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EN 14778:2011

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by

Solid biofuels - Sampling

Superseded date

01-04-2017

Superseded by

EN ISO 18135:2017

Published date

15-06-2011

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Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Symbols and abbreviations
5 Principle
6 Establishing a sampling scheme (sampling plan)
7 Visual inspection
8 Number of increments
9 Calculation of the size of increment
10 Combined sample - Calculation of the
   volume of the combined sample
11 Sampling equipment
12 Sampling in practice
13 Sample generation
14 Performance characteristics
15 Handling and storage of samples
16 Sampling certificates
Annex A (informative) - Model Sampling Plan and
        Sampling Certificate
Annex B (informative) - Sampling from large stockpiles
Annex C (informative) - Bulk densities of biofuels
Annex D (informative) - Empirical values for
        P[L], V[I] and V[PT]
Annex E (informative) - Guidelines for the number
        of increments to be taken
Annex F (informative) - Quality parameters for various
        solid biofuels in BioNorm projects and
        large shipments of wood pellets
Bibliography

This European Standard describes methods for preparing sampling plans and certificates and taking samples of solid biofuels, for example, from the place where the raw materials grow, from production plant, from deliveries e.g. lorry loads, or from stock. It includes both manual and mechanical methods, and is applicable to solid biofuels that are either:-fine (particle size up to about 10 mm) and regularly-shaped particulate materials that can be sampled using a scoop or pipe, for example: sawdust, olive stones and wood pellets;-coarse or irregularly-shaped particulate materials, particle sizes up to about 200 mm that can be sampled using a fork or shovel, for example: wood chips and nut shells, forest residue chips, and straw;-baled materials for example: baled straw or grass;-large pieces (particles sizes above 200 mm) which are either picked manually or automatically;-vegetable waste, fibrous waste from virgin pulp production and from production of paper from pulp that has been dewatered;- round wood.It may be possible to use this standard on other solid biofuels. The methods described in this European Standard may be used, for example, when the samples are to be tested for moisture content, ash content, calorific value, bulk density, durability, particle size distribution, ash melting behaviour and chemical composition. The methods are not intended for obtaining the very large samples required for the testing of bridging properties.

Committee
CEN/TC 335
DevelopmentNote
Supersedes CEN/TS 14778-1, CEN/TS 14778-2 & CEN/TS 14779. (06/2011) Supersedes PREN 14778. (08/2011)
DocumentType
Standard
PublisherName
Comite Europeen de Normalisation
Status
Superseded
SupersededBy
Supersedes

Standards Relationship
NBN EN 14778 : 2011 Identical
DIN EN 14778:2011-09 Identical
UNI EN 14778 : 2011 Identical
NEN EN 14778 : 2011 Identical
I.S. EN 14778:2011 Identical
SN EN 14778 : 2011 Identical
NS EN 14778 : 2011 Identical
NF EN 14778 : 2011 Identical
UNE-EN 14778:2013 Identical
PN EN 14778 : 2011 Identical
BS EN 14778:2011 Identical

