• EN 14778:2011

    Superseded A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

    Solid biofuels - Sampling

    Available format(s): 

    Superseded date:  01-04-2017

    Language(s): 

    Published date:  15-06-2011

    Publisher:  Comite Europeen de Normalisation

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    Table of Contents - (Show below) - (Hide below)

    Foreword
    Introduction
    1 Scope
    2 Normative references
    3 Terms and definitions
    4 Symbols and abbreviations
    5 Principle
    6 Establishing a sampling scheme (sampling plan)
    7 Visual inspection
    8 Number of increments
    9 Calculation of the size of increment
    10 Combined sample - Calculation of the
       volume of the combined sample
    11 Sampling equipment
    12 Sampling in practice
    13 Sample generation
    14 Performance characteristics
    15 Handling and storage of samples
    16 Sampling certificates
    Annex A (informative) - Model Sampling Plan and
            Sampling Certificate
    Annex B (informative) - Sampling from large stockpiles
    Annex C (informative) - Bulk densities of biofuels
    Annex D (informative) - Empirical values for
            P[L], V[I] and V[PT]
    Annex E (informative) - Guidelines for the number
            of increments to be taken
    Annex F (informative) - Quality parameters for various
            solid biofuels in BioNorm projects and
            large shipments of wood pellets
    Bibliography

    Abstract - (Show below) - (Hide below)

    This European Standard describes methods for preparing sampling plans and certificates and taking samples of solid biofuels, for example, from the place where the raw materials grow, from production plant, from deliveries e.g. lorry loads, or from stock. It includes both manual and mechanical methods, and is applicable to solid biofuels that are either:-fine (particle size up to about 10 mm) and regularly-shaped particulate materials that can be sampled using a scoop or pipe, for example: sawdust, olive stones and wood pellets;-coarse or irregularly-shaped particulate materials, particle sizes up to about 200 mm that can be sampled using a fork or shovel, for example: wood chips and nut shells, forest residue chips, and straw;-baled materials for example: baled straw or grass;-large pieces (particles sizes above 200 mm) which are either picked manually or automatically;-vegetable waste, fibrous waste from virgin pulp production and from production of paper from pulp that has been dewatered;- round wood.It may be possible to use this standard on other solid biofuels. The methods described in this European Standard may be used, for example, when the samples are to be tested for moisture content, ash content, calorific value, bulk density, durability, particle size distribution, ash melting behaviour and chemical composition. The methods are not intended for obtaining the very large samples required for the testing of bridging properties.

    General Product Information - (Show below) - (Hide below)

    Committee CEN/TC 335
    Development Note Supersedes CEN/TS 14778-1, CEN/TS 14778-2 & CEN/TS 14779. (06/2011) Supersedes PREN 14778. (08/2011)
    Document Type Standard
    Publisher Comite Europeen de Normalisation
    Status Superseded
    Superseded By
    Supersedes

    Standards Referenced By This Book - (Show below) - (Hide below)

