UNI EN ISO 12677 : 2011
Current
The latest, up-to-date edition.
CHEMICAL ANALYSIS OF REFRACTORY PRODUCTS BY X-RAY FLUORESCENCE (XRF) - FUSED CAST-BEAD METHOD
26-10-2011
Foreword
1 Scope
2 Normative references
3 Types of material
4 Principle
5 Apparatus
6 Sample grinding
7 Loss on ignition (and/or drying)
8 Flux
9 Fusion casting procedures
10 Calibration
11 Corrections
12 Reproducibility and repeatability
13 Accuracy determined by certified reference materials
14 Definitions of limits of detection
15 Test report
Annex A (normative) - Calibration range and required
detection limits
Annex B (normative) - Corrections for tungsten carbide
grinding media
Annex C (informative) - Examples of fluxes/flux ratios
Annex D (normative) - Examples of CRM to be used to
check synthetic calibrations
Annex E (normative) - Examples of SeRM
Annex F (normative) - Equation for theoretical calculations
Annex G (normative) - Certified reference materials (CRMs)
Annex H (normative) - Method of inter-element correction
used to compensate for the effects of co-existing
components when using SeRM for calibration
Annex I (normative) - Standard deviations achieved with
certified reference materials
Bibliography
Describes a method for the chemical analysis of refractory and technical ceramic raw materials, intermediates and products, by means of the X-ray fluorescence (XRF) fused cast-bead method.
| Committee |
CT 700
|
| DocumentType |
Standard
|
| PublisherName |
Ente Nazionale Italiano di Unificazione (UNI)
|
| Status |
Current
|
| Supersedes |
| Standards | Relationship |
| UNE-EN ISO 12677:2012 | Identical |
| SN EN ISO 12677:2012 | Identical |
| NBN EN ISO 12677 : 2011 | Identical |
| DIN EN ISO 12677:2013-02 | Identical |
| NEN EN ISO 12677 : 2011 | Identical |
| EN ISO 12677:2011 | Identical |
| I.S. EN ISO 12677:2011 | Identical |
| NF EN ISO 12677 : 2011 | Identical |
| BS EN ISO 12677:2011 | Identical |
| ISO 12677:2011 | Identical |
| NS EN ISO 12677 : 2011 | Identical |
| AS 2503.6-2007 | Refractories and refractory materials - Chemical analysis Refractories, refractory mortars and silicate materials - Determination of major and minor elements - Wavelength dispersive X-ray fluorescence spectrometry using lithium borate fusion (Reconfirmed 2017) |
| ISO 565:1990 | Test sieves — Metal wire cloth, perforated metal plate and electroformed sheet — Nominal sizes of openings |
| ISO Guide 35:2017 | Reference materials — Guidance for characterization and assessment of homogeneity and stability |
| ISO 21068-2:2008 | Chemical analysis of silicon-carbide-containing raw materials and refractory products — Part 2: Determination of loss on ignition, total carbon, free carbon and silicon carbide, total and free silica and total and free silicon |
| ISO 3534-2:2006 | Statistics — Vocabulary and symbols — Part 2: Applied statistics |
| ISO 21068-1:2008 | Chemical analysis of silicon-carbide-containing raw materials and refractory products — Part 1: General information and sample preparation |
| ISO 21068-3:2008 | Chemical analysis of silicon-carbide-containing raw materials and refractory products — Part 3: Determination of nitrogen, oxygen and metallic and oxidic constituents |
| ISO 26845:2008 | Chemical analysis of refractories General requirements for wet chemical analysis, atomic absorption spectrometry (AAS) and inductively coupled plasma atomic emission spectrometry (ICP-AES) methods |
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