• ASTM D 524 : 2015

    Superseded A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

    Standard Test Method for Ramsbottom Carbon Residue of Petroleum Products

    Available format(s):  Hardcopy, PDF

    Superseded date:  16-12-2019

    Language(s):  English

    Published date:  10-06-2015

    Publisher:  American Society for Testing and Materials

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    Abstract - (Show below) - (Hide below)

    This test method covers the determination of the amount of carbon residue (Note 1) left after evaporation and pyrolysis of an oil, and it is intended to provide some indication of relative coke-forming propensity.

    Scope - (Show below) - (Hide below)

    1.1This test method covers the determination of the amount of carbon residue (Note 1) left after evaporation and pyrolysis of an oil, and it is intended to provide some indication of relative coke-forming propensity. This test method is generally applicable to relatively nonvolatile petroleum products which partially decompose on distillation at atmospheric pressure. This test method also covers the determination of carbon residue on 10 % (V/V) distillation residues (see Section 10). Petroleum products containing ash-forming constituents as determined by Test Method D482, will have an erroneously high carbon residue, depending upon the amount of ash formed (Notes 2 and 3).

    Note 1:The term carbon residue is used throughout this test method to designate the carbonaceous residue formed during evaporation and pyrolysis of a petroleum product. The residue is not composed entirely of carbon, but is a coke which can be further changed by pyrolysis. The term carbon residue is continued in this test method only in deference to its wide common usage.

    Note 2:Values obtained by this test method are not numerically the same as those obtained by Test Method D189, or Test Method D4530. Approximate correlations have been derived (see Fig. X2.1) but need not apply to all materials which can be tested because the carbon residue test is applicable to a wide variety of petroleum products. The Ramsbottom Carbon Residue test method is limited to those samples that are mobile below 90 °C.

    Note 3:In diesel fuel, the presence of alkyl nitrates such as amyl nitrate, hexyl nitrate, or octyl nitrate, causes a higher carbon residue value than observed in untreated fuel, which can lead to erroneous conclusions as to the coke-forming propensity of the fuel. The presence of alkyl nitrate in the fuel can be detected by Test Method D4046.

    Note 4:The test procedure in Section 10 is being modified to allow the use of a 100 mL volume automated distillation apparatus. No precision data is available for the procedure at this time, but a round robin is being planned to develop precision data. The 250 mL volume bulb distillation method described in Section 10 for determining carbon residue on a 10 % distillation residue is considered the referee test.

    1.2The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

    1.3WARNING—Mercury has been designated by many regulatory agencies as a hazardous material that can cause central nervous system, kidney and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury containing products. See the applicable product Material Safety Data Sheet (MSDS) for details and EPA’s website—http://www.epa.gov/mercury/faq.htm—for additional information. Users should be aware that selling mercury and/or mercury containing products into your state or country may be prohibited by law.

    1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

    General Product Information - (Show below) - (Hide below)

    Committee D 02
    Document Type Test Method
    Publisher American Society for Testing and Materials
    Status Superseded
    Superseded By
    Supersedes

    Standards Referenced By This Book - (Show below) - (Hide below)

    ASTM D 396 : 2021 Standard Specification for Fuel Oils
    ASTM D 7665 : 2022 Standard Guide for Evaluation of Biodegradable Heat Transfer Fluids
    ASTM D 7467 : 2020 : REV A Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
    ASTM D 5967 : 2021 Standard Test Method for Evaluation of Diesel Engine Oils in T-8 Diesel Engine
    ASTM D 6074 : 2015 : R2022 Standard Guide for Characterizing Hydrocarbon Lubricant Base Oils
    ASTM D 7583 : 2016 Standard Test Method for John Deere Coolant Cavitation Test
    ASTM D 189 : 2006 : R2019 Standard Test Method for Conradson Carbon Residue of Petroleum Products
    ASTM D 5966 : 2022 Standard Test Method for Evaluation of Engine Oils for Roller Follower Wear in Light-Duty Diesel Engine
    ASTM D 7549 : 2021 Standard Test Method for Evaluation of Heavy-Duty Engine Oils under High Output Conditions—Caterpillar C13 Test Procedure
    ASTM D 6681 : 2017 Standard Test Method for Evaluation of Engine Oils in a High Speed, Single-Cylinder Diesel Engine—Caterpillar 1P Test Procedure
    ASTM D 7468 : 2022 Standard Test Method for Cummins ISM Test
    ASTM D 7484 : 2023 Standard Test Method for Evaluation of Automotive Engine Oils for Valve-Train Wear Performance in Cummins ISB Medium-Duty Diesel Engine
    ASTM D 6923 : 2018 Standard Test Method for Evaluation of Engine Oils in a High Speed, Single-Cylinder Diesel Engine—Caterpillar 1R Test Procedure
    ASTM D 975 : 2022 : REV A Standard Specification for Diesel Fuel
    ASTM D 6750 : 2019 : EDT 1 Standard Test Methods for Evaluation of Engine Oils in a High-Speed, Single-Cylinder Diesel Engine—1K Procedure (0.4 % Fuel Sulfur) and 1N Procedure (0.04 % Fuel Sulfur)
    ASTM D 6710 : 2021 Standard Guide for Evaluation of Hydrocarbon-Based Quench Oil
    ASTM D 8048 : 2021 : REV A : EDT 1 Standard Test Method for Evaluation of Diesel Engine Oils in T-13 Diesel Engine
    ASTM D 7156 : 2019 Standard Test Method for Evaluation of Diesel Engine Oils in the T-11 Exhaust Gas Recirculation Diesel Engine
    ASTM D 7422 : 2022 Standard Test Method for Evaluation of Diesel Engine Oils in T-12 Exhaust Gas Recirculation Diesel Engine
    ASTM D 8074 : 2022 Standard Test Method for Evaluation of Diesel Engine Oils in DD13 Diesel Engine
    ASTM D 5372 : 2020 Standard Guide for Evaluation of Hydrocarbon Heat Transfer Fluids
    ASTM F 715 : 2007 : R2018 Standard Test Methods for Coated Fabrics Used for Oil Spill Control and Storage
    ASTM D 6618 : 2016 Standard Test Method for Evaluation of Engine Oils in Diesel Four-Stroke Cycle Supercharged 1M-PC Single Cylinder Oil Test Engine