BS EN 15234-4:2012 Solid biofuels. Fuel quality assurance Wood chips for non-industrial use
BS EN ISO 18122:2015 Solid biofuels. Determination of ash content
BS EN 16640:2017 Bio-based products. Bio-based carbon content. Determination of the bio-based carbon content using the radiocarbon method
BS EN ISO 17830:2016 Solid biofuels. Particle size distribution of disintegrated pellets
DIN EN ISO 18123:2016-03 Solid biofuels - Determination of the content of volatile matter (ISO 18123:2015)
BS EN ISO 17827-1:2016 Solid biofuels. Determination of particle size distribution for uncompressed fuels Oscillating screen method using sieves with apertures of 3,15 mm and above
16/30303043 DC : DRAFT MAR 2016 BS EN ISO 19743 - SOLID BIOFUELS - DETERMINATION OF CONTENT OF HEAVY EXTRANEOUS MATERIALS LARGE THAN 3,15 MM
I.S. EN 16127:2012 SOLID BIOFUELS - DETERMINATION OF LENGTH AND DIAMETER OF PELLETS
DIN EN ISO 18122:2016-03 Solid biofuels - Determination of ash content (ISO 18122:2015)
DIN EN 16640:2015-09 (Draft) BIO-BASED PRODUCTS - BIO-BASED CARBON CONTENT - DETERMINATION OF THE BIO-BASED CARBON CONTENT USING THE RADIOCARBON METHOD
I.S. EN 14780:2011 SOLID BIOFUELS - SAMPLE PREPARATION
15/30319064 DC : 0 BS EN ISO 18125 - SOLID BIOFUELS - DETERMINATION OF CALORIFIC VALUE
UNE-EN ISO 17827-1:2016 Solid biofuels - Determination of particle size distribution for uncompressed fuels - Part 1: Oscillating screen method using sieves with apertures of 3,15 mm and above (ISO 17827-1:2016)
BS EN 15150:2011 Solid biofuels. Determination of particle density
BS EN 16126:2012 Solid biofuels. Determination of particle size distribution of disintegrated pellets
UNE-EN ISO 18123:2016 Solid biofuels - Determination of the content of volatile matter (ISO 18123:2015)
I.S. EN 16785-1:2015 BIO-BASED PRODUCTS - BIO-BASED CONTENT - PART 1: DETERMINATION OF THE BIO-BASED CONTENT USING THE RADIOCARBON ANALYSIS AND ELEMENTAL ANALYSIS
I.S. EN ISO 18134-3:2015 SOLID BIOFUELS - DETERMINATION OF MOISTURE CONTENT - OVEN DRY METHOD - PART 3: MOISTURE IN GENERAL ANALYSIS SAMPLE (ISO 18134-3:2015)
S.R. CEN/TR 15149-3:2014 SOLID BIOFUELS - DETERMINATION OF PARTICLE SIZE DISTRIBUTION - PART 3: ROTARY SCREEN METHOD
I.S. EN ISO 17827-1:2016 SOLID BIOFUELS - DETERMINATION OF PARTICLE SIZE DISTRIBUTION FOR UNCOMPRESSED FUELS - PART 1: OSCILLATING SCREEN METHOD USING SIEVES WITH APERTURES OF 3,15 MM AND ABOVE (ISO 17827-1:2016)
S.R. CEN/TS 16640:2014 BIO-BASED PRODUCTS - DETERMINATION OF THE BIO BASED CARBON CONTENT OF PRODUCTS USING THE RADIOCARBON METHOD
UNE-EN 15234-4:2012 Solid biofuels - Fuel quality assurance - Part 4: Wood chips for non-industrial use
I.S. EN 16640:2017 BIO-BASED PRODUCTS - BIO-BASED CARBON CONTENT - DETERMINATION OF THE BIO-BASED CARBON CONTENT USING THE RADIOCARBON METHOD
UNE-EN ISO 17829:2016 Solid biofuels - Determination of length and diameter of pellets (ISO 17829:2015)
BS EN 303-5:2012 Heating boilers Heating boilers for solid fuels, manually and automatically stoked, nominal heat output of up to 500 kW. Terminology, requirements, testing and marking
EN 14780:2011 Solid biofuels - Sample preparation
CEN/TS 16640:2014 Bio-based products - Determination of the bio based carbon content of products using the radiocarbon method
DIN EN 16127:2012-05 SOLID BIOFUELS - DETERMINATION OF LENGTH AND DIAMETER OF PELLETS
CEN/TR 15149-3:2014 Solid biofuels - Determination of particle size distribution - Part 3: Rotary screen method
BS EN ISO 18134-3:2015 Solid biofuels. Determination of moisture content. Oven dry method Moisture in general analysis sample
UNE-EN 16127:2012 Solid biofuels - Determination of length and diameter of pellets
