Heat-Treated, Finished-Part Properties Short-Transverse Tensile Strength and Fracture Toughness
SAE AS1227C Hose Assembly, Convoluted Polytetrafluoroethylene, Metallic Reinforced, Low Pressure, Up to 400 °F, Aircraft
AWS WHC4.05 : 0 MATERIALS AND APPLICATION - PART 1 - WELDING HANDBOOK, 9TH EDITION, VOLUME 4 - CHAPTER 5: STAINLESS AND HEAT-RESISTANT STEELS
SAE AS4897 Hose Assembly, Polytetrafluoroethylene (PTFE), Low Pressure, 450 °F and Fireproof, Procurement Specification for
ASTM F 621 : 2012 : R2017 Standard Specification for Stainless Steel Forgings for Surgical Implants
API 5LD : 2017 CRA CLAD OR LINED STEEL PIPE
ASTM F 1387 : 1999 Standard Specification for Performance of Piping and Tubing Mechanically Attached Fittings
ASTM F 3160 : 2016 Standard Guide for Metallurgical Characterization of Absorbable Metallic Materials for Medical Implants
ASTM F 56 : 1982 Specification for Stainless Steel Sheet and Strip for Surgical Implants (Withdrawn 1989)
ASTM B 463 : 2010 : R2016 Standard Specification for UNS N08020 Alloy Plate, Sheet, and Strip
ASTM A 943/A943M : 2001 Standard Specification for Spray-Formed Seamless Austenitic Stainless Steel Pipes
ASTM F 594 : 2009 : EDT 1 Standard Specification for Stainless Steel Nuts
API 7-1 : 2006/ADD 4 : 2019 SPECIFICATION FOR ROTARY DRILL STEM ELEMENTS
BS EN ISO 10424-1:2004 Petroleum and natural gas industries. Rotary drilling equipment Rotary drill stem elements
EN ISO 10424-1:2004 Petroleum and natural gas industries - Rotary drilling equipment - Part 1: Rotary drill stem elements (ISO 10424-1:2004)
ASTM F 880M : 2016 : REDLINE Standard Specification for Stainless Steel Socket Set Screws (Metric)
ASTM B 472 : 2010 : R2015 Standard Specification for Nickel Alloy Billets and Bars for Reforging
MIL H 85800 : 0 HOSE ASSEMBLIES, POLYTETRAFLUOROETHYLENE, ARAMID FIBER REINFORCED, 5000 & 8000 PSI, GENERAL SPECIFICATION FOR
SAE AMS5363F Steel Castings, Sand and Centrifugal, Corrosion and Heat Resistant 18.5Cr - 10.5Ni - 0.90 (Cb+Ta) Solution Heat Treated
ASTM A 851 : 1996 Standard Specification for High-Frequency Induction Welded, Unannealed, Austenitic Steel Condenser Tubes (Withdrawn 2002)
QQ-S-766 Revision D:1988 STEEL PLATES, SHEETS AND STRIP CORROSION RESISTING
SAE AS 7229 : 2013 RIVETS, STEEL, CORROSION AND HEAT RESISTANT, 18CR - 10.5NI - 0.70(CB+TA), SOLUTION HEAT TREATED, PROCUREMENT SPECIFICATION FOR
SAE AMS5560N Steel, Corrosion Resistant, Seamless Tubing 19Cr - 10Ni (304) Solution Heat Treated
SAE AMS5639J Steel, Corrosion-Resistant, Bars, Wire, Forgings, Mechanical Tubing, and Rings 19Cr - 10Ni Solution Heat Treated
QQ-S-763 Revision F:1996 STEEL BARS, WIRE, SHAPES AND FORGINGS; CORROSION RESISTANT
ISO 21610:2009 Corrosion of metals and alloys Accelerated corrosion test for intergranular corrosion susceptibility of austenitic stainless steels
BS 7993:2011 Twin ferrule connectors and associated tubing for 316 stainless steel systems. Specification and test methods
ASTM G 4 : 2001 Standard Guide for Conducting Corrosion Tests in Field Applications
ASTM G 1 : 2003 Standard Practice for Preparing, Cleaning, and Evaluating Corrosion Test Specimens
SAE AMS5648M Steel, Corrosion and Heat-Resistant, Bars, Wire, Forgings, Tubing, and Rings, 17Cr - 12Ni - 2.5Mo (316) Solution Heat Treated
SAE AMS5570Q Steel, Corrosion and Heat-Resistant, Seamless Tubing 18Cr - 11Ni - 0.40Ti (321) Solution Heat Treated
ASTM F 880 : 2012 Standard Specification for Stainless Steel Socket, Square Head, and Slotted Headless-Set Screws
BS 8010-3:1993 Code of practice for pipelines Pipelines subsea: design, construction and installation
