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ASTM D 7578 : 2020

Current

Current

The latest, up-to-date edition.

Standard Guide for Calibration Requirements for Elemental Analysis of Petroleum Products and Lubricants

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

01-05-2020

€61.92
Excluding VAT

Committee
D 02
DocumentType
Guide
Pages
13
PublisherName
American Society for Testing and Materials
Status
Current
Supersedes

1.1This guide covers different ways by which the test methods used for elemental analysis of petroleum product and lubricant samples are calibrated before the sample analysis.

1.2Uniform practice for test method calibration is beneficial in standardizing the procedures, and obtaining consistent results across different laboratories.

1.3This guide includes only the basic steps for generally encountered instrument types. Anything out of the ordinary may require special procedures. See individual test methods for instructions to handle such situations.

1.4This guide is not a substitute for a thorough understanding of the actual test method to be used, caveats it contains, and additional instrument preparation that may be required.

1.5The user should not expand the scope of the test methods to materials or concentrations outside the scope of the test methods being used.

1.6This guide should also be applicable to sample preparation of non-petroleum based bio-fuels for elemental analysis. Work is underway on these aspects in Subcommittee D02.03. As more information becomes available, it will be added to this standard.

1.7The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.8This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.9This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM D 8056 : 2018 Standard Guide for Elemental Analysis of Crude Oil
ASTM D 7961 : 2017 Standard Practice for Calibrating U-tube Density Cells over Large Ranges of Temperature and Pressure