    BS EN 15234-4:2012 Solid biofuels. Fuel quality assurance Wood chips for non-industrial use
    BS EN ISO 18122:2015 Solid biofuels. Determination of ash content
    BS EN 16640:2017 Bio-based products. Bio-based carbon content. Determination of the bio-based carbon content using the radiocarbon method
    BS EN ISO 17830:2016 Solid biofuels. Particle size distribution of disintegrated pellets
    DIN EN ISO 18123:2016-03 Solid biofuels - Determination of the content of volatile matter (ISO 18123:2015)
    BS EN ISO 17827-1:2016 Solid biofuels. Determination of particle size distribution for uncompressed fuels Oscillating screen method using sieves with apertures of 3,15 mm and above
    16/30303043 DC : DRAFT MAR 2016 BS EN ISO 19743 - SOLID BIOFUELS - DETERMINATION OF CONTENT OF HEAVY EXTRANEOUS MATERIALS LARGE THAN 3,15 MM
    I.S. EN 16127:2012 SOLID BIOFUELS - DETERMINATION OF LENGTH AND DIAMETER OF PELLETS
    DIN EN ISO 18122:2016-03 Solid biofuels - Determination of ash content (ISO 18122:2015)
    DIN EN 16640:2015-09 (Draft) BIO-BASED PRODUCTS - BIO-BASED CARBON CONTENT - DETERMINATION OF THE BIO-BASED CARBON CONTENT USING THE RADIOCARBON METHOD
    I.S. EN 14780:2011 SOLID BIOFUELS - SAMPLE PREPARATION
    15/30319064 DC : 0 BS EN ISO 18125 - SOLID BIOFUELS - DETERMINATION OF CALORIFIC VALUE
    UNE-EN ISO 17827-1:2016 Solid biofuels - Determination of particle size distribution for uncompressed fuels - Part 1: Oscillating screen method using sieves with apertures of 3,15 mm and above (ISO 17827-1:2016)
    BS EN 15150:2011 Solid biofuels. Determination of particle density
    BS EN 16126:2012 Solid biofuels. Determination of particle size distribution of disintegrated pellets
    UNE-EN ISO 18123:2016 Solid biofuels - Determination of the content of volatile matter (ISO 18123:2015)
    I.S. EN 16785-1:2015 BIO-BASED PRODUCTS - BIO-BASED CONTENT - PART 1: DETERMINATION OF THE BIO-BASED CONTENT USING THE RADIOCARBON ANALYSIS AND ELEMENTAL ANALYSIS
    I.S. EN ISO 18134-3:2015 SOLID BIOFUELS - DETERMINATION OF MOISTURE CONTENT - OVEN DRY METHOD - PART 3: MOISTURE IN GENERAL ANALYSIS SAMPLE (ISO 18134-3:2015)
    S.R. CEN/TR 15149-3:2014 SOLID BIOFUELS - DETERMINATION OF PARTICLE SIZE DISTRIBUTION - PART 3: ROTARY SCREEN METHOD
    I.S. EN ISO 17827-1:2016 SOLID BIOFUELS - DETERMINATION OF PARTICLE SIZE DISTRIBUTION FOR UNCOMPRESSED FUELS - PART 1: OSCILLATING SCREEN METHOD USING SIEVES WITH APERTURES OF 3,15 MM AND ABOVE (ISO 17827-1:2016)
    S.R. CEN/TS 16640:2014 BIO-BASED PRODUCTS - DETERMINATION OF THE BIO BASED CARBON CONTENT OF PRODUCTS USING THE RADIOCARBON METHOD
    UNE-EN 15234-4:2012 Solid biofuels - Fuel quality assurance - Part 4: Wood chips for non-industrial use
    I.S. EN 16640:2017 BIO-BASED PRODUCTS - BIO-BASED CARBON CONTENT - DETERMINATION OF THE BIO-BASED CARBON CONTENT USING THE RADIOCARBON METHOD
    UNE-EN ISO 17829:2016 Solid biofuels - Determination of length and diameter of pellets (ISO 17829:2015)
    BS EN 303-5:2012 Heating boilers Heating boilers for solid fuels, manually and automatically stoked, nominal heat output of up to 500 kW. Terminology, requirements, testing and marking
    EN 14780:2011 Solid biofuels - Sample preparation
