ASTM A 262 : 2015 : REDLINE
Current
The latest, up-to-date edition.
Standard Practices for Detecting Susceptibility to Intergranular Attack in Austenitic Stainless Steels
English
01-09-2015
CONTAINED IN VOL. 01.03, 2017 Defines the following five tests: 1) Practice A - Oxalic Acid Etch Test for Classification of Etch Structures of Austenitic Stainless Steels, 2) Practice B - Ferric Sulfate-Sulfuric Acid Test for Detecting Susceptibility to Intergranular Attack in Austenitic Stainless Steels, 3) Practice C - Nitric Acid Test for Detecting Susceptibility to Intergranular Attack in Austenitic Stainless Steels, 4) Practice E - Copper-Copper Sulfate-Sulfuric Acid Test for Detecting Susceptibility to Intergranular Attack in Austenitic Stainless Steels, and 5) Practice F - Copper-Copper Sulfate-50% Sulfuric Acid Test for Detecting Susceptibility to Intergranular Attack in Molybdenum-Bearing Cast Austenitic Stainless Steels.
Committee |
A 01
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DevelopmentNote |
Supersedes ASTM A 393. (04/2002)
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DocumentType |
Redline
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Pages |
27
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PublisherName |
American Society for Testing and Materials
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Status |
Current
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1.1These practices cover the following five tests:
1.1.1Practice A—Oxalic Acid Etch Test for Classification of Etch Structures of Austenitic Stainless Steels (Sections 4 to 13, inclusive),
1.1.2Practice B—Ferric Sulfate-Sulfuric Acid Test for Detecting Susceptibility to Intergranular Attack in Austenitic Stainless Steels (Sections 14 to 25, inclusive),
1.1.3Practice C—Nitric Acid Test for Detecting Susceptibility to Intergranular Attack in Austenitic Stainless Steels (Sections 26 to 36, inclusive),
1.1.4Practice E—Copper–Copper Sulfate–Sulfuric Acid Test for Detecting Susceptibility to Intergranular Attack in Austenitic Stainless Steels (Sections 37 to 46, inclusive), and
1.1.5Practice F—Copper–Copper Sulfate–50 % Sulfuric Acid Test for Detecting Susceptibility to Intergranular Attack in Molybdenum-Bearing Austenitic Stainless Steels (Sections 47 to 58, inclusive).
1.2The Oxalic Acid Etch Test is a rapid method of identifying, by simple etching, those specimens of certain stainless steel grades that are essentially free of susceptibility to intergranular attack associated with chromium carbide precipitates. These specimens will have low corrosion rates in certain corrosion tests and therefore can be eliminated (screened) from testing as “acceptable.” The etch test is applicable only to those grades listed in the individual hot acid tests and classifies the specimens either as “acceptable” or as “suspect.”
1.3The ferric sulfate-sulfuric acid test, the copper–copper sulfate–50 % sulfuric acid test, and the nitric acid test are based on weight loss determinations and, thus, provide a quantitative measure of the relative performance of specimens evaluated. In contrast, the copper–copper sulfate–16 % sulfuric acid test is based on visual examination of bend specimens and, therefore, classifies the specimens only as acceptable or nonacceptable.
1.4The presence or absence of intergranular attack in these tests is not necessarily a measure of the performance of the material in other corrosive environments. These tests do not provide a basis for predicting resistance to forms of corrosion other than intergranular, such as general corrosion, pitting, or stress-corrosion cracking.
Note 1:See Appendix X1 for information regarding test selection.
1.5The values stated in SI units are to be regarded as standard. The inch-pound equivalents are in parentheses and may be approximate.
1.6This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Some specific hazards statements are given in 10.1, 20.1.1, 20.1.9, 31.3, 34.4, 53.1.1, and 53.1.10.
