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ASTM D 6299 : 2010 : EDT 2

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance

Available format(s)

Hardcopy , PDF

Superseded date

11-11-2014

Superseded by

ASTM D 6299 : 2013

Language(s)

English

Published date

01-03-2010

€96.91
Excluding VAT

Committee
D 02
DocumentType
Standard Practice
Pages
27
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

1.1 This practice covers information for the design and operation of a program to monitor and control ongoing stability and precision and bias performance of selected analytical measurement systems using a collection of generally accepted statistical quality control (SQC) procedures and tools.

Note 1—A complete list of criteria for selecting measurement systems to which this practice should be applied and for determining the frequency at which it should be applied is beyond the scope of this practice. However, some factors to be considered include (1) frequency of use of the analytical measurement system, (2) criticality of the parameter being measured, (3) system stability and precision performance based on historical data, (4) business economics, and (5) regulatory, contractual, or test method requirements.

1.2 This practice is applicable to stable analytical measurement systems that produce results on a continuous numerical scale.

1.3 This practice is applicable to laboratory test methods.

1.4 This practice is applicable to validated process stream analyzers.

1.5 This practice is applicable to monitoring the differences between two analytical measurement systems that purport to measure the same property provided that both systems have been assessed in accordance with the statistical methodology in Practice D6708 and the appropriate bias applied.

Note 2—For validation of univariate process stream analyzers, see also Practice D3764.

Note 3—One or both of the analytical systems in 1.5 can be laboratory test methods or validated process stream analyzers.

1.6 This practice assumes that the normal (Gaussian) model is adequate for the description and prediction of measurement system behavior when it is in a state of statistical control.

Note 4—For non-Gaussian processes, transformations of test results may permit proper application of these tools. Consult a statistician for further guidance and information.