    CEN/TS 16640 : 2014 BIO-BASED PRODUCTS - DETERMINATION OF THE BIO BASED CARBON CONTENT OF PRODUCTS USING THE RADIOCARBON METHOD
    DIN EN 16127:2012-05 SOLID BIOFUELS - DETERMINATION OF LENGTH AND DIAMETER OF PELLETS
    CEN/TR 15149-3:2014 Solid biofuels - Determination of particle size distribution - Part 3: Rotary screen method
    EN 16640:2017/AC:2017 BIO-BASED PRODUCTS - BIO-BASED CARBON CONTENT - DETERMINATION OF THE BIO-BASED CARBON CONTENT USING THE RADIOCARBON METHOD
    BS EN ISO 18134-3:2015 Solid biofuels. Determination of moisture content. Oven dry method Moisture in general analysis sample
    UNE-EN 16127:2012 Solid biofuels - Determination of length and diameter of pellets
    UNE-EN ISO 18134-3:2016 Solid biofuels - Determination of moisture content - Oven dry method - Part 3: Moisture in general analysis sample (ISO 18134-3:2015)
    DIN EN ISO 17827-1:2016-10 SOLID BIOFUELS - DETERMINATION OF PARTICLE SIZE DISTRIBUTION FOR UNCOMPRESSED FUELS - PART 1: OSCILLATING SCREEN METHOD USING SIEVES WITH APERTURES OF 3,15 MM AND ABOVE (ISO 17827-1:2016)
    BS EN 16127:2012 Solid biofuels. Determination of length and diameter of pellets
    DIN EN 15150:2012-01 SOLID BIOFUELS - DETERMINATION OF PARTICLE DENSITY
    DIN EN 14961-6:2012-04 SOLID BIOFUELS - FUEL SPECIFICATIONS AND CLASSES - PART 6: NON-WOODY PELLETS FOR NON-INDUSTRIAL USE
    CSA ISO 18134-3 : 2015 SOLID BIOFUELS - DETERMINATION OF MOISTURE CONTENT - OVEN DRY METHOD - PART 3: MOISTURE IN GENERAL ANALYSIS SAMPLE
    DIN EN ISO 17829 E : 2016 SOLID BIOFUELS - DETERMINATION OF LENGTH AND DIAMETER OF PELLETS (ISO 17829:2015)
    UNI EN 15234-4 : 2012 SOLID BIOFUELS - FUEL QUALITY ASSURANCE - PART 4: WOOD CHIPS FOR NON-INDUSTRIAL USE
    UNE-EN ISO 18122:2016 Solid biofuels - Determination of ash content (ISO 18122:2015)
    UNI EN 14961-6 : 2012 SOLID BIOFUELS - FUEL SPECIFICATIONS AND CLASSES - PART 6: NON-WOODY PELLETS FOR NON-INDUSTRIAL USE
    I.S. EN 15150:2011 SOLID BIOFUELS - DETERMINATION OF PARTICLE DENSITY
    BS EN 14780:2011 Solid biofuels. Sample preparation
    DIN EN 303-5:2012-10 Heating boilers - Part 5: Heating boilers for solid fuels, manually and automatically stoked, nominal heat output of up to 500 kW - Terminology, requirements, testing and marking
    ISO 18134-3:2015 Solid biofuels — Determination of moisture content — Oven dry method — Part 3: Moisture in general analysis sample
    I.S. EN 303-5:2012 HEATING BOILERS - PART 5: HEATING BOILERS FOR SOLID FUELS, MANUALLY AND AUTOMATICALLY STOKED, NOMINAL HEAT OUTPUT OF UP TO 500 KW - TERMINOLOGY, REQUIREMENTS, TESTING AND MARKING
    DIN EN 16640:2017-08 BIO-BASED PRODUCTS - BIO-BASED CARBON CONTENT - DETERMINATION OF THE BIO-BASED CARBON CONTENT USING THE RADIOCARBON METHOD
    DIN EN 14780:2011-09 SOLID BIOFUELS - SAMPLE PREPARATION
    EN 303-5:2012 Heating boilers - Part 5: Heating boilers for solid fuels, manually and automatically stoked, nominal heat output of up to 500 kW - Terminology, requirements, testing and marking
    DIN EN ISO 18134-1 E : 2015 SOLID BIOFUELS - DETERMINATION OF MOISTURE CONTENT - OVEN DRY METHOD - PART 1: TOTAL MOISTURE - REFERENCE METHOD (ISO 181341:2015)
    PD CEN/TR 15149-3:2014 Solid biofuels. Determination of particle size distribution Rotary screen method