UNE-EN ISO 18134-3:2016 Solid biofuels - Determination of moisture content - Oven dry method - Part 3: Moisture in general analysis sample (ISO 18134-3:2015)
DIN EN ISO 17827-1:2016-10 Solid biofuels - Determination of particle size distribution for uncompressed fuels - Part 1: Oscillating screen method using sieves with apertures of 3,15 mm and above (ISO 17827-1:2016)
BS EN 16127:2012 Solid biofuels. Determination of length and diameter of pellets
DIN EN 15150:2012-01 SOLID BIOFUELS - DETERMINATION OF PARTICLE DENSITY
DIN EN 14961-6:2012-04 SOLID BIOFUELS - FUEL SPECIFICATIONS AND CLASSES - PART 6: NON-WOODY PELLETS FOR NON-INDUSTRIAL USE
CSA ISO 18134-3 : 2015 SOLID BIOFUELS - DETERMINATION OF MOISTURE CONTENT - OVEN DRY METHOD - PART 3: MOISTURE IN GENERAL ANALYSIS SAMPLE
UNI EN 15234-4 : 2012 SOLID BIOFUELS - FUEL QUALITY ASSURANCE - PART 4: WOOD CHIPS FOR NON-INDUSTRIAL USE
UNE-EN ISO 18122:2016 Solid biofuels - Determination of ash content (ISO 18122:2015)
UNI EN 14961-6 : 2012 SOLID BIOFUELS - FUEL SPECIFICATIONS AND CLASSES - PART 6: NON-WOODY PELLETS FOR NON-INDUSTRIAL USE
I.S. EN 15150:2011 SOLID BIOFUELS - DETERMINATION OF PARTICLE DENSITY
BS EN 14780:2011 Solid biofuels. Sample preparation
DIN EN 303-5:2012-10 Heating boilers - Part 5: Heating boilers for solid fuels, manually and automatically stoked, nominal heat output of up to 500 kW - Terminology, requirements, testing and marking
ISO 18134-3:2015 Solid biofuels — Determination of moisture content — Oven dry method — Part 3: Moisture in general analysis sample
I.S. EN 303-5:2012 HEATING BOILERS - PART 5: HEATING BOILERS FOR SOLID FUELS, MANUALLY AND AUTOMATICALLY STOKED, NOMINAL HEAT OUTPUT OF UP TO 500 KW - TERMINOLOGY, REQUIREMENTS, TESTING AND MARKING
DIN EN 16640:2017-08 BIO-BASED PRODUCTS - BIO-BASED CARBON CONTENT - DETERMINATION OF THE BIO-BASED CARBON CONTENT USING THE RADIOCARBON METHOD
DIN EN 14780:2011-09 SOLID BIOFUELS - SAMPLE PREPARATION
EN 303-5:2012 Heating boilers - Part 5: Heating boilers for solid fuels, manually and automatically stoked, nominal heat output of up to 500 kW - Terminology, requirements, testing and marking
PD CEN/TR 15149-3:2014 Solid biofuels. Determination of particle size distribution Rotary screen method
DIN EN ISO 17829:2016-03 SOLID BIOFUELS - DETERMINATION OF LENGTH AND DIAMETER OF PELLETS (ISO 17829:2015)
DIN EN 16126:2012-05 SOLID BIOFUELS - DETERMINATION OF PARTICLE SIZE DISTRIBUTION OF DISINTEGRATED PELLETS
I.S. EN ISO 18134-1:2015 SOLID BIOFUELS - DETERMINATION OF MOISTURE CONTENT - OVEN DRY METHOD - PART 1: TOTAL MOISTURE - REFERENCE METHOD (ISO 18134-1:2015)
BS EN 14961-6:2012 Solid biofuels. Fuel specifications and classes Non-woody pellets for non-industrial use
UNE-EN ISO 18134-1:2016 Solid biofuels - Determination of moisture content - Oven dry method - Part 1: Total moisture - Reference method (ISO 18134-1:2015)
DIN EN ISO 18134-3:2015-12 Solid biofuels - Determination of moisture content - Oven dry method - Part 3: Moisture in general analysis sample (ISO 18134-3:2015)
DIN EN ISO 17827-1 E : 2016 SOLID BIOFUELS - DETERMINATION OF PARTICLE SIZE DISTRIBUTION FOR UNCOMPRESSED FUELS - PART 1: OSCILLATING SCREEN METHOD USING SIEVES WITH APERTURES OF 3,15 MM AND ABOVE (ISO 17827-1:2016)
BS ISO 18466:2016 Stationary source emissions. Determination of the biogenic fraction in C O<sub>2</sub> in stack gas using the balance method
DIN EN ISO 18134-1:2015-12 Solid biofuels - Determination of moisture content - Oven dry method - Part 1: Total moisture - Reference method (ISO 18134-1:2015)
UNI EN 303-5 : 2012 HEATING BOILERS - PART 5: HEATING BOILERS FOR SOLID FUELS, MANUALLY AND AUTOMATICALLY STOKED, NOMINAL HEAT OUTPUT OF UP TO 500 KW - TERMINOLOGY, REQUIREMENTS, TESTING AND MARKING