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API 7-1 SPANISH : 2006 | SPECIFICATION FOR ROTARY DRILL STEM ELEMENTS |
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SAE AMS5565L | Steel, Corrosion Resistant, Welded Tubing 19Cr - 9.5Ni (304) Solution Heat Treated |
ASTM G 108 : 1994 : R2004 : EDT 1 | Standard Test Method for Electrochemical Reactivation (EPR) for Detecting Sensitization of AISI Type 304 and 304L Stainless Steels |
SAE MA2126B | Hose Assembly, Polytetrafluoroethylene (PTFE), up to 232 °C and 10 500 kPa Procurement Specification, Metric (ISO/DIS 10502) |
SAE AS614D | Hose Assembly, Polytetrafluoroethylene, Metallic Reinforced, 4000 psi, 400 °F, Heavy Duty, Hydraulic and Pneumatic |
ASTM G 108 : 1994 : R2004 | Standard Test Method for Electrochemical Reactivation (EPR) for Detecting Sensitization of AISI Type 304 and 304L Stainless Steels |
ASTM A 409/A409M : 2015 : REDLINE | Standard Specification for Welded Large Diameter Austenitic Steel Pipe for Corrosive or High-Temperature Service |
ASTM A 632 : 2004 : R2014 | Standard Specification for Seamless and Welded Austenitic Stainless Steel Tubing (Small-Diameter) for General Service |
ASTM B 906 : 2002 : R2017 | Standard Specification for General Requirements for Flat-Rolled Nickel and Nickel Alloys Plate, Sheet, and Strip |
ASTM F 1387 : 1999 : R2012 | Standard Specification for Performance of Piping and Tubing Mechanically Attached Fittings |
ASTM G 28 : 2002 : R2015 | Standard Test Methods for Detecting Susceptibility to Intergranular Corrosion in Wrought, Nickel-Rich, Chromium-Bearing Alloys |
ASTM E 235/E235M : 2012 | Standard Specification for Type K and Type N Mineral-Insulated, Metal-Sheathed Thermocouples for Nuclear or for Other High-Reliability Applications |
ASTM B 672 : 2002 : R2013 | Standard Specification for Nickel-Iron-Chromium-Molybdenum-Columbium Stabilized Alloy (UNS N08700) Bar and Wire |
ASTM A 555/A555M : 2016 : REDLINE | Standard Specification for General Requirements for Stainless Steel Wire and Wire Rods |
ASTM B 906 :2002 | Standard Specification for General Requirements for Flat-Rolled Nickel and Nickel Alloys Plate, Sheet, and Strip |
ASTM B 906 : 2002 : R2006 | Standard Specification for General Requirements for Flat-Rolled Nickel and Nickel Alloys Plate, Sheet, and Strip |
ASTM G 108 : 1994 : R2015 | Standard Test Method for Electrochemical Reactivation (EPR) for Detecting Sensitization of AISI Type 304 and 304L Stainless Steels |
ASTM B 672 : 2002 | Standard Specification for Nickel-Iron-Chromium-Molybdenum-Columbium Stabilized Alloy (UNS N08700) Bar and Wire |
ASTM F 880 : 2012 : R2017 | Standard Specification for Stainless Steel Socket, Square Head, and Slotted Headless-Set Screws |
ASTM A 480/A480M : 2017-11 | SPECIFICATION FOR GENERAL REQUIREMENTS FOR FLAT-ROLLED STAINLESS AND HEAT-RESISTING STEEL PLATE, SHEET, AND STRIP |
ASTM A 270/A270M : 2015 : REDLINE | Standard Specification for Seamless and Welded Austenitic and Ferritic/Austenitic Stainless Steel Sanitary Tubing |
NASA KSC SPEC Z 0007 : 1994 | TUBING, STEEL, CORROSION RESISTANT TYPES 304 AND 316, SEAMLESS, ANNEALED, SPECIFICATION FOR |
ASTM F 2281 : 2004 | Standard Specification for Stainless Steel and Nickel Alloy Bolts, Hex Cap Screws, and Studs, for Heat Resistance and High Temperature Applications |
ASTM A 744/A744M : 2013 : REDLINE | Standard Specification for Castings, Iron-Chromium-Nickel, Corrosion Resistant, for Severe Service |
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DOD HDBK 270 : 0 | METALLIC MATERIALS, MAGNETIC PERMEABILITY AND ELECTRICAL CONDUCTIVITY, CHARACTERISTICS OF (METRIC) |