    DIN EN ISO 17829:2016-03 SOLID BIOFUELS - DETERMINATION OF LENGTH AND DIAMETER OF PELLETS (ISO 17829:2015)
    DIN EN 16126:2012-05 SOLID BIOFUELS - DETERMINATION OF PARTICLE SIZE DISTRIBUTION OF DISINTEGRATED PELLETS
    I.S. EN ISO 18134-1:2015 SOLID BIOFUELS - DETERMINATION OF MOISTURE CONTENT - OVEN DRY METHOD - PART 1: TOTAL MOISTURE - REFERENCE METHOD (ISO 18134-1:2015)
    BS EN 14961-6:2012 Solid biofuels. Fuel specifications and classes Non-woody pellets for non-industrial use
    UNE-EN ISO 18134-1:2016 Solid biofuels - Determination of moisture content - Oven dry method - Part 1: Total moisture - Reference method (ISO 18134-1:2015)
    DIN EN ISO 18134-3:2015-12 Solid biofuels - Determination of moisture content - Oven dry method - Part 3: Moisture in general analysis sample (ISO 18134-3:2015)
    DIN EN ISO 17827-1 E : 2016 SOLID BIOFUELS - DETERMINATION OF PARTICLE SIZE DISTRIBUTION FOR UNCOMPRESSED FUELS - PART 1: OSCILLATING SCREEN METHOD USING SIEVES WITH APERTURES OF 3,15 MM AND ABOVE (ISO 17827-1:2016)
    BS ISO 18466:2016 Stationary source emissions. Determination of the biogenic fraction in C O2 in stack gas using the balance method
    DIN EN ISO 18134-1:2015-12 Solid biofuels - Determination of moisture content - Oven dry method - Part 1: Total moisture - Reference method (ISO 18134-1:2015)
    UNI EN 303-5 : 2012 HEATING BOILERS - PART 5: HEATING BOILERS FOR SOLID FUELS, MANUALLY AND AUTOMATICALLY STOKED, NOMINAL HEAT OUTPUT OF UP TO 500 KW - TERMINOLOGY, REQUIREMENTS, TESTING AND MARKING
    14/30304809 DC : 0 BS EN 16785 - BIO-BASED PRODUCTS - DETERMINATION OF THE BIO-BASED CONTENT USING THE RADIOCARBON ANALYSIS AND ELEMENTAL ANALYSIS
    CAN/CSA-ISO 17827-1:17 SOLID BIOFUELS - DETERMINATION OF PARTICLE SIZE DISTRIBUTION FOR UNCOMPRESSED FUELS - PART 1: OSCILLATING SCREEN METHOD USING SIEVES WITH APERTURES OF 3,15 MM AND ABOVE
    BS EN ISO 17829:2015 Solid biofuels. Determination of length and diameter of pellets
    I.S. EN ISO 18122:2015 SOLID BIOFUELS - DETERMINATION OF ASH CONTENT (ISO 18122:2015)
    NF EN 15234-4 : 2012 SOLID BIOFUELS - FUEL QUALITY ASSURANCE - PART 4: WOOD CHIPS FOR NON-INDUSTRIAL USE
    ISO 18466:2016 Stationary source emissions — Determination of the biogenic fraction in CO2 in stack gas using the balance method
    UNI EN 16126 : 2012 SOLID BIOFUELS - DETERMINATION OF PARTICLE SIZE DISTRIBUTION OF DISINTEGRATED PELLETS
    UNE-EN 16640:2017 Bio-based products - Bio-based carbon content - Determination of the bio-based carbon content using the radiocarbon method
    ISO 17827-1:2016 Solid biofuels Determination of particle size distribution for uncompressed fuels Part 1: Oscillating screen method using sieves with apertures of 3,15 mm and above
    EN ISO 17829:2015 Solid biofuels - Determination of length and diameter of pellets (ISO 17829:2015)
    DIN EN ISO 18123 E : 2016 SOLID BIOFUELS - DETERMINATION OF THE CONTENT OF VOLATILE MATTER (ISO 18123:2015)
    BS EN ISO 18123:2015 Solid biofuels. Determination of the content of volatile matter
    UNI EN 16127 : 2012 SOLID BIOFUELS - DETERMINATION OF LENGTH AND DIAMETER OF PELLETS
    UNE-EN ISO 17830:2016 Solid biofuels - Particle size distribution of disintegrated pellets (ISO 17830:2016)