ASTM F 3301 : 2018 Standard for Additive Manufacturing – Post Processing Methods – Standard Specification for Thermal Post-Processing Metal Parts Made Via Powder Bed Fusion
MIL-C-24707-3 Base Document:1989 CASTINGS, FERROUS, CORROSION RESISTANT, AUSTENITIC, CHROMIUM NICKEL
IFI 153 : 2003 STAINLESS STEEL WIRE AND RODS FOR MECHANICAL FASTENERS
SAE AMS5896B Steel, Corrosion and Heat-Resistant, Seamless or Welded Hydraulic Tubing 18.5Cr - 10.5Ni - 0.55Ti (321) Solution Heat Treated and Cold Drawn, 1/8 Hard Temper
AWWA C223 : 2013 FABRICATED STEEL AND STAINLESS STEEL-TAPPING SLEEVES
SAE MA2079 Hose Assembly, Convoluted Polytetrafluoroethylene, High Temperature, Medium Pressure, Aircraft, Metric
AWS WHC4.07 : 0 MATERIALS AND APPLICATION - PART 1 - WELDING HANDBOOK, 9TH EDITION, VOLUME 4 - CHAPTER 7: SURFACING MATERIALS
MSS SP 114 : 2007 CORROSION RESISTANT PIPE FITTINGS THREADED AND SOCKET WELDING CLASS 150 AND 1000
SAE AMS5571J Steel, Corrosion and Heat-Resistant, Seamless Tubing 18Cr - 10.5Ni - 0.70Cb (Nb) (347) Solution Heat Treated
SAE MA4623 Hose Assembly, Polytetrafluoroethylene, Para Aramid Reinforced Heavy-Duty, 21 000 kPa, 135 °C, Aircraft Hydraulic Systems, Metric
ASTM F 3184 : 2016 Standard Specification for Additive Manufacturing Stainless Steel Alloy (UNS S31603) with Powder Bed Fusion
ASTM B 672 : 2002 : R2007 Standard Specification for Nickel-Iron-Chromium-Molybdenum-Columbium Stabilized Alloy (UNS N08700) Bar and Wire
SAE AS1946E Hose Assembly, Polytetrafluoroethylene, Metallic Reinforced, Up to 1500 psi and 450 °F, Hydraulic and Pneumatic
ASTM G 4 : 2001 : R2014 Standard Guide for Conducting Corrosion Tests in Field Applications (Withdrawn 2023)
ASTM F 879M : 2016 : REDLINE Standard Specification for Stainless Steel Socket Button and Flat Countersunk Head Cap Screws (Metric)
ASTM G 28 : 2002 Standard Test Methods of Detecting Susceptibility to Intergranular Corrosion in Wrought, Nickel-Rich, Chromium-Bearing Alloys
ASTM A 778/A778M : 2016 : REDLINE Standard Specification for Welded, Unannealed Austenitic Stainless Steel Tubular Products
ASTM G 28 : 2002 : R2008 Standard Test Methods for Detecting Susceptibility to Intergranular Corrosion in Wrought, Nickel-Rich, Chromium-Bearing Alloys
ASTM G 1 : 2003 : R2017 : EDT 1 Standard Practice for Preparing, Cleaning, and Evaluating Corrosion Test Specimens
ASTM G 1 : 2003 : R2011 Standard Practice for Preparing, Cleaning, and Evaluating Corrosion Test Specimens
ASTM B 473 : 2007 : R2013 Standard Specification for UNS N08020, UNS N08024, and UNS N08026 Nickel Alloy Bar and Wire
ASTM F 593 : 2017 : REDLINE Standard Specification for Stainless Steel Bolts, Hex Cap Screws, and Studs
ASTM F 621 : 2012 Standard Specification for Stainless Steel Forgings for Surgical Implants
ASTM B 468 : 2010 Standard Specification for Welded UNS N08020 Alloy Tubes
ASTM B 804 : 2002 Standard Specification for UNS N08367 and UNS N08926 Welded Pipe
ISO 10424-1:2004 Petroleum and natural gas industries — Rotary drilling equipment — Part 1: Rotary drill stem elements
ASME NQA 2 : 89 SPECIAL NOTICE QUALITY ASSURANCE REQUIREMENTS FOR NUCLEAR FACILITY APPLICATIONS

ASME PV CODE 9 : 2017 BOILER AND PRESSURE VESSEL CODE - WELDING, BRAZING, AND FUSING QUALIFICATIONS - QUALIFICATION STANDARD FOR WELDING, BRAZING, AND FUSING PROCEDURES; WELDERS; BRAZERS; AND WELDING, BRAZING, AND FUSING OPERATORS
ISO 3651-2:1998 Determination of resistance to intergranular corrosion of stainless steels — Part 2: Ferritic,austenitic and ferritic-austenitic (duplex) stainless steels — Corrosion test in media containing sulfuric acid
ASTM A 380/A380M : 2017 Standard Practice for Cleaning, Descaling, and Passivation of Stainless Steel Parts, Equipment, and Systems

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