11/30124825 DC : 0 | BS 7993 - TWIN FERRULE CONNECTORS AND ASSOCIATED TUBING FOR 316 STAINLESS STEEL SYSTEMS - SPECIFICATION AND TEST METHODS |
SAE AMS5524L | Steel, Corrosion and Heat-Resistant, Sheet, Strip and Plate 18Cr - 13Ni - 2.5Mo (SAE 30316) Solution Heat Treated |
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MIL P 1144 : D NOTICE 1 | PIPE, CORROSION RESISTANT, STAINLESS STEEL, SEAMLESS OR WELDED |
ASTM A 943/A943M : 2001 : R2019 | Standard Specification for Spray-Formed Seamless Austenitic Stainless Steel Pipes (Withdrawn 2024) |
ASTM A 688/A688M : 2015-03 | SPECIFICATION FOR SEAMLESS AND WELDED AUSTENITIC STAINLESS STEEL FEEDWATER HEATER TUBES |
ASTM A 943/A943M : 2001 : R2014 | Standard Specification for Spray-Formed Seamless Austenitic Stainless Steel Pipes |
ASTM B 804 : 2002 : R2007 | Standard Specification for UNS N08367 and UNS N08926 Welded Pipe |
MIL-PRF-2939 Revision G:2001 | Cooling Coils, Air, Duct Type and Gravity Type, Naval Shipboard Environmental Control Systems |
ASTM F 837M : 2016 : REDLINE | Standard Specification for Stainless Steel Socket Head Cap Screws [Metric] |
SAE AMS5689G | Steel, Corrosion and Heat Resistant, Wire 18Cr - 10.5Ni - 0.40Ti (321) Solution Heat Treated |
AASHTO M 285M/M 285 : 2011 : R2015 | SPECIFICATION FOR CASTINGS, IRON-CHROMIUM-NICKEL, CORROSION RESISTANT, FOR SEVERE SERVICE |
PD 8010-2:2004 | Code of practice for pipelines Subsea pipelines |
ASTM F 1387 : 1999 : R2005 | Standard Specification for Performance of Piping and Tubing Mechanically Attached Fittings |
ASTM A 493 : 2016 : REDLINE | Standard Specification for Stainless Steel Wire and Wire Rods for Cold Heading and Cold Forging |
ASTM A 632 : 2004 : R2009 | Standard Specification for Seamless and Welded Austenitic Stainless Steel Tubing (Small-Diameter) for General Service |
ASTM G 31 : 2012 | GUIDE FOR LABORATORY IMMERSION CORROSION TESTING OF METALS |
ASTM F 2281 : 2004 : R2012 | Standard Specification for Stainless Steel and Nickel Alloy Bolts, Hex Cap Screws, and Studs, for Heat Resistance and High Temperature Applications |
SAE AMS5556J | Steel, Corrosion and Heat-Resistant, Seamless or Welded Hydraulic Tubing 18Cr - 11Ni - 0.70Cb (347) Solution Heat Treated |
ASTM B 853 : 2016 : REDLINE | Standard Specification for Powder Metallurgy (PM) Boron Stainless Steel Structural Components |
ASTM F 2229 : 2012 : REDLINE | Standard Specification for Wrought, Nitrogen Strengthened 23Manganese-21Chromium-1Molybdenum Low-Nickel Stainless Steel Alloy Bar and Wire for Surgical Implants (UNS S29108) |
SAE AMS5513J | Steel, Corrosion-Resistant, Sheet, Strip, and Plate 19Cr – 9.2Ni (SAE 30304) Solution Heat Treated |
SAE MA1339 | Hose Assembly, Polytetrafluoroethylene, Metallic Reinforced, 21,000 kPa, 204 °C, Lightweight, Hydraulic and Pneumatic, Metric |
SAE AS1339H | Hose Assembly, Polytetrafluoroethylene, Metallic Reinforced, 3000 psi, 400 °F, Lightweight, Hydraulic and Pneumatic |
SAE AMS6474B | Forgings, Hardenable Steels and Corrosion-Resistant Steels Heat-Treated, Finished-Part Properties Short-Transverse Tensile Strength and Fracture Toughness |
SAE AS1227C | Hose Assembly, Convoluted Polytetrafluoroethylene, Metallic Reinforced, Low Pressure, Up to 400 °F, Aircraft |
AWS WHC4.05 : 0 | MATERIALS AND APPLICATION - PART 1 - WELDING HANDBOOK, 9TH EDITION, VOLUME 4 - CHAPTER 5: STAINLESS AND HEAT-RESISTANT STEELS |
SAE AS4897 | Hose Assembly, Polytetrafluoroethylene (PTFE), Low Pressure, 450 °F and Fireproof, Procurement Specification for |