    DIN EN 15234-4:2012-04 Solid biofuels - Fuel quality assurance - Part 4: Wood chips for non-industrial use
    CSA ISO 18134-2 : 2015 SOLID BIOFUELS - DETERMINATION OF MOISTURE CONTENT - OVEN DRY METHOD - PART 2: TOTAL MOISTURE - SIMPLIFIED METHOD
    BS EN 16785-1:2015 Bio-based products. Bio-based content Determination of the bio-based content using the radiocarbon analysis and elemental analysis
    DIN EN 16785-1 E : 2016 BIO-BASED PRODUCTS - BIO-BASED CONTENT - PART 1: DETERMINATION OF THE BIO-BASED CONTENT USING THE RADIOCARBON ANALYSIS AND ELEMENTAL ANALYSIS
    UNE-EN 16785-1:2016 Bio-based products - Bio-based content - Part 1: Determination of the bio-based content using the radiocarbon analysis and elemental analysis
    15/30326869 DC : 0 BS EN 16640 - BIO-BASED PRODUCTS - BIO-BASED CARBON CONTENT - DETERMINATION OF THE BIO-BASED CARBON CONTENT USING THE RADIOCARBON METHOD
    I.S. EN 16126:2012 SOLID BIOFUELS - DETERMINATION OF PARTICLE SIZE DISTRIBUTION OF DISINTEGRATED PELLETS
    I.S. EN ISO 18123:2015 SOLID BIOFUELS - DETERMINATION OF THE CONTENT OF VOLATILE MATTER (ISO 18123:2015)
    CAN/CSA-ISO 17830:17 Solid biofuels — Particle size distribution of disintegrated pellets (Adopted ISO 17830:2016, first edition, 2016-03-01)
    UNI CEN/TS 16640 : 2014 BIO-BASED PRODUCTS - DETERMINATION OF THE BIO BASED CARBON CONTENT OF PRODUCTS USING THE RADIOCARBON METHOD
    UNE-EN 14961-6:2012 Solid biofuels - Fuel specifications and classes - Part 6: Non-woody pellets for non-industrial use
    I.S. EN 14961-6:2012 SOLID BIOFUELS - FUEL SPECIFICATIONS AND CLASSES - PART 6: NON-WOODY PELLETS FOR NON-INDUSTRIAL USE
    I.S. EN ISO 17830:2016 SOLID BIOFUELS - PARTICLE SIZE DISTRIBUTION OF DISINTEGRATED PELLETS (ISO 17830:2016)
    ISO 18123:2015 Solid biofuels — Determination of the content of volatile matter
    ISO 17830:2016 Solid biofuels Particle size distribution of disintegrated pellets
    ISO 18134-1:2015 Solid biofuels — Determination of moisture content — Oven dry method — Part 1: Total moisture — Reference method
    ISO 18122:2015 Solid biofuels — Determination of ash content
    ISO 17829:2015 Solid Biofuels Determination of length and diameter of pellets
    EN 16785-1:2015 Bio-based products - Bio-based content - Part 1: Determination of the bio-based content using the radiocarbon analysis and elemental analysis
    EN ISO 18134-3:2015 Solid biofuels - Determination of moisture content - Oven dry method - Part 3: Moisture in general analysis sample (ISO 18134-3:2015)
    EN 14961-6:2012 Solid biofuels - Fuel specifications and classes - Part 6: Non-woody pellets for non-industrial use
    EN ISO 18123:2015 Solid biofuels - Determination of the content of volatile matter (ISO 18123:2015)
    EN 16126:2012 Solid biofuels - Determination of particle size distribution of disintegrated pellets
    EN 15234-4:2012 Solid biofuels - Fuel quality assurance - Part 4: Wood chips for non-industrial use
    EN ISO 17827-1:2016 Solid biofuels - Determination of particle size distribution for uncompressed fuels - Part 1: Oscillating screen method using sieves with apertures of 3,15 mm and above (ISO 17827-1:2016)