ASTM D 5863 : 2022 Standard Test Methods for Determination of Nickel, Vanadium, Iron, and Sodium in Crude Oils and Residual Fuels by Flame Atomic Absorption Spectrometry
ASTM D 129 : 2018 Standard Test Method for Sulfur in Petroleum Products (General High Pressure Decomposition Device Method) (Withdrawn 2023)
ASTM D 5291 : 2021 Standard Test Methods for Instrumental Determination of Carbon, Hydrogen, and Nitrogen in Petroleum Products and Lubricants
ASTM D 4929 : 2024 Standard Test Method for Determination of Organic Chloride Content in Crude Oil
ASTM D 6792 : 2021 : REV A Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 3341 : 2016 Standard Test Method for Lead in Gasoline—Iodine Monochloride Method (Withdrawn 2022)
ASTM D 874 : 2013 : REV A : R2018 Standard Test Method for Sulfated Ash from Lubricating Oils and Additives
ASTM D 6667 : 2021 Standard Test Method for Determination of Total Volatile Sulfur in Gaseous Hydrocarbons and Liquefied Petroleum Gases by Ultraviolet Fluorescence
ASTM D 7328 : 2022 Standard Test Method for Determination of Existent and Potential Inorganic Sulfate and Total Inorganic Chloride in Fuel Ethanol by Ion Chromatography Using Aqueous Sample Injection
ASTM D 5762 : 2024 Standard Test Method for Nitrogen in Liquid Hydrocarbons, Petroleum and Petroleum Products by Boat-Inlet Chemiluminescence
ASTM D 3120 : 1996 Standard Test Method for Trace Quantities of Sulfur in Light Liquid Petroleum Hydrocarbons by Oxidative Microcoulometry
ASTM D 7757 : 2022 Standard Test Method for Silicon in Gasoline and Related Products by Monochromatic Wavelength Dispersive X-ray Fluorescence Spectrometry
ASTM D 5056 : 2017 Standard Test Method for Trace Metals in Petroleum Coke by Atomic Absorption
ASTM D 7111 : 2016 Standard Test Method for Determination of Trace Elements in Middle Distillate Fuels by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
ASTM D 7303 : 2017 Standard Test Method for Determination of Metals in Lubricating Greases by Inductively Coupled Plasma Atomic Emission Spectrometry
ASTM D 5800 : 2018 : REV A Standard Test Method for Evaporation Loss of Lubricating Oils by the Noack Method
ASTM D 7220 : 2012 : R2017 Standard Test Method for Sulfur in Automotive, Heating, and Jet Fuels by Monochromatic Energy Dispersive X-ray Fluorescence Spectrometry
ASTM D 6728 : 2016 : R2021 Standard Test Method for Determination of Contaminants in Gas Turbine and Diesel Engine Fuel by Rotating Disc Electrode Atomic Emission Spectrometry
ASTM D 1018 : 2011 : R2016 Standard Test Method for Hydrogen In Petroleum Fractions (Withdrawn 2021)
ASTM D 482 : 2013 Standard Test Method for Ash from Petroleum Products
ASTM D 892 : 2018 Standard Test Method for Foaming Characteristics of Lubricating Oils
ASTM D 5184 : 2012 : R2017 Standard Test Methods for Determination of Aluminum and Silicon in Fuel Oils by Ashing, Fusion, Inductively Coupled Plasma Atomic Emission Spectrometry, and Atomic Absorption Spectrometry
ASTM D 4628 : 2023 Standard Test Method for Analysis of Barium, Calcium, Magnesium, and Zinc in Unused Lubricating Oils by Atomic Absorption Spectrometry
ASTM D 4929 : 2019 : REV A Standard Test Method for Determination of Organic Chloride Content in Crude Oil
ASTM D 3605 : 2022 Standard Test Method for Trace Metals in Gas Turbine Fuels by Atomic Absorption and Flame Emission Spectroscopy
ASTM D 808 : 2016 Standard Test Method for Chlorine in New and Used Petroleum Products (High Pressure Decomposition Device Method) (Withdrawn 2021)
ASTM D 4929 : 2022 Standard Test Method for Determination of Organic Chloride Content in Crude Oil
ASTM D 5184 : 2022 Standard Test Methods for Determination of Aluminum and Silicon in Fuel Oils by Ashing, Fusion, Inductively Coupled Plasma Atomic Emission Spectrometry, and Atomic Absorption Spectrometry
ASTM D 3230 : 2013 : R2018 Standard Test Method for Salts in Crude Oil (Electrometric Method)
ASTM D 7041 : 2016 : R2021 Standard Test Method for Determination of Total Sulfur in Liquid Hydrocarbons and Hydrocarbon-Oxygenate Blends by Gas Chromatography with Flame Photometric Detection
ASTM D 6443 : 2024 Standard Test Method for Determination of Calcium, Chlorine, Copper, Magnesium, Phosphorus, Sulfur, and Zinc in Unused Lubricating Oils and Additives by Wavelength Dispersive X-ray Fluorescence Spectrometry (Mathematical Correction Procedure)
ASTM D 3605 : 2017 Standard Test Method for Trace Metals in Gas Turbine Fuels by Atomic Absorption and Flame Emission Spectroscopy