ASTM F 621 : 2012 : R2017 | Standard Specification for Stainless Steel Forgings for Surgical Implants |
API 5LD : 2017 | CRA CLAD OR LINED STEEL PIPE |
ASTM F 1387 : 1999 | Standard Specification for Performance of Piping and Tubing Mechanically Attached Fittings |
ASTM F 3160 : 2016 | Standard Guide for Metallurgical Characterization of Absorbable Metallic Materials for Medical Implants |
ASTM F 56 : 1982 | Specification for Stainless Steel Sheet and Strip for Surgical Implants (Withdrawn 1989) |
ASTM B 463 : 2010 : R2016 | Standard Specification for UNS N08020 Alloy Plate, Sheet, and Strip |
ASTM A 943/A943M : 2001 | Standard Specification for Spray-Formed Seamless Austenitic Stainless Steel Pipes |
ASTM F 594 : 2009 : EDT 1 | Standard Specification for Stainless Steel Nuts |
API 7-1 : 2006/ADD 4 : 2019 | SPECIFICATION FOR ROTARY DRILL STEM ELEMENTS |
BS EN ISO 10424-1:2004 | Petroleum and natural gas industries. Rotary drilling equipment Rotary drill stem elements |
EN ISO 10424-1:2004 | Petroleum and natural gas industries - Rotary drilling equipment - Part 1: Rotary drill stem elements (ISO 10424-1:2004) |
ASTM F 880M : 2016 : REDLINE | Standard Specification for Stainless Steel Socket Set Screws (Metric) |
ASTM B 472 : 2010 : R2015 | Standard Specification for Nickel Alloy Billets and Bars for Reforging |
MIL H 85800 : 0 | HOSE ASSEMBLIES, POLYTETRAFLUOROETHYLENE, ARAMID FIBER REINFORCED, 5000 & 8000 PSI, GENERAL SPECIFICATION FOR |
SAE AMS5363F | Steel Castings, Sand and Centrifugal, Corrosion and Heat Resistant 18.5Cr - 10.5Ni - 0.90 (Cb+Ta) Solution Heat Treated |
ASTM A 851 : 1996 | Standard Specification for High-Frequency Induction Welded, Unannealed, Austenitic Steel Condenser Tubes (Withdrawn 2002) |
QQ-S-766 Revision D:1988 | STEEL PLATES, SHEETS AND STRIP CORROSION RESISTING |
SAE AS 7229 : 2013 | RIVETS, STEEL, CORROSION AND HEAT RESISTANT, 18CR - 10.5NI - 0.70(CB+TA), SOLUTION HEAT TREATED, PROCUREMENT SPECIFICATION FOR |
SAE AMS5560N | Steel, Corrosion Resistant, Seamless Tubing 19Cr - 10Ni (304) Solution Heat Treated |
SAE AMS5639J | Steel, Corrosion-Resistant, Bars, Wire, Forgings, Mechanical Tubing, and Rings 19Cr - 10Ni Solution Heat Treated |
QQ-S-763 Revision F:1996 | STEEL BARS, WIRE, SHAPES AND FORGINGS; CORROSION RESISTANT |
ISO 21610:2009 | Corrosion of metals and alloys Accelerated corrosion test for intergranular corrosion susceptibility of austenitic stainless steels |
BS 7993:2011 | Twin ferrule connectors and associated tubing for 316 stainless steel systems. Specification and test methods |
ASTM G 4 : 2001 | Standard Guide for Conducting Corrosion Tests in Field Applications |
ASTM G 1 : 2003 | Standard Practice for Preparing, Cleaning, and Evaluating Corrosion Test Specimens |
SAE AMS5648M | Steel, Corrosion and Heat-Resistant, Bars, Wire, Forgings, Tubing, and Rings, 17Cr - 12Ni - 2.5Mo (316) Solution Heat Treated |
SAE AMS5570Q | Steel, Corrosion and Heat-Resistant, Seamless Tubing 18Cr - 11Ni - 0.40Ti (321) Solution Heat Treated |
ASTM F 880 : 2012 | Standard Specification for Stainless Steel Socket, Square Head, and Slotted Headless-Set Screws |
BS 8010-3:1993 | Code of practice for pipelines Pipelines subsea: design, construction and installation |
ASTM F 3301 : 2018 | Standard for Additive Manufacturing – Post Processing Methods – Standard Specification for Thermal Post-Processing Metal Parts Made Via Powder Bed Fusion |
MIL-C-24707-3 Base Document:1989 | CASTINGS, FERROUS, CORROSION RESISTANT, AUSTENITIC, CHROMIUM NICKEL |
IFI 153 : 2003 | STAINLESS STEEL WIRE AND RODS FOR MECHANICAL FASTENERS |