14/30304809 DC : 0 BS EN 16785 - BIO-BASED PRODUCTS - DETERMINATION OF THE BIO-BASED CONTENT USING THE RADIOCARBON ANALYSIS AND ELEMENTAL ANALYSIS
CAN/CSA-ISO 17827-1:17 SOLID BIOFUELS - DETERMINATION OF PARTICLE SIZE DISTRIBUTION FOR UNCOMPRESSED FUELS - PART 1: OSCILLATING SCREEN METHOD USING SIEVES WITH APERTURES OF 3,15 MM AND ABOVE
BS EN ISO 17829:2015 Solid biofuels. Determination of length and diameter of pellets
I.S. EN ISO 18122:2015 SOLID BIOFUELS - DETERMINATION OF ASH CONTENT (ISO 18122:2015)
NF EN 15234-4 : 2012 SOLID BIOFUELS - FUEL QUALITY ASSURANCE - PART 4: WOOD CHIPS FOR NON-INDUSTRIAL USE
ISO 18466:2016 Stationary source emissions — Determination of the biogenic fraction in CO2 in stack gas using the balance method
UNI EN 16126 : 2012 SOLID BIOFUELS - DETERMINATION OF PARTICLE SIZE DISTRIBUTION OF DISINTEGRATED PELLETS
UNE-EN 16640:2017 Bio-based products - Bio-based carbon content - Determination of the bio-based carbon content using the radiocarbon method
ISO 17827-1:2016 Solid biofuels — Determination of particle size distribution for uncompressed fuels — Part 1: Oscillating screen method using sieves with apertures of 3,15 mm and above
EN ISO 17829:2015 Solid biofuels - Determination of length and diameter of pellets (ISO 17829:2015)
BS EN ISO 18123:2015 Solid biofuels. Determination of the content of volatile matter
UNI EN 16127 : 2012 SOLID BIOFUELS - DETERMINATION OF LENGTH AND DIAMETER OF PELLETS
UNE-EN ISO 17830:2016 Solid biofuels - Particle size distribution of disintegrated pellets (ISO 17830:2016)
DIN EN 15234-4:2012-04 Solid biofuels - Fuel quality assurance - Part 4: Wood chips for non-industrial use
CSA ISO 18134-2 : 2015 SOLID BIOFUELS - DETERMINATION OF MOISTURE CONTENT - OVEN DRY METHOD - PART 2: TOTAL MOISTURE - SIMPLIFIED METHOD
BS EN 16785-1:2015 Bio-based products. Bio-based content Determination of the bio-based content using the radiocarbon analysis and elemental analysis
UNE-EN 16785-1:2016 Bio-based products - Bio-based content - Part 1: Determination of the bio-based content using the radiocarbon analysis and elemental analysis
15/30326869 DC : 0 BS EN 16640 - BIO-BASED PRODUCTS - BIO-BASED CARBON CONTENT - DETERMINATION OF THE BIO-BASED CARBON CONTENT USING THE RADIOCARBON METHOD
I.S. EN 16126:2012 SOLID BIOFUELS - DETERMINATION OF PARTICLE SIZE DISTRIBUTION OF DISINTEGRATED PELLETS
I.S. EN ISO 18123:2015 SOLID BIOFUELS - DETERMINATION OF THE CONTENT OF VOLATILE MATTER (ISO 18123:2015)
CAN/CSA-ISO 17830:17 Solid biofuels — Particle size distribution of disintegrated pellets (Adopted ISO 17830:2016, first edition, 2016-03-01)
UNI CEN/TS 16640 : 2014 BIO-BASED PRODUCTS - DETERMINATION OF THE BIO BASED CARBON CONTENT OF PRODUCTS USING THE RADIOCARBON METHOD
UNE-EN 14961-6:2012 Solid biofuels - Fuel specifications and classes - Part 6: Non-woody pellets for non-industrial use
I.S. EN 14961-6:2012 SOLID BIOFUELS - FUEL SPECIFICATIONS AND CLASSES - PART 6: NON-WOODY PELLETS FOR NON-INDUSTRIAL USE
I.S. EN ISO 17830:2016 SOLID BIOFUELS - PARTICLE SIZE DISTRIBUTION OF DISINTEGRATED PELLETS (ISO 17830:2016)
ISO 18123:2015 Solid biofuels — Determination of the content of volatile matter
ISO 17830:2016 Solid biofuels — Particle size distribution of disintegrated pellets
ISO 18134-1:2015 Solid biofuels — Determination of moisture content — Oven dry method — Part 1: Total moisture — Reference method
ISO 18122:2015 Solid biofuels — Determination of ash content
ISO 17829:2015 Solid Biofuels Determination of length and diameter of pellets
EN 16785-1:2015 Bio-based products - Bio-based content - Part 1: Determination of the bio-based content using the radiocarbon analysis and elemental analysis