    Standards Referencing This Book - (Show below) - (Hide below)

    ASTM D 4175 : 2014 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4057 : 2019 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 4175 : 2009 : REV A : EDT 1 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2008 : REV B : EDT 1 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4046 : 1991 : R2000 : EDT 1 Standard Test Method for Alkyl Nitrate in Diesel Fuels by Spectrophotometry
    ASTM D 4175 : 2005 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2005 : EDT 2 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4530 : 2003 Standard Test Method for Determination of Carbon Residue (Micro Method)
    ASTM D 4177 : 2016 : EDT 1 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 4175 : 2015 : REV C Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2017 : REV A : EDT 1 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 4177 : 1995 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 4175 : 2008 : REV A Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4057 : 2012 : R2018 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 4175 : 2017 : REV B Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 4175 : 2009 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2009 : REV A : EDT 4 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2009 : REV A : EDT 3 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4057 : 1981 : EDT 2 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 4175 : 2018 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 4046 : 2014 : R2019 Standard Test Method for Alkyl Nitrate in Diesel Fuels by Spectrophotometry (Withdrawn 2019)
    ASTM D 4175 : 2001 : EDT 1 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2001 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2005 : EDT 1 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2002 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4057 : 2006 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 4175 : 2015 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2002 : REV A : EDT 2 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4177 : 2015 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 4057 : 2012 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 4046 : 2014 Standard Test Method for Alkyl Nitrate in Diesel Fuels by Spectrophotometry
    ASTM D 4530 : 2000 Standard Test Method for Determination of Carbon Residue (Micro Method)
    ASTM D 4175 : 2009 : REV A : EDT 5 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2016 : REV C Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 4175 : 2015 : REV B Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2015 : REV A Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2009 : REV A Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2016 : REV B Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 4177 : 1995 : R2010 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 4175 : 2002 : REV A : EDT 1 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2008 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2002 : REV A Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4177 : 1995 : R2000 Standard Practice for Automatic Sampling of Peroleum and Petroleum Products
    ASTM D 4175 : 2000 : EDT 1 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4175 : 2016 : REV A Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 4046 : 1991 : R2005 Standard Test Method for Alkyl Nitrate in Diesel Fuels by Spectrophotometry
    ASTM D 4175 : 2017 : REV A Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 4175 : 2009 : REV A : EDT 2 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4530 : 2007 Standard Test Method for Determination of Carbon Residue (Micro Method)
    ASTM D 4177 : 2016 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 4177 : 1995 : R2005 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 4175 : 2018 : EDT 1 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 4175 : 2016 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 4530 : 2015 Standard Test Method for Determination of Carbon Residue (Micro Method)
    ASTM D 4530 : 2006 : EDT 1 Standard Test Method for Determination of Carbon Residue (Micro Method)
    ASTM D 4530 : 2006 Standard Test Method for Determination of Carbon Residue (Micro Method)
    ASTM D 4057 : 1995 : R2000 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 4175 : 2017 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 4175 : 2019 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants
    ASTM D 4177 : 2015 : REV A Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
    ASTM D 4057 : 2006 : R2011 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
    ASTM D 4530 : 2011 Standard Test Method for Determination of Carbon Residue (Micro Method)
    ASTM D 4175 : 2015 : REV B : EDT 1 Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
    ASTM D 4046 : 2011 Standard Test Method for Alkyl Nitrate in Diesel Fuels by Spectrophotometry
    ASTM D 4175 : 2008 : REV B Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants
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