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ASTM D 5827 : 2009 : R2015

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by

Standard Test Method for Analysis of Engine Coolant for Chloride and Other Anions by Ion Chromatography

Available format(s)

Hardcopy , PDF

Superseded date

20-06-2022

Superseded by

ASTM D 5827 : 2022

Language(s)

English

Published date

05-06-2015

€67.30
Excluding VAT

This test method covers the chemical analysis of engine coolant for chloride ion by high-performance ion chromatography (HPIC).

Committee
D 15
DocumentType
Test Method
Pages
6
ProductNote
Reconfirmed 2015
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

1.1This test method covers the chemical analysis of engine coolant for chloride ion by high-performance ion chromatography (HPIC). Several other common anions found in engine coolant can be determined in one chromatographic analysis by this test method.

1.2This test method is applicable to both new and used engine coolant.

1.3Coelution of other ions may cause interferences for any of the listed anions. In the case of unfamiliar formulations, identification verification should be performed by either or both fortification and dilution of the sample matrix with the anions of interest.

1.4Analysis can be performed directly by this test method without pretreatment, other than dilution, as required by the linear ranges of the equipment. Table 1 indicates several applicable anions and approximate detection limits.

(A)Determined using 100-μL sample volume. Sample diluted 99 + 1 (v/v) with chromatographic eluant 30-μS/cm full scale, suppressed conductivity detection. Dionex AS4ASC column with AG4ASC guard columns. Other systems will require MDL determinations using chosen dilution factors, eluants, columns, and detector.

1.5The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.6This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to its use.

ASTM E 1177 : 2022 Standard Specification for Engine Coolant Grade Glycol
ASTM D 2847 : 2022 Standard Practice for Testing Engine Coolants in Car and Light Truck Service
ASTM D 7388 : 2018 Standard Specification for Engine Coolant Grade 1,3-Propanediol (PDO)
ASTM E 1177 : 2014 Standard Specification for Engine Coolant Grade Glycol
ASTM D 7640 : 2016 Standard Specification for Engine Coolant Grade Glycerin
ASTM D 3585 : 2008 : R2013 Standard Specification for ASTM Reference Fluid for Coolant Tests
ASTM D 7319 : 2017 Standard Test Method for Determination of Existent and Potential Sulfate and Inorganic Chloride in Fuel Ethanol and Butanol by Direct Injection Suppressed Ion Chromatography
ASTM D 4985 : 2010 : R2015 Standard Specification for Low Silicate Ethylene Glycol Base Engine Coolant for Heavy Duty Engines Requiring a Pre-Charge of Supplemental Coolant Additive (SCA)
ASTM D 8039 : 2016 Standard Specification for Heat Transfer Fluids (HTF) for Heating and Air Conditioning (HVAC) Systems
ASTM D 7714 : 2011 : R2016 : EDT 1 Standard Specification for Glycerin Base Engine Coolant for Automobile and Light-Duty Service
ASTM D 3585 : 2008 : R2020 Standard Specification for ASTM Reference Fluid for Coolant Tests
ASTM D 7714 : 2011 : R2021 Standard Specification for Glycerin Base Engine Coolant for Automobile and Light-Duty Service
ASTM D 7640 : 2016 : R2021 Standard Specification for Engine Coolant Grade Glycerin
ASTM D 8149 : 2020 Standard Practice for Optimization, Calibration, and Validation of Ion Chromatographic Determination of Heteroatoms and Anions in Petroleum Products and Lubricants
ASTM D 3306 : 2021 Standard Specification for Glycol Base Engine Coolant for Automobile and Light-Duty Service
ASTM D 7518 : 2020 Standard Specification for 1,3 Propanediol (PDO) Base Engine Coolant for Automobile and Light-Duty Service
ASTM D 5752 : 2010 : R2017 Standard Specification for Supplemental Coolant Additives (SCAs) for Use in Precharging Coolants for Heavy-Duty Engines
ASTM D 7517 : 2019 Standard Specification for Fully-Formulated 1,3 Propanediol (PDO) Base Engine Coolant for Heavy-Duty Engines
ASTM D 8149 : 2017 Standard Practice for Optimization, Calibration, and Validation of Ion Chromatographic Determination of Heteroatoms and Anions in Petroleum Products and Lubricants
ASTM D 7328 : 2017 Standard Test Method for Determination of Existent and Potential Inorganic Sulfate and Total Inorganic Chloride in Fuel Ethanol by Ion Chromatography Using Aqueous Sample Injection
ASTM D 8116 : 2018 Standard Specification for Fully-Formulated Non-Aqueous Engine Coolant for Heavy-Duty Engines (Withdrawn 2019)
ASTM D 7518 : 2010 : R2015 : EDT 1 Standard Specification for 1,3 Propanediol (PDO) Base Engine Coolant for Automobile and Light-Duty Service
ASTM D 7713 : 2018 Standard Specification for Aqueous Engine Coolant Grade Glycol (53 % by Volume Nominal)
ASTM D 2847 : 2015 Standard Practice for Testing Engine Coolants in Car and Light Truck Service
ASTM D 3306 : 2019 Standard Specification for Glycol Base Engine Coolant for Automobile and Light-Duty Service
ASTM D 8085 : 2017 Standard Specification for Non-Aqueous Engine Coolant for Automobile and Light-Duty Service

ASTM E 177 : 1990 : REV A : R1996 Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods
ASTM E 177 : 2014 : REDLINE Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods
ASTM D 1176 : 2014 : REDLINE Standard Practice for Sampling and Preparing Aqueous Solutions of Engine Coolants or Antirusts for Testing Purposes
ASTM D 1176 : 1998 : R2008 Standard Practice for Sampling and Preparing Aqueous Solutions of Engine Coolants or Antirusts for Testing Purposes
ASTM D 1193 : 1977 : R1983 : EDT 1 Standard Specification for Reagent Water
ASTM D 1176 : 1998 : R2002 Standard Practice for Sampling and Preparing Aqueous Solutions of Engine Coolants or Antirusts for Testing Purposes
ASTM E 691 : 2020 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM E 691 : 2019 : EDT 1 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 1193 : 2006 : R2011 Standard Specification for Reagent Water
ASTM E 691 : 2009 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 1193 : 1991 Standard Specification for Reagent Water
ASTM D 1176 : 1998 Standard Practice for Sampling and Preparing Aqueous Solutions of Engine Coolants or Antirusts for Testing Purposes
ASTM E 691 : 2021 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 1176 : 2014 : R2019 Standard Practice for Sampling and Preparing Aqueous Solutions of Engine Coolants or Antirusts for Testing Purposes
ASTM D 1176 : 2014 Standard Practice for Sampling and Preparing Aqueous Solutions of Engine Coolants or Antirusts for Testing Purposes
ASTM D 1193 : 1970 Standard Specification For Reagent Water
ASTM D 1193 : 2006 Standard Specification for Reagent Water
ASTM D 1193 : 1999 Standard Specification for Reagent Water
ASTM D 1193 : 2006 : R2018 Standard Specification for Reagent Water

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