• ASTM D 2369 : 2020

    Superseded A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

    Standard Test Method for Volatile Content of Coatings

    Available format(s):  Hardcopy, PDF

    Superseded date:  12-02-2024

    Language(s):  English

    Published date:  03-07-2020

    Publisher:  American Society for Testing and Materials

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    1.1This test method describes a procedure for the determination of the weight percent volatile content of solventborne and waterborne coatings. Test specimens are heated at 110 ± 5°C for 60 min.

    Note 1:The coatings used in these round-robin studies represented air-dried, air-dried oxidizing, heat-cured baking systems, and also included multicomponent paint systems.

    1.2Sixty minutes at 110 ± 5°C is a general purpose test method based on the precision obtained with both solventborne and waterborne coatings (see Section 9).

    1.3This test method is viable for coatings wherein one or more parts may, at ambient conditions, contain liquid coreactants that are volatile until a chemical reaction has occurred with another component of the multi-package system.

    Note 2:Committee D01 has run round-robin studies on volatiles of multicomponent paint systems. The only change in procedure is to premix the weighed components in the correct proportions and allow the specimens to stand at room temperature for 1 h prior to placing them into the oven.

    1.4Test Method D5095 for Determination of the Nonvolatile Content in Silanes, Siloxanes and Silane-Siloxane Blends Used in Masonry Water Repellent Treatments is the standard method for nonvolatile content of these types of materials.

    1.5Test Methods D5403 for Volatile Content of Radiation Curable Materials is the standard method for determining nonvolatile content of radiation curable coatings, inks and adhesives.

    1.6Test Method D6419 for Volatile Content of Sheet-Fed and Coldset Web Offset Printing Inks is the method of choice for these types of printing inks.

    1.7This test method may not be applicable to all types of coatings. Other procedures may be substituted with mutual agreement between the producer and the user.

    Note 3:If unusual decomposition or degradation of the specimen occurs during heating, the actual time and temperature used to cure the coating in practice may be substituted for the time and temperature specified in this test method, subject to mutual agreement between the producer and the user. The U.S. EPA Reference Method 24 specifies 110 ± 5°C for 1 h for coatings.

    Note 4:Practice D3960 for Determining Volatile Organic Compound (VOC) Content of Paints and Related Coatings describes procedures and calculations and provides guidance on selecting test methods to determine VOC content of solventborne and waterborne coatings.

    1.8The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

    1.9This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

    1.10This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

    General Product Information - (Show below) - (Hide below)

    Committee D 01
    Document Type Test Method
    Publisher American Society for Testing and Materials
    Status Superseded
    Superseded By
    Supersedes

    Standards Referenced By This Book - (Show below) - (Hide below)

