ASTM D 524 : 2015 : REDLINE
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
Standard Test Method for Ramsbottom Carbon Residue of Petroleum Products
10-06-2015
English
10-06-2015
CONTAINED IN VOL. 05.01, 2015 Describes the amount of carbon residue left after evaporation and pyrolysis of an oil, and it is intended to provide some indication of relative coke-forming propensity.
Committee |
D 02
|
DevelopmentNote |
Also Numbered as IP 14 (12/2001)
|
DocumentType |
Redline
|
Pages |
12
|
PublisherName |
American Society for Testing and Materials
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Status |
Superseded
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1.1This test method covers the determination of the amount of carbon residue (Note 1) left after evaporation and pyrolysis of an oil, and it is intended to provide some indication of relative coke-forming propensity. This test method is generally applicable to relatively nonvolatile petroleum products which partially decompose on distillation at atmospheric pressure. This test method also covers the determination of carbon residue on 10 % (V/V) distillation residues (see Section 10). Petroleum products containing ash-forming constituents as determined by Test Method D482, will have an erroneously high carbon residue, depending upon the amount of ash formed (Notes 2 and 3).
Note 1:The term carbon residue is used throughout this test method to designate the carbonaceous residue formed during evaporation and pyrolysis of a petroleum product. The residue is not composed entirely of carbon, but is a coke which can be further changed by pyrolysis. The term carbon residue is continued in this test method only in deference to its wide common usage.
Note 2:Values obtained by this test method are not numerically the same as those obtained by Test Method D189, or Test Method D4530. Approximate correlations have been derived (see Fig. X2.1) but need not apply to all materials which can be tested because the carbon residue test is applicable to a wide variety of petroleum products. The Ramsbottom Carbon Residue test method is limited to those samples that are mobile below 90 °C.
Note 3:In diesel fuel, the presence of alkyl nitrates such as amyl nitrate, hexyl nitrate, or octyl nitrate, causes a higher carbon residue value than observed in untreated fuel, which can lead to erroneous conclusions as to the coke-forming propensity of the fuel. The presence of alkyl nitrate in the fuel can be detected by Test Method D4046.
Note 4:The test procedure in Section 10 is being modified to allow the use of a 100 mL volume automated distillation apparatus. No precision data is available for the procedure at this time, but a round robin is being planned to develop precision data. The 250 mL volume bulb distillation method described in Section 10 for determining carbon residue on a 10 % distillation residue is considered the referee test.
1.2The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3WARNING—Mercury has been designated by many regulatory agencies as a hazardous material that can cause central nervous system, kidney and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury containing products. See the applicable product Material Safety Data Sheet (MSDS) for details and EPA’s website—http://www.epa.gov/mercury/faq.htm—for additional information. Users should be aware that selling mercury and/or mercury containing products into your state or country may be prohibited by law.
1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
Standards | Relationship |
BS 4451:1980 | Identical |
UNE 51124:1985 | Identical |
MIL-L-46152 Revision E:1990 | LUBRICATING OIL, INTERNAL COMBUSTION ENGINE, ADMINISTRATIVE SERVICE, METRIC |
MIL L 21260 : D | LUBRICATING OIL, INTERNAL COMBUSTION ENGINE, PRESERVATIVE AND BREAK IN |
MIL-PRF-46167 Revision D:2005 | LUBRICATING OIL, INTERNAL COMBUSTION ENGINE, ARCTIC |
MIL-DTL-16884 Revision P:2017 | FUEL, NAVAL DISTILLATE |
ASTM D 8048 : 2017-05 | TEST METHOD FOR EVALUATION OF DIESEL ENGINE OILS IN T-13 DIESEL ENGINE |
ASTM D 6985 : 2004 | Standard Specification for Middle Distillate Fuel Oil-Military Marine Applications |
ASTM D 189 : 2006 : R2014 | Standard Test Method for Conradson Carbon Residue of Petroleum Products |
ASTM D 6975 : 2004 : R2010 | Standard Test Method for Cummins M11 EGR Test (Withdrawn 2019) |
ASTM D 7468 : 2016 : REDLINE | TEST METHOD FOR CUMMINS ISM TEST |
A-A-52306 Revision A:1995 | LUBRICATING OIL, HEAVY-DUTY DIESEL ENGINE |
MIL L 83767 : B | LUBRICATING OIL, VACUUM PUMP, MECHANICAL |
