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ASTM D 524 : 2015 : REDLINE

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Standard Test Method for Ramsbottom Carbon Residue of Petroleum Products

Available format(s)

PDF

Superseded date

10-06-2015

Language(s)

English

Published date

10-06-2015

€67.30
Excluding VAT

CONTAINED IN VOL. 05.01, 2015 Describes the amount of carbon residue left after evaporation and pyrolysis of an oil, and it is intended to provide some indication of relative coke-forming propensity.

Committee
D 02
DevelopmentNote
Also Numbered as IP 14 (12/2001)
DocumentType
Redline
Pages
12
PublisherName
American Society for Testing and Materials
Status
Superseded

1.1This test method covers the determination of the amount of carbon residue (Note 1) left after evaporation and pyrolysis of an oil, and it is intended to provide some indication of relative coke-forming propensity. This test method is generally applicable to relatively nonvolatile petroleum products which partially decompose on distillation at atmospheric pressure. This test method also covers the determination of carbon residue on 10 % (V/V) distillation residues (see Section 10). Petroleum products containing ash-forming constituents as determined by Test Method D482, will have an erroneously high carbon residue, depending upon the amount of ash formed (Notes 2 and 3).

Note 1:The term carbon residue is used throughout this test method to designate the carbonaceous residue formed during evaporation and pyrolysis of a petroleum product. The residue is not composed entirely of carbon, but is a coke which can be further changed by pyrolysis. The term carbon residue is continued in this test method only in deference to its wide common usage.

Note 2:Values obtained by this test method are not numerically the same as those obtained by Test Method D189, or Test Method D4530. Approximate correlations have been derived (see Fig. X2.1) but need not apply to all materials which can be tested because the carbon residue test is applicable to a wide variety of petroleum products. The Ramsbottom Carbon Residue test method is limited to those samples that are mobile below 90 °C.

Note 3:In diesel fuel, the presence of alkyl nitrates such as amyl nitrate, hexyl nitrate, or octyl nitrate, causes a higher carbon residue value than observed in untreated fuel, which can lead to erroneous conclusions as to the coke-forming propensity of the fuel. The presence of alkyl nitrate in the fuel can be detected by Test Method D4046.

Note 4:The test procedure in Section 10 is being modified to allow the use of a 100 mL volume automated distillation apparatus. No precision data is available for the procedure at this time, but a round robin is being planned to develop precision data. The 250 mL volume bulb distillation method described in Section 10 for determining carbon residue on a 10 % distillation residue is considered the referee test.

1.2The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.3WARNING—Mercury has been designated by many regulatory agencies as a hazardous material that can cause central nervous system, kidney and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury containing products. See the applicable product Material Safety Data Sheet (MSDS) for details and EPA’s website—http://www.epa.gov/mercury/faq.htm—for additional information. Users should be aware that selling mercury and/or mercury containing products into your state or country may be prohibited by law.

1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Standards Relationship
BS 4451:1980 Identical
UNE 51124:1985 Identical