ASTM D 5622 : 2017 Standard Test Methods for Determination of Total Oxygen in Gasoline and Methanol Fuels by Reductive Pyrolysis
ASTM D 445 : 2021 : EDT 2 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM D 3348 : 2012 : R2017 Standard Test Method for Rapid Field Test for Trace Lead in Unleaded Gasoline (Colorimetric Method) (Withdrawn 2022)
ASTM D 7328 : 2023 Standard Test Method for Determination of Existent and Potential Inorganic Sulfate and Total Inorganic Chloride in Fuel Ethanol by Ion Chromatography Using Aqueous Sample Injection
ASTM D 3231 : 2024 Standard Test Method for Phosphorus in Gasoline
ASTM D 6792 : 2021 : REV B Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 6792 : 2023 : REV C Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 5800 : 2019 Standard Test Method for Evaporation Loss of Lubricating Oils by the Noack Method
ASTM D 445 : 2017 : REV A Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM D 6334 : 2012 : R2017 : EDT 1 Standard Test Method for Sulfur in Gasoline by Wavelength Dispersive X-Ray Fluorescence (Withdrawn 2022)
ASTM D 4628 : 2016 Standard Test Method for Analysis of Barium, Calcium, Magnesium, and Zinc in Unused Lubricating Oils by Atomic Absorption Spectrometry
ASTM D 1318 : 2023 Standard Test Method for Sodium in Residual Fuel Oil (Flame Photometric Method)
ASTM D 7319 : 2022 Standard Test Method for Determination of Existent and Potential Sulfate and Inorganic Chloride in Fuel Ethanol and Butanol by Direct Injection Suppressed Ion Chromatography
ASTM D 5291 : 2016 Standard Test Methods for Instrumental Determination of Carbon, Hydrogen, and Nitrogen in Petroleum Products and Lubricants
ASTM D 3231 : 2018 Standard Test Method for Phosphorus in Gasoline
ASTM D 3831 : 2022 Standard Test Method for Manganese in Gasoline By Atomic Absorption Spectroscopy
ASTM D 445 : 1988 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and the Calculation of Dynamic Viscosity)
ASTM D 6792 : 2023 : REV B Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 1552 : 2023 Standard Test Method for Sulfur in Petroleum Products by High Temperature Combustion and Infrared (IR) Detection or Thermal Conductivity Detection (TCD)
ASTM D 5863 : 2000 : REV A : R2016 Standard Test Methods for Determination of Nickel, Vanadium, Iron, and Sodium in Crude Oils and Residual Fuels by Flame Atomic Absorption Spectrometry
ASTM D 3228 : 2022 Standard Test Method for Total Nitrogen in Lubricating Oils and Fuel Oils by Modified Kjeldahl Method
ASTM D 5059 : 2021 Standard Test Methods for Lead and Manganese in Gasoline by X-Ray Fluorescence Spectroscopy
ASTM D 4294 : 2008 Standard Test Method for Sulfur in Petroleum and Petroleum Products by Energy Dispersive X-ray Fluorescence Spectrometry
ASTM E 77 : 2014 : EDT 1 Standard Test Method for Inspection and Verification of Thermometers
ASTM D 6792 : 2020 Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 6792 : 2021 Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 6728 : 2016 Standard Test Method for Determination of Contaminants in Gas Turbine and Diesel Engine Fuel by Rotating Disc Electrode Atomic Emission Spectrometry
ASTM D 1318 : 2016 Standard Test Method for Sodium in Residual Fuel Oil (Flame Photometric Method)
ASTM D 5622 : 2024 Standard Test Methods for Determination of Total Oxygen in Gasoline and Methanol Fuels by Reductive Pyrolysis
ASTM D 7212 : 2013 : R2018 Standard Test Method for Low Sulfur in Automotive Fuels by Energy-Dispersive X-ray Fluorescence Spectrometry Using a Low-Background Proportional Counter (Withdrawn 2024)
ASTM D 2622 : 2024 Standard Test Method for Sulfur in Petroleum Products by Wavelength Dispersive X-ray Fluorescence Spectrometry
ASTM D 1091 : 2011 : R2016 Standard Test Methods for Phosphorus in Lubricating Oils and Additives (Withdrawn 2021)
ASTM D 6481 : 2014 : R2019 Standard Test Method for Determination of Phosphorus, Sulfur, Calcium, and Zinc in Lubrication Oils by Energy Dispersive X-ray Fluorescence Spectroscopy
ASTM D 5056 : 1996 Standard Test Method for Trace Metals in Petroleum Coke by Atomic Absorption
ASTM D 7319 : 2017 Standard Test Method for Determination of Existent and Potential Sulfate and Inorganic Chloride in Fuel Ethanol and Butanol by Direct Injection Suppressed Ion Chromatography
ASTM D 1552 : 2016 : EDT 1 Standard Test Method for Sulfur in Petroleum Products by High Temperature Combustion and Infrared (IR) Detection or Thermal Conductivity Detection (TCD)