    ASTM D 6093 : 1997 : R2022 Standard Test Method for Percent Volume Nonvolatile Matter in Clear or Pigmented Coatings Using a Helium Gas Pycnometer
    ASTM D 5325 : 2003 : R2021 Standard Test Method for Determination of Weight Percent Volatile Content of Water-Borne Aerosol Paints
    ASTM D 2698 : 2005 : R2022 Standard Test Method for Determination of the Pigment Content of Solvent-Reducible Paints by High-Speed Centrifuging
    ASTM F 940 : 1999 : R2019 : EDT 1 Standard Practice for Quality Control Receipt Inspection Procedures for Protective Coatings (Paint), Used in Marine Construction and Shipbuilding
    ASTM C 156 : 2020 Standard Test Method for Water Loss [from a Mortar Specimen] Through Liquid Membrane-Forming Curing Compounds for Concrete
    ASTM D 7805 : 2013 : R2021 Standard Terminology for Printing Ink Vehicles and Related Materials
    ASTM D 6511/D6511M : 2018 Standard Test Methods for Solvent Bearing Bituminous Compounds
    ASTM D 3794 : 2022 Standard Guide for Testing Coil Coatings
    ASTM D 5286 : 2020 Standard Test Methods for Determination of Transfer Efficiency Under General Production Conditions for Spray Application of Paints
    ASTM D 5327 : 1997 : R2021 : EDT 1 Standard Practice for Evaluating and Comparing Transfer Efficiency of Spray Applied Coatings Under General Laboratory Conditions
    ASTM D 5146 : 2010 : R2019 Standard Guide to Testing Solvent-Borne Architectural Coatings
    ASTM D 4143 : 2016 : R2022 Standard Guide for Testing Latex Vehicles
    ASTM D 6763 : 2016 : R2022 Standard Guide for Testing Exterior Wood Stains and Clear Water Repellents
    ASTM D 4302 : 2014 : R2021 Standard Specification for Artists’ Oil, Resin-Oil, and Alkyd Paints
    ASTM D 7270 : 2007 : R2021 Standard Guide for Environmental and Performance Verification of Factory-Applied Liquid Coatings
    ASTM D 4713 : 2012 : R2020 Standard Test Methods for Nonvolatile Content of Heatset and Liquid Printing Ink Systems
    ASTM D 2697 : 2022 Standard Test Method for Volume Nonvolatile Matter in Clear or Pigmented Coatings
    ASTM D 5324 : 2016 : R2022 Standard Guide for Testing Water-Borne Architectural Coatings
    ASTM D 5087 : 2002 : R2021 Standard Test Method for Determining Amount of Volatile Organic Compound (VOC) Released from Solventborne Automotive Coatings and Available for Removal in a VOC Control Device (Abatement)
    ASTM D 5201 : 2005 : REV A : R2020 Standard Practice for Calculating Formulation Physical Constants of Paints and Coatings
    ASTM D 7232 : 2006 : R2022 Standard Test Method for Rapid Determination of the Nonvolatile Content of Coatings by Loss in Weight
    ASTM D 4764 : 2001 : R2023 Standard Test Method for Determination by X-ray Fluorescence Spectroscopy of Titanium Dioxide Content in Paint
    ASTM D 2205 : 2020 Standard Guide for Selection of Tests for Traffic Paints
    ASTM D 3730 : 2017 : R2022 Standard Guide for Testing High-Performance Interior Architectural Wall Coatings
    ASTM D 3794 : 2018 Standard Guide for Testing Coil Coatings
    ASTM D 2832 : 1992 : R2016 Standard Guide for Determining Volatile and Nonvolatile Content of Paint and Related Coatings
    ASTM D 5201 : 2005 : REV A : R2014 Standard Practice for Calculating Formulation Physical Constants of Paints and Coatings
    ASTM D 6886 : 2018 Standard Test Method for Determination of the Weight Percent Individual Volatile Organic Compounds in Waterborne Air-Dry Coatings by Gas Chromatography
    ASTM D 7805 : 2013 Standard Terminology for Printing Ink Vehicles and Related Materials
    ASTM D 5009 : 2002 : R2017 Standard Test Method for Evaluating and Comparing Transfer Efficiency of Spray Applied Coatings Under Laboratory Conditions
    ASTM D 5403 : 1993 : R2013 Standard Test Methods for Volatile Content of Radiation Curable Materials
    ASTM D 2698 : 2005 : R2015 Standard Test Method for Determination of the Pigment Content of Solvent-Reducible Paints by High-Speed Centrifuging
    ASTM D 3960 : 2005 : R2018 Standard Practice for Determining Volatile Organic Compound (VOC) Content of Paints and Related Coatings
    ASTM D 7232 : 2006 : R2016 Standard Test Method for Rapid Determination of the Nonvolatile Content of Coatings by Loss in Weight
    ASTM D 7270 : 2007 : R2013 Standard Guide for Environmental and Performance Verification of Factory-Applied Liquid Coatings
    ASTM D 5324 : 2016 Standard Guide for Testing Water-Borne Architectural Coatings
    ASTM D 6419 : 2000 : R2017 Standard Test Method for Volatile Content of Sheet-Fed and Coldset Web Offset Printing Inks
    ASTM C 461 : 2017 Standard Test Methods for Mastics and Coatings Used With Thermal Insulation
    ASTM D 6093 : 1997 : R2016 Standard Test Method for Percent Volume Nonvolatile Matter in Clear or Pigmented Coatings Using a Helium Gas Pycnometer
    ASTM D 5327 : 1997 : R2013 Standard Practice for Evaluating and Comparing Transfer Efficiency of Spray Applied Coatings Under General Laboratory Conditions
    ASTM D 4302 : 2014 Standard Specification for Artists’ Oil, Resin-Oil, and Alkyd Paints
    ASTM D 3730 : 2017 Standard Guide for Testing High-Performance Interior Architectural Wall Coatings
    ASTM C 309 : 2019 Standard Specification for Liquid Membrane-Forming Compounds for Curing Concrete
    ASTM D 5066 : 1991 : R2017 Standard Test Method for Determination of the Transfer Efficiency Under Production Conditions for Spray Application of Automotive Paints—Weight Basis
    ASTM D 5087 : 2002 : R2014 Standard Test Method for Determining Amount of Volatile Organic Compound (VOC) Released from Solventborne Automotive Coatings and Available for Removal in a VOC Control Device (Abatement)
    ASTM D 2697 : 2003 : R2014 Standard Test Method for Volume Nonvolatile Matter in Clear or Pigmented Coatings
    ASTM D 2205 : 2015 Standard Guide for Selection of Tests for Traffic Paints
    ASTM D 5325 : 2003 : R2014 Standard Test Method for Determination of Weight Percent Volatile Content of Water-Borne Aerosol Paints
    ASTM D 4209 : 2007 : R2019 Standard Practice for Determining Volatile and Nonvolatile Content of Cellulosics, Emulsions, Resin Solutions, Shellac, and Varnishes
    ASTM D 3105 : 2017 Standard Index of Methods for Testing Elastomeric and Plastomeric Roofing and Waterproofing Materials
    ASTM D 3451 : 2006 : R2017 Standard Guide for Testing Coating Powders and Powder Coatings
    ASTM D 6763 : 2016 Standard Guide for Testing Exterior Wood Stains and Clear Water Repellents
    ASTM D 4764 : 2001 : R2016 Standard Test Method for Determination by X-ray Fluorescence Spectroscopy of Titanium Dioxide Content in Paint
    ASTM C 156 : 2017 Standard Test Method for Water Loss [from a Mortar Specimen] Through Liquid Membrane-Forming Curing Compounds for Concrete
    ASTM D 6266 : 2000 : REV A : R2017 Standard Test Method for Determining the Amount of Volatile Organic Compound (VOC) Released From Waterborne Automotive Coatings and Available for Removal in a VOC Control Device (Abatement)
    ASTM D 6583 : 2013 : R2019 Standard Test Method for Porosity of Paint Film by Mineral Oil Absorption
    ASTM D 6577 : 2015 : R2019 Standard Guide for Testing Industrial Protective Coatings
    ASTM D 4143 : 2016 Standard Guide for Testing Latex Vehicles
    AWWA C217:2023 Microcrystalline Wax and Petrolatum Tape Coating Systems for Steel Water Pipe and Fittings
    ASTM D 3105 : 2017 : R2024 Standard Index of Methods for Testing Elastomeric and Plastomeric Roofing and Waterproofing Materials
    ASTM D 6266 : 2000 : REV A : R2023 Standard Test Method for Determining the Amount of Volatile Organic Compound (VOC) Released From Waterborne Automotive Coatings and Available for Removal in a VOC Control Device (Abatement)
    ASTM D 5066 : 1991 : R2023 Standard Test Method for Determination of the Transfer Efficiency Under Production Conditions for Spray Application of Automotive Paints—Weight Basis
    ASTM C 461 : 2023 Standard Test Methods for Mastics and Coatings Used With Thermal Insulation
    ASTM D 5009 : 2002 : R2023 Standard Test Method for Evaluating and Comparing Transfer Efficiency of Spray Applied Coatings Under Laboratory Conditions