    EN ISO 18134-1:2015 Solid biofuels - Determination of moisture content - Oven dry method - Part 1: Total moisture - Reference method (ISO 18134-1:2015)
    EN ISO 17830:2016 Solid biofuels - Particle size distribution of disintegrated pellets (ISO 17830:2016)
    EN 16127:2012 Solid biofuels - Determination of length and diameter of pellets
    DIN EN 16640 E : 2017 BIO-BASED PRODUCTS - BIO-BASED CARBON CONTENT - DETERMINATION OF THE BIO-BASED CARBON CONTENT USING THE RADIOCARBON METHOD
    UNE-EN 16126:2012 Solid biofuels - Determination of particle size distribution of disintegrated pellets
    BS EN ISO 18134-1:2015 Solid biofuels. Determination of moisture content. Oven dry method Total moisture. Reference method
    DIN EN 16785-1:2016-03 BIO-BASED PRODUCTS - BIO-BASED CONTENT - PART 1: DETERMINATION OF THE BIO-BASED CONTENT USING THE RADIOCARBON ANALYSIS AND ELEMENTAL ANALYSIS
    DIN EN ISO 18122 E : 2016 SOLID BIOFUELS - DETERMINATION OF ASH CONTENT (ISO 18122:2015)
    UNE-EN 14780:2012 Solid biofuels - Sample preparation
    DIN EN ISO 18134-3 E : 2015 SOLID BIOFUELS - DETERMINATION OF MOISTURE CONTENT - OVEN DRY METHOD - PART 3: MOISTURE IN GENERAL ANALYSIS SAMPLE (ISO 18134-3:2015)
    PD CEN/TS 16640:2014 Bio-based products. Determination of the bio based carbon content of products using the radiocarbon method
    I.S. EN 15234-4:2012 SOLID BIOFUELS - FUEL QUALITY ASSURANCE - PART 4: WOOD CHIPS FOR NON-INDUSTRIAL USE
    UNI EN 14780 : 2011 SOLID BIOFUELS - SAMPLE PREPARATION
    16/30275160 DC : 0 BS ISO 18466 - STATIONARY SOURCE EMISSIONS - DETERMINATION OF THE BIOGENIC FRACTION IN CO[2]IN STACK GAS USING THE BALANCE METHOD
    CSA ISO 18134-1 : 2015 SOLID BIOFUELS - DETERMINATION OF MOISTURE CONTENT - OVEN DRY METHOD - PART 1: TOTAL MOISTURE - REFERENCE METHOD
    UNI EN 15150 : 2011 SOLID BIOFUELS - DETERMINATION OF PARTICLE DENSITY
    UNE-EN 15150:2012 Solid biofuels - Determination of particle density
    I.S. EN ISO 17829:2015 SOLID BIOFUELS - DETERMINATION OF LENGTH AND DIAMETER OF PELLETS (ISO 17829:2015)
    CSA ISO 18122 : 2016 SOLID BIOFUELS - DETERMINATION OF ASH CONTENT
    NF EN 15150 : 2011 SOLID BIOFUELS - DETERMINATION OF PARTICLE DENSITY
    UNE-EN 303-5:2013 Heating boilers - Part 5: Heating boilers for solid fuels, manually and automatically stoked, nominal heat output of up to 500 kW - Terminology, requirements, testing and marking
    EN 15150:2011 Solid biofuels - Determination of particle density

    Standards Referencing This Book - (Show below) - (Hide below)

    EN 15103:2009 Solid biofuels - Determination of bulk density
    ISO 3310-1:2016 Test sieves Technical requirements and testing Part 1: Test sieves of metal wire cloth
    EN 15210-1:2009 Solid biofuels - Determination of mechanical durability of pellets and briquettes - Part 1: Pellets
    EN 14588:2010 Solid biofuels - Terminology, definitions and descriptions
    ISO 13909-7:2016 Hard coal and coke — Mechanical sampling — Part 7: Methods for determining the precision of sampling, sample preparation and testing
    EN 14780:2011 Solid biofuels - Sample preparation
    ISO 13909-8:2016 Hard coal and coke — Mechanical sampling — Part 8: Methods of testing for bias
    ISO 18283:2006 Hard coal and coke Manual sampling
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