ASTM D 7318 : 2019 Standard Test Method for Existent Inorganic Sulfate in Ethanol by Potentiometric Titration
ASTM D 5600 : 2022 Standard Test Method for Trace Metals in Petroleum Coke by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
ASTM D 3228 : 2020 Standard Test Method for Total Nitrogen in Lubricating Oils and Fuel Oils by Modified Kjeldahl Method
ASTM D 874 : 2023 Standard Test Method for Sulfated Ash from Lubricating Oils and Additives
ASTM E 319 : 1985 : R2014 Standard Practice for the Evaluation of Single-Pan Mechanical Balances (Withdrawn 2021)
ASTM D 445 : 2019 : REV A Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM D 6481 : 2024 Standard Test Method for Determination of Phosphorus, Sulfur, Calcium, and Zinc in Lubrication Oils by Energy Dispersive X-ray Fluorescence Spectroscopy
ASTM D 6792 : 2021 : REV C Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 5059 : 2020 Standard Test Methods for Lead and Manganese in Gasoline by X-Ray Spectroscopy
ASTM D 8127 : 2017 : EDT 1 Standard Test Method for Coupled Particulate and Elemental Analysis using X-ray Fluorescence (XRF) for In-Service Lubricants
ASTM D 4307 : 2017 Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards
ASTM D 5762 : 1998 Standard Test Method for Nitrogen in Petroleum and Petroleum Products by Boat-Inlet Chemiluminescence
ASTM D 6667 : 2014 : R2019 Standard Test Method for Determination of Total Volatile Sulfur in Gaseous Hydrocarbons and Liquefied Petroleum Gases by Ultraviolet Fluorescence
ASTM D 6595 : 2022 Standard Test Method for Determination of Wear Metals and Contaminants in Used Lubricating Oils or Used Hydraulic Fluids by Rotating Disc Electrode Atomic Emission Spectrometry
ASTM D 6792 : 2023 : REV A Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 4294 : 2016 : EDT 1 Standard Test Method for Sulfur in Petroleum and Petroleum Products by Energy Dispersive X-ray Fluorescence Spectrometry
ASTM D 5453 : 2016 : EDT 1 Standard Test Method for Determination of Total Sulfur in Light Hydrocarbons, Spark Ignition Engine Fuel, Diesel Engine Fuel, and Engine Oil by Ultraviolet Fluorescence
ASTM D 8150 : 2022 Standard Test Method for Determination of Organic Chloride Content in Crude Oil by Distillation Followed by Detection Using Combustion Ion Chromatography
ASTM D 7691 : 2016 Standard Test Method for Multielement Analysis of Crude Oils Using Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
ASTM D 8127 : 2023 Standard Test Method for Coupled Particulate and Elemental Analysis using X-ray Fluorescence (XRF) for In-Service Lubricants
ASTM D 5600 : 2017 Standard Test Method for Trace Metals in Petroleum Coke by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
ASTM D 7220 : 2022 Standard Test Method for Sulfur in Automotive, Heating, and Jet Fuels by Monochromatic Energy Dispersive X-ray Fluorescence Spectrometry
ASTM D 5800 : 2021 Standard Test Method for Evaporation Loss of Lubricating Oils by the Noack Method
ASTM D 445 : 2019 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM D 4629 : 2017 Standard Test Method for Trace Nitrogen in Liquid Hydrocarbons by Syringe/Inlet Oxidative Combustion and Chemiluminescence Detection
ASTM D 4307 : 2017 : R2021 Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards
ASTM D 3246 : 2015 Standard Test Method for Sulfur in Petroleum Gas by Oxidative Microcoulometry (Withdrawn 2024)
ASTM D 4294 : 2021 Standard Test Method for Sulfur in Petroleum and Petroleum Products by Energy Dispersive X-ray Fluorescence Spectrometry
ASTM D 5291 : 2001 Standard Test Methods for Instrumental Determination of Carbon, Hydrogen, and Nitrogen in Petroleum Products and Lubricants
ASTM D 445 : 2001 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (the Calculation of Dynamic Viscosity)
ASTM D 2622 : 2021 Standard Test Method for Sulfur in Petroleum Products by Wavelength Dispersive X-ray Fluorescence Spectrometry
ASTM D 445 : 2024 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM D 445 : 2021 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM D 6792 : 2022 Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 5453 : 2019 : REV A Standard Test Method for Determination of Total Sulfur in Light Hydrocarbons, Spark Ignition Engine Fuel, Diesel Engine Fuel, and Engine Oil by Ultraviolet Fluorescence
ASTM D 7751 : 2016 Standard Test Method for Determination of Additive Elements in Lubricating Oils by EDXRF Analysis