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ASTM D 7303 : 2017 Standard Test Method for Determination of Metals in Lubricating Greases by Inductively Coupled Plasma Atomic Emission Spectrometry
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ASTM D 3606 : 2017 Standard Test Method for Determination of Benzene and Toluene in Spark Ignition Fuels by Gas Chromatography
ASTM D 5056 : 2017 Standard Test Method for Trace Metals in Petroleum Coke by Atomic Absorption
ASTM D 7551 : 2010 : R2015 Standard Test Method for Determination of Total Volatile Sulfur in Gaseous Hydrocarbons and Liquefied Petroleum Gases and Natural Gas by Ultraviolet Fluorescence (Withdrawn 2024)
ASTM E 2313 : 2015 Standard Test Method for Aldehydes in Mono-, Di-, and Triethylene Glycol (using Spectrophotometry)
ASTM D 8071 : 2017 Standard Test Method for Determination of Hydrocarbon Group Types and Select Hydrocarbon and Oxygenate Compounds in Automotive Spark-Ignition Engine Fuel Using Gas Chromatography with Vacuum Ultraviolet Absorption Spectroscopy Detection (GC-VUV)
ASTM D 5188 : 2016 Standard Test Method for Vapor-Liquid Ratio Temperature Determination of Fuels (Evacuated Chamber and Piston Based Method)
ASTM D 8150 : 2017 Standard Test Method for Determination of Organic Chloride Content in Crude Oil by Distillation Followed by Detection Using Combustion Ion Chromatography
ASTM D 2700 : 2019 Standard Test Method for Motor Octane Number of Spark-Ignition Engine Fuel
ASTM D 7423 : 2017 Standard Test Method for Determination of Oxygenates in C2, C3, C4, and C5 Hydrocarbon Matrices by Gas Chromatography and Flame Ionization Detection
ASTM D 7623 : 2010 : R2015 Standard Test Method for Total Mercury in Crude Oil Using Combustion-Gold Amalgamation and Cold Vapor Atomic Absorption Method
ASTM D 7591 : 2012 : R2017 Standard Test Method for Determination of Free and Total Glycerin in Biodiesel Blends by Anion Exchange Chromatography
ASTM D 6450 : 2016 : REV A Standard Test Method for Flash Point by Continuously Closed Cup (CCCFP) Tester
ASTM D 5600 : 2017 Standard Test Method for Trace Metals in Petroleum Coke by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
ASTM D 6617 : 2017 Standard Practice for Laboratory Bias Detection Using Single Test Result from Standard Material
ASTM D 7751 : 2016 Standard Test Method for Determination of Additive Elements in Lubricating Oils by EDXRF Analysis
ASTM D 6375 : 2009 : R2014 Standard Test Method for Evaporation Loss of Lubricating Oils by Thermogravimetric Analyzer (TGA) Noack Method
ASTM D 7372 : 2017 Standard Guide for Analysis and Interpretation of Proficiency Test Program Results
ASTM E 2469 : 2016 Standard Test Method for Chloride in Mono-, Di- and Tri-ethylene Glycol by Ion Chromatography
ASTM F 2980 : 2013 : R2017 Standard Test Method for Analysis of Heavy Metals in Glass by Field Portable X-Ray Fluorescence (XRF)
ASTM D 3246 : 2015 Standard Test Method for Sulfur in Petroleum Gas by Oxidative Microcoulometry (Withdrawn 2024)
ASTM D 3828 : 2016 : REV A Standard Test Methods for Flash Point by Small Scale Closed Cup Tester
ASTM F 3078 : 2015 Standard Test Method for Identification and Quantification of Lead in Paint and Similar Coating Materials using Energy Dispersive X-ray Fluorescence Spectrometry (EDXRF)
ASTM D 7920 : 2015 : EDT 1 Standard Test Method for Determination of Fuel Methanol (M99) and Methanol Fuel Blends (M10 to M99) by Gas Chromatography
ASTM D 7622 : 2010 : R2015 Standard Test Method for Total Mercury in Crude Oil Using Combustion and Direct Cold Vapor Atomic Absorption Method with Zeeman Background Correction
ASTM D 5863 : 2000 : REV A : R2016 Standard Test Methods for Determination of Nickel, Vanadium, Iron, and Sodium in Crude Oils and Residual Fuels by Flame Atomic Absorption Spectrometry
ASTM D 7111 : 2016 Standard Test Method for Determination of Trace Elements in Middle Distillate Fuels by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
ASTM D 7170 : 2016 Standard Test Method for Determination of Derived Cetane Number (DCN) of Diesel Fuel Oils—Fixed Range Injection Period, Constant Volume Combustion Chamber Method (Withdrawn 2019)
ASTM D 4294 : 2016 : EDT 1 Standard Test Method for Sulfur in Petroleum and Petroleum Products by Energy Dispersive X-ray Fluorescence Spectrometry