    Standards Referencing This Book - (Show below) - (Hide below)

    ASTM E 177 : 1990 : REV A : R1996 Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods
    ASTM E 691 : 2020 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
    ASTM E 691 : 2019 : EDT 1 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
    ASTM E 691 : 2023 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
    ASTM D 3960 : 1998 Standard Practice for Determining Volatile Organic Compound (VOC) Content of Paints and Related Coatings
    ASTM D 5095 : 1991 : R2013 Standard Test Method for Determination of the Nonvolatile Content in Silanes, Siloxanes and Silane-Siloxane Blends Used in Masonry Water Repellent Treatments
    ASTM E 691 : 2022 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
    ASTM D 5403 : 1993 : R1998 Standard Test Methods for Volatile Content of Radiation Curable Materials
    ASTM E 691 : 2009 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
    ASTM D 5403 : 1993 : R2021 Standard Test Methods for Volatile Content of Radiation Curable Materials
    ASTM D 3925 : 2002 : R2022 Standard Practice for Sampling Liquid Paints and Related Pigmented Coatings
    ASTM E 691 : 2021 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
    ASTM D 5095 : 1991 : R2022 Standard Test Method for Determination of the Nonvolatile Content in Silanes, Siloxanes and Silane-Siloxane Blends Used in Masonry Water Repellent Treatments
    ASTM D 6419 : 2000 : R2023 Standard Test Method for Volatile Content of Sheet-Fed and Coldset Web Offset Printing Inks
    ASTM D 3925 : 2002 : R2015 Standard Practice for Sampling Liquid Paints and Related Pigmented Coatings
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