SAE AMS5896B | Steel, Corrosion and Heat-Resistant, Seamless or Welded Hydraulic Tubing 18.5Cr - 10.5Ni - 0.55Ti (321) Solution Heat Treated and Cold Drawn, 1/8 Hard Temper |
AWWA C223 : 2013 | FABRICATED STEEL AND STAINLESS STEEL-TAPPING SLEEVES |
SAE MA2079 | Hose Assembly, Convoluted Polytetrafluoroethylene, High Temperature, Medium Pressure, Aircraft, Metric |
AWS WHC4.07 : 0 | MATERIALS AND APPLICATION - PART 1 - WELDING HANDBOOK, 9TH EDITION, VOLUME 4 - CHAPTER 7: SURFACING MATERIALS |
MSS SP 114 : 2007 | CORROSION RESISTANT PIPE FITTINGS THREADED AND SOCKET WELDING CLASS 150 AND 1000 |
SAE AMS5571J | Steel, Corrosion and Heat-Resistant, Seamless Tubing 18Cr - 10.5Ni - 0.70Cb (Nb) (347) Solution Heat Treated |
SAE MA4623 | Hose Assembly, Polytetrafluoroethylene, Para Aramid Reinforced Heavy-Duty, 21 000 kPa, 135 °C, Aircraft Hydraulic Systems, Metric |
ASTM F 3184 : 2016 | Standard Specification for Additive Manufacturing Stainless Steel Alloy (UNS S31603) with Powder Bed Fusion |
ASTM B 672 : 2002 : R2007 | Standard Specification for Nickel-Iron-Chromium-Molybdenum-Columbium Stabilized Alloy (UNS N08700) Bar and Wire |
SAE AS1946E | Hose Assembly, Polytetrafluoroethylene, Metallic Reinforced, Up to 1500 psi and 450 °F, Hydraulic and Pneumatic |
ASTM G 4 : 2001 : R2014 | Standard Guide for Conducting Corrosion Tests in Field Applications (Withdrawn 2023) |
ASTM F 879M : 2016 : REDLINE | Standard Specification for Stainless Steel Socket Button and Flat Countersunk Head Cap Screws (Metric) |
ASTM G 28 : 2002 | Standard Test Methods of Detecting Susceptibility to Intergranular Corrosion in Wrought, Nickel-Rich, Chromium-Bearing Alloys |
ASTM A 778/A778M : 2016 : REDLINE | Standard Specification for Welded, Unannealed Austenitic Stainless Steel Tubular Products |
ASTM G 28 : 2002 : R2008 | Standard Test Methods for Detecting Susceptibility to Intergranular Corrosion in Wrought, Nickel-Rich, Chromium-Bearing Alloys |
ASTM G 1 : 2003 : R2017 : EDT 1 | Standard Practice for Preparing, Cleaning, and Evaluating Corrosion Test Specimens |
ASTM G 1 : 2003 : R2011 | Standard Practice for Preparing, Cleaning, and Evaluating Corrosion Test Specimens |
ASTM B 473 : 2007 : R2013 | Standard Specification for UNS N08020, UNS N08024, and UNS N08026 Nickel Alloy Bar and Wire |
ASTM F 593 : 2017 : REDLINE | Standard Specification for Stainless Steel Bolts, Hex Cap Screws, and Studs |
ASTM F 621 : 2012 | Standard Specification for Stainless Steel Forgings for Surgical Implants |
ASTM B 468 : 2010 | Standard Specification for Welded UNS N08020 Alloy Tubes |
ASTM B 804 : 2002 | Standard Specification for UNS N08367 and UNS N08926 Welded Pipe |
ISO 10424-1:2004 | Petroleum and natural gas industries — Rotary drilling equipment — Part 1: Rotary drill stem elements |
ASME NQA 2 : 89 SPECIAL NOTICE | QUALITY ASSURANCE REQUIREMENTS FOR NUCLEAR FACILITY APPLICATIONS |
ASME PV CODE 9 : 2017 | BOILER AND PRESSURE VESSEL CODE - WELDING, BRAZING, AND FUSING QUALIFICATIONS - QUALIFICATION STANDARD FOR WELDING, BRAZING, AND FUSING PROCEDURES; WELDERS; BRAZERS; AND WELDING, BRAZING, AND FUSING OPERATORS |
ISO 3651-2:1998 | Determination of resistance to intergranular corrosion of stainless steels — Part 2: Ferritic,austenitic and ferritic-austenitic (duplex) stainless steels — Corrosion test in media containing sulfuric acid |
ASTM A 380/A380M : 2017 | Standard Practice for Cleaning, Descaling, and Passivation of Stainless Steel Parts, Equipment, and Systems |
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