ASTM D 6595 : 2017 Standard Test Method for Determination of Wear Metals and Contaminants in Used Lubricating Oils or Used Hydraulic Fluids by Rotating Disc Electrode Atomic Emission Spectrometry
ASTM D 892 : 2023 Standard Test Method for Foaming Characteristics of Lubricating Oils
ASTM D 6443 : 2014 : R2019 : EDT 1 Standard Test Method for Determination of Calcium, Chlorine, Copper, Magnesium, Phosphorus, Sulfur, and Zinc in Unused Lubricating Oils and Additives by Wavelength Dispersive X-ray Fluorescence Spectrometry (Mathematical Correction Procedure)
ASTM D 7328 : 2017 Standard Test Method for Determination of Existent and Potential Inorganic Sulfate and Total Inorganic Chloride in Fuel Ethanol by Ion Chromatography Using Aqueous Sample Injection
ASTM D 7455 : 2024 Standard Practice for Sample Preparation of Petroleum and Lubricant Products for Elemental Analysis
ASTM D 7041 : 2016 Standard Test Method for Determination of Total Sulfur in Liquid Hydrocarbons and Hydrocarbon-Oxygenate Blends by Gas Chromatography with Flame Photometric Detection
ASTM D 5800 : 2020 Standard Test Method for Evaporation Loss of Lubricating Oils by the Noack Method
ASTM D 892 : 2018 : EDT 1 Standard Test Method for Foaming Characteristics of Lubricating Oils
ASTM D 3237 : 2017 Standard Test Method for Lead in Gasoline by Atomic Absorption Spectroscopy
ASTM D 5453 : 2019 Standard Test Method for Determination of Total Sulfur in Light Hydrocarbons, Spark Ignition Engine Fuel, Diesel Engine Fuel, and Engine Oil by Ultraviolet Fluorescence
ASTM D 3831 : 1998 Standard Test Method for Manganese In Gasoline By Atomic Absorption Spectroscopy
ASTM D 445 : 2018 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM D 8150 : 2017 Standard Test Method for Determination of Organic Chloride Content in Crude Oil by Distillation Followed by Detection Using Combustion Ion Chromatography
ASTM D 7757 : 2017 Standard Test Method for Silicon in Gasoline and Related Products by Monochromatic Wavelength Dispersive X-ray Fluorescence Spectrometry
ASTM D 3237 : 1997 Standard Test Method for Lead In Gasoline By Atomic Absorption Spectroscopy
ASTM D 4629 : 2024 Standard Test Method for Trace Nitrogen in Liquid Hydrocarbons by Syringe/Inlet Oxidative Combustion and Chemiluminescence Detection
ASTM D 6792 : 2023 Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 445 : 2021 : EDT 1 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM D 1552 : 2016 : R2021 Standard Test Method for Sulfur in Petroleum Products by High Temperature Combustion and Infrared (IR) Detection or Thermal Conductivity Detection (TCD)
ASTM D 7111 : 2016 : R2021 Standard Test Method for Determination of Trace Elements in Middle Distillate Fuels by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
ASTM D 3831 : 2012 : R2017 Standard Test Method for Manganese in Gasoline By Atomic Absorption Spectroscopy
ASTM D 7303 : 2023 Standard Test Method for Determination of Metals in Lubricating Greases by Inductively Coupled Plasma Atomic Emission Spectrometry
ASTM D 7455 : 2019 Standard Practice for Sample Preparation of Petroleum and Lubricant Products for Elemental Analysis
ASTM D 5056 : 2022 Standard Test Method for Trace Metals in Petroleum Coke by Atomic Absorption
ASTM E 77 : 1998 Standard Test Method for Inspection and Verification of Thermometers
ASTM D 6792 : 2022 : REV A Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ASTM D 3237 : 2022 Standard Test Method for Lead in Gasoline by Atomic Absorption Spectroscopy
ASTM D 7751 : 2016 : R2021 Standard Test Method for Determination of Additive Elements in Lubricating Oils by EDXRF Analysis
ASTM D 5453 : 2024 Standard Test Method for Determination of Total Sulfur in Light Hydrocarbons, Spark Ignition Engine Fuel, Diesel Engine Fuel, and Engine Oil by Ultraviolet Fluorescence
ASTM E 77 : 2014 : R2021 Standard Test Method for Inspection and Verification of Thermometers
ASTM D 5762 : 2018 : REV A Standard Test Method for Nitrogen in Liquid Hydrocarbons, Petroleum and Petroleum Products by Boat-Inlet Chemiluminescence
ASTM D 7691 : 2023 Standard Test Method for Multielement Analysis of Crude Oils Using Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
ASTM D 445 : 2023 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM D 2622 : 2016 Standard Test Method for Sulfur in Petroleum Products by Wavelength Dispersive X-ray Fluorescence Spectrometry

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