MIL-L-46152 Revision E:1990 LUBRICATING OIL, INTERNAL COMBUSTION ENGINE, ADMINISTRATIVE SERVICE, METRIC
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ASTM D 7468 : 2016 : REDLINE TEST METHOD FOR CUMMINS ISM TEST
A-A-52306 Revision A:1995 LUBRICATING OIL, HEAVY-DUTY DIESEL ENGINE
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MIL-PRF-53074 Revision A:1998 LUBRICATING OIL, STEAM-CYLINDER, MINERAL
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ASTM D 6074 : 2015 : REDLINE Standard Guide for Characterizing Hydrocarbon Lubricant Base Oils
ASTM D 6985 : 2004 : REV A Standard Specification for Middle Distillate Fuel Oil-Military Marine Applications (Withdrawn 2010)
ASTM D 6838 : 2004 : R2010 Standard Test Method for Cummins M11 High Soot Test (Withdrawn 2019)
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ASTM D 7583 : 2016 : REDLINE Standard Test Method for John Deere Coolant Cavitation Test
ASTM D 5372 : 2017 : REDLINE Standard Guide for Evaluation of Hydrocarbon Heat Transfer Fluids
VV-F-800 Revision E:1987 FUEL OIL, DIESEL
MIL-PRF-21260 Revision E:1998 LUBRICATING OIL, INTERNAL COMBUSTION ENGINE, PRESERVATIVE BREAK-IN
MIL-STD-3004 Revision D:2014 QUALITY ASSURANCE/SURVEILLANCE FOR FUELS, LUBRICANTS AND RELATED PRODUCTS
ASTM D 189 : 2006 : EDT 1 Standard Test Method for Conradson Carbon Residue of Petroleum Products
ASTM D 189 : 2006 : R2010 : EDT 1 Standard Test Method for Conradson Carbon Residue of Petroleum Products
ASTM D 6894 : 2013 : REDLINE Standard Test Method for Evaluation of Aeration Resistance of Engine Oils in Direct-Injected Turbocharged Automotive Diesel Engine
MIL F 16884 : J FUEL, NAVAL DISTILLATE
SAE J 313 : 2017 DIESEL FUELS
SAE J 2361 : 1998 LUBRICATING OIL, INTERNAL COMBUSTION ENGINE, PRESERVATION BREAK-IN
ASTM D 7665 : 2017 : REDLINE Standard Guide for Evaluation of Biodegradable Heat Transfer Fluids
MIL PRF 16884 : K FUEL, NAVAL DISTILLATE
ASTM D 2069 : 1991 : R1998 Standard Specification for Marine Fuels (Withdrawn 2003)
FED-STD-791 Revision D:2007 TESTING METHOD OF LUBRICANTS, LIQUID FUELS, AND RELATED PRODUCTS
ASTM D 6710 : 2017 : REDLINE Standard Guide for Evaluation of Hydrocarbon-Based Quench Oil
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DEFSTAN 91-43/2(1993) : 1993 LUBRICATING OIL, ENGINE: GRADE 50 NATO CODE NO. 0-182 JOINT SERVICE DESIGNATION: OMD-330
ASTM D 7156 : 2017 : REDLINE Standard Test Method for Evaluation of Diesel Engine Oils in the T-11 Exhaust Gas Recirculation Diesel Engine
ASTM D 189 : 2006 : EDT 2 Standard Test Method for Conradson Carbon Residue of Petroleum Products
MIL-DTL-83767 Revision C:2007 Lubricating Oil, Vacuum Pump, Mechanical
ASTM D 6618 : 2016 : REDLINE Standard Test Method for Evaluation of Engine Oils in Diesel Four-Stroke Cycle Supercharged 1M-PC Single Cylinder Oil Test Engine
MIL L 2104 : F LUBRICATING OIL, INTERNAL COMBUSTION ENGINE, COMBAT TACTICAL SERVICE
MIL-DTL-46162 Revision E:2002 FUEL, DIESEL, REFEREE GRADE
MIL-PRF-12070 Revision E:1998 FOG OIL
ASTM F 715 : 2007 : R2012 Standard Test Methods for Coated Fabrics Used for Oil Spill Control and Storage
SAE J357_201601 PHYSICAL AND CHEMICAL PROPERTIES OF ENGINE OILS
ASTM D 7467 : 2017-03 SPECIFICATION FOR DIESEL FUEL OIL, BIODIESEL BLEND (B6 TO B20)
ASTM D 6483 : 2004 Standard Test Method for Evaluation of Diesel Engine Oils in T-9 Diesel Engine (Withdrawn 2009)
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ASTM D 6681 : 2017 : REDLINE Standard Test Method for Evaluation of Engine Oils in a High Speed, Single-Cylinder Diesel Engine—Caterpillar 1P Test Procedure

ASTM E 1 : 2014 : REDLINE Standard Specification for ASTM Liquid-in-Glass Thermometers
ASTM D 189 : 2006 : EDT 1 Standard Test Method for Conradson Carbon Residue of Petroleum Products
ASTM D 86 : 2017-06 TEST METHOD FOR DISTILLATION OF PETROLEUM PRODUCTS AND LIQUID FUELS AT ATMOSPHERIC PRESSURE
ASTM D 4530 : 2015 : REDLINE Standard Test Method for Determination of Carbon Residue (Micro Method)

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