EN ISO 18134-3:2015 Solid biofuels - Determination of moisture content - Oven dry method - Part 3: Moisture in general analysis sample (ISO 18134-3:2015)
EN 14961-6:2012 Solid biofuels - Fuel specifications and classes - Part 6: Non-woody pellets for non-industrial use
EN ISO 18123:2015 Solid biofuels - Determination of the content of volatile matter (ISO 18123:2015)
EN 16126:2012 Solid biofuels - Determination of particle size distribution of disintegrated pellets
EN 15234-4:2012 Solid biofuels - Fuel quality assurance - Part 4: Wood chips for non-industrial use
EN ISO 17827-1:2016 Solid biofuels - Determination of particle size distribution for uncompressed fuels - Part 1: Oscillating screen method using sieves with apertures of 3,15 mm and above (ISO 17827-1:2016)
EN ISO 18134-1:2015 Solid biofuels - Determination of moisture content - Oven dry method - Part 1: Total moisture - Reference method (ISO 18134-1:2015)
EN ISO 17830:2016 Solid biofuels - Particle size distribution of disintegrated pellets (ISO 17830:2016)
EN 16127:2012 Solid biofuels - Determination of length and diameter of pellets
DIN EN 16640 E : 2017 BIO-BASED PRODUCTS - BIO-BASED CARBON CONTENT - DETERMINATION OF THE BIO-BASED CARBON CONTENT USING THE RADIOCARBON METHOD
UNE-EN 16126:2012 Solid biofuels - Determination of particle size distribution of disintegrated pellets
BS EN ISO 18134-1:2015 Solid biofuels. Determination of moisture content. Oven dry method Total moisture. Reference method
DIN EN 16785-1:2016-03 BIO-BASED PRODUCTS - BIO-BASED CONTENT - PART 1: DETERMINATION OF THE BIO-BASED CONTENT USING THE RADIOCARBON ANALYSIS AND ELEMENTAL ANALYSIS
UNE-EN 14780:2012 Solid biofuels - Sample preparation
PD CEN/TS 16640:2014 Bio-based products. Determination of the bio based carbon content of products using the radiocarbon method
I.S. EN 15234-4:2012 SOLID BIOFUELS - FUEL QUALITY ASSURANCE - PART 4: WOOD CHIPS FOR NON-INDUSTRIAL USE
UNI EN 14780 : 2011 SOLID BIOFUELS - SAMPLE PREPARATION
16/30275160 DC : 0 BS ISO 18466 - STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE BIOGENIC FRACTION IN CO[2]IN STACK GAS USING THE BALANCE METHOD
CSA ISO 18134-1 : 2015 SOLID BIOFUELS - DETERMINATION OF MOISTURE CONTENT - OVEN DRY METHOD - PART 1: TOTAL MOISTURE - REFERENCE METHOD
UNI EN 15150 : 2011 SOLID BIOFUELS - DETERMINATION OF PARTICLE DENSITY
UNE-EN 15150:2012 Solid biofuels - Determination of particle density
I.S. EN ISO 17829:2015 SOLID BIOFUELS - DETERMINATION OF LENGTH AND DIAMETER OF PELLETS (ISO 17829:2015)
CSA ISO 18122 : 2016 SOLID BIOFUELS - DETERMINATION OF ASH CONTENT
NF EN 15150 : 2011 SOLID BIOFUELS - DETERMINATION OF PARTICLE DENSITY
UNE-EN 303-5:2013 Heating boilers - Part 5: Heating boilers for solid fuels, manually and automatically stoked, nominal heat output of up to 500 kW - Terminology, requirements, testing and marking
EN 15150:2011 Solid biofuels - Determination of particle density

EN 15103:2009 Solid biofuels - Determination of bulk density
ISO 3310-1:2016 Test sieves Technical requirements and testing Part 1: Test sieves of metal wire cloth
EN 15210-1:2009 Solid biofuels - Determination of mechanical durability of pellets and briquettes - Part 1: Pellets
EN 14588:2010 Solid biofuels - Terminology, definitions and descriptions
ISO 13909-7:2016 Hard coal and coke — Mechanical sampling — Part 7: Methods for determining the precision of sampling, sample preparation and testing
EN 14780:2011 Solid biofuels - Sample preparation
ISO 13909-8:2016 Hard coal and coke — Mechanical sampling — Part 8: Methods of testing for bias
ISO 18283:2006 Hard coal and coke Manual sampling

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