MIL F 46162 : D | FUEL, DIESEL, REFEREE GRADE |
MIL F 12070 : D | FOG OIL |
ASTM D 6838 : 2004 | Standard Test Method for Cummins M11 High Soot Test |
MIL-PRF-53074 Revision A:1998 | LUBRICATING OIL, STEAM-CYLINDER, MINERAL |
SAE J 2359 : 1998 | LUBRICATING OIL, INTERNAL COMBUSTION ENGINE, MILITARY COMBAT/TACTICAL SERVICE |
ASTM F 715 : 2007 | Standard Test Methods for Coated Fabrics Used for Oil Spill Control and Storage |
ASTM D 5967 : 2017 : REDLINE | Standard Test Method for Evaluation of Diesel Engine Oils in T-8 Diesel Engine |
ASTM D 5290 : 1991 | Standard Test Method for Measurement of Oil Consumption, Piston Deposits and Wear in a Heavy-Duty High Speed Diesel Engine-NTC-400 Procedure (Withdrawn 1997) |
ASTM D 6074 : 2015 : REDLINE | Standard Guide for Characterizing Hydrocarbon Lubricant Base Oils |
ASTM D 6985 : 2004 : REV A | Standard Specification for Middle Distillate Fuel Oil-Military Marine Applications (Withdrawn 2010) |
ASTM D 6838 : 2004 : R2010 | Standard Test Method for Cummins M11 High Soot Test (Withdrawn 2019) |
ASTM D 6975 : 2004 | Standard Test Method for Cummins M11 EGR Test |
ASTM D 7583 : 2016 : REDLINE | Standard Test Method for John Deere Coolant Cavitation Test |
ASTM D 5372 : 2017 : REDLINE | Standard Guide for Evaluation of Hydrocarbon Heat Transfer Fluids |
VV-F-800 Revision E:1987 | FUEL OIL, DIESEL |
MIL-PRF-21260 Revision E:1998 | LUBRICATING OIL, INTERNAL COMBUSTION ENGINE, PRESERVATIVE BREAK-IN |
MIL-STD-3004 Revision D:2014 | QUALITY ASSURANCE/SURVEILLANCE FOR FUELS, LUBRICANTS AND RELATED PRODUCTS |
ASTM D 189 : 2006 : EDT 1 | Standard Test Method for Conradson Carbon Residue of Petroleum Products |
ASTM D 189 : 2006 : R2010 : EDT 1 | Standard Test Method for Conradson Carbon Residue of Petroleum Products |
ASTM D 6894 : 2013 : REDLINE | Standard Test Method for Evaluation of Aeration Resistance of Engine Oils in Direct-Injected Turbocharged Automotive Diesel Engine |
MIL F 16884 : J | FUEL, NAVAL DISTILLATE |
SAE J 313 : 2017 | DIESEL FUELS |
SAE J 2361 : 1998 | LUBRICATING OIL, INTERNAL COMBUSTION ENGINE, PRESERVATION BREAK-IN |
ASTM D 7665 : 2017 : REDLINE | Standard Guide for Evaluation of Biodegradable Heat Transfer Fluids |
MIL PRF 16884 : K | FUEL, NAVAL DISTILLATE |
ASTM D 2069 : 1991 : R1998 | Standard Specification for Marine Fuels (Withdrawn 2003) |
FED-STD-791 Revision D:2007 | TESTING METHOD OF LUBRICANTS, LIQUID FUELS, AND RELATED PRODUCTS |
ASTM D 6710 : 2017 : REDLINE | Standard Guide for Evaluation of Hydrocarbon-Based Quench Oil |
MIL L 2105 : D | LUBRICATING OIL, GEAR, MULTI PURPOSE |
MIL-PRF-17672 Revision E:2010 | Hydraulic Fluid, Petroleum, Inhibited |
DEFSTAN 91-43/2(1993) : 1993 | LUBRICATING OIL, ENGINE: GRADE 50 NATO CODE NO. 0-182 JOINT SERVICE DESIGNATION: OMD-330 |
ASTM D 7156 : 2017 : REDLINE | Standard Test Method for Evaluation of Diesel Engine Oils in the T-11 Exhaust Gas Recirculation Diesel Engine |
ASTM D 189 : 2006 : EDT 2 | Standard Test Method for Conradson Carbon Residue of Petroleum Products |
MIL-DTL-83767 Revision C:2007 | Lubricating Oil, Vacuum Pump, Mechanical |
ASTM D 6618 : 2016 : REDLINE | Standard Test Method for Evaluation of Engine Oils in Diesel Four-Stroke Cycle Supercharged 1M-PC Single Cylinder Oil Test Engine |
MIL L 2104 : F | LUBRICATING OIL, INTERNAL COMBUSTION ENGINE, COMBAT TACTICAL SERVICE |
MIL-DTL-46162 Revision E:2002 | FUEL, DIESEL, REFEREE GRADE |
MIL-PRF-12070 Revision E:1998 | FOG OIL |
ASTM F 715 : 2007 : R2012 | Standard Test Methods for Coated Fabrics Used for Oil Spill Control and Storage |
SAE J357_201601 | PHYSICAL AND CHEMICAL PROPERTIES OF ENGINE OILS |
ASTM D 7467 : 2017-03 | SPECIFICATION FOR DIESEL FUEL OIL, BIODIESEL BLEND (B6 TO B20) |
ASTM D 6483 : 2004 | Standard Test Method for Evaluation of Diesel Engine Oils in T-9 Diesel Engine (Withdrawn 2009) |
ASTM D 8074 : 2016 | Standard Test Method for Evaluation of Diesel Engine Oils in DD13 Diesel Engine |
ASTM D 6681 : 2017 : REDLINE | Standard Test Method for Evaluation of Engine Oils in a High Speed, Single-Cylinder Diesel Engine—Caterpillar 1P Test Procedure |
ASTM E 1 : 2014 : REDLINE | Standard Specification for ASTM Liquid-in-Glass Thermometers |
ASTM D 189 : 2006 : EDT 1 | Standard Test Method for Conradson Carbon Residue of Petroleum Products |
ASTM D 86 : 2017-06 | TEST METHOD FOR DISTILLATION OF PETROLEUM PRODUCTS AND LIQUID FUELS AT ATMOSPHERIC PRESSURE |
ASTM D 4530 : 2015 : REDLINE | Standard Test Method for Determination of Carbon Residue (Micro Method) |
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