ASTM D 4057 : 2012 : R2018 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
ASTM D 3120 : 2008 : R2019 Standard Test Method for Trace Quantities of Sulfur in Light Liquid Petroleum Hydrocarbons by Oxidative Microcoulometry
ASTM D 7371 : 2014 Standard Test Method for Determination of Biodiesel (Fatty Acid Methyl Esters) Content in Diesel Fuel Oil Using Mid Infrared Spectroscopy (FTIR-ATR-PLS Method)
ASTM D 7040 : 2004 : R2015 Standard Test Method for Determination of Low Levels of Phosphorus in ILSAC GF 4 and Similar Grade Engine Oils by Inductively Coupled Plasma Atomic Emission Spectrometry
ASTM D 7862 : 2019 Standard Specification for Butanol for Blending with Gasoline for Use as Automotive Spark-Ignition Engine Fuel
ASTM D 8267 : 2019 Standard Test Method for Determination of Saturated Hydrocarbon, Aromatic, and Diaromatic Content of Aviation Turbine Fuels Using Gas Chromatography with Vacuum Ultraviolet Absorption Spectroscopy Detection (GC-VUV)
ASTM D 8185 : 2018 Standard Guide for In-Service Lubricant Viscosity Measurement
ASTM D 7861 : 2014 : R2019 Standard Test Method for Determination of Fatty Acid Methyl Esters (FAME) in Diesel Fuel by Linear Variable Filter (LVF) Array Based Mid-Infrared Spectroscopy
ASTM D 8088 : 2016 Standard Practice for Determination of the Six Major Rare Earth Elements in Fluid Catalytic Cracking Catalysts, Zeolites, Additives, and Related Materials by Inductively Coupled Plasma Optical Emission Spectroscopy
ASTM D 7806 : 2012 Standard Test Method for Determination of the Fatty Acid Methyl Ester (FAME) Content of a Blend of Biodiesel and Petroleum-Based Diesel Fuel Oil Using Mid-Infrared Spectroscopy
ASTM D 7828 : 2012 Standard Test Method for Determination of Residue Composition in Liquefied Petroleum Gas (LPG) Using Automated Thermal Desorption/Gas Chromatography (ATD/GC) (Withdrawn 2021)
ASTM D 5708 : 2015 Standard Test Methods for Determination of Nickel, Vanadium, and Iron in Crude Oils and Residual Fuels by Inductively Coupled Plasma (ICP) Atomic Emission Spectrometry
ASTM D 7807 : 2012 Standard Test Method for Determination of Boiling Range Distribution of Hydrocarbon and Sulfur Components of Petroleum Distillates by Gas Chromatography and Chemiluminescence Detection
ASTM D 5501 : 2012 : R2016 Standard Test Method for Determination of Ethanol and Methanol Content in Fuels Containing Greater than 20% Ethanol by Gas Chromatography
ASTM D 6550 : 2015 Standard Test Method for Determination of Olefin Content of Gasolines by Supercritical-Fluid Chromatography
ASTM D 2622 : 2016 Standard Test Method for Sulfur in Petroleum Products by Wavelength Dispersive X-ray Fluorescence Spectrometry
ASTM D 6278 : 2017 : EDT 1 Standard Test Method for Shear Stability of Polymer Containing Fluids Using a European Diesel Injector Apparatus
ASTM D 7319 : 2017 Standard Test Method for Determination of Existent and Potential Sulfate and Inorganic Chloride in Fuel Ethanol and Butanol by Direct Injection Suppressed Ion Chromatography
ASTM D 1218 : 2012 : R2016 Standard Test Method for Refractive Index and Refractive Dispersion of Hydrocarbon Liquids
ASTM D 8001 : 2016 : EDT 1 Standard Test Method for Determination of Total Nitrogen, Total Kjeldahl Nitrogen by Calculation, and Total Phosphorus in Water, Wastewater by Ion Chromatography
ASTM D 3231 : 2018 Standard Test Method for Phosphorus in Gasoline
ASTM D 4929 : 2017 Standard Test Method for Determination of Organic Chloride Content in Crude Oil
ASTM D 6378 : 2018 : REV A Standard Test Method for Determination of Vapor Pressure (VP<inf>X</inf>) of Petroleum Products, Hydrocarbons, and Hydrocarbon-Oxygenate Mixtures (Triple Expansion Method)
ASTM D 6443 : 2014 : R2019 : EDT 1 Standard Test Method for Determination of Calcium, Chlorine, Copper, Magnesium, Phosphorus, Sulfur, and Zinc in Unused Lubricating Oils and Additives by Wavelength Dispersive X-ray Fluorescence Spectrometry (Mathematical Correction Procedure)
ASTM D 3831 : 2012 : R2017 Standard Test Method for Manganese in Gasoline By Atomic Absorption Spectroscopy
ASTM D 56 : 2016 : REV A Standard Test Method for Flash Point by Tag Closed Cup Tester
ASTM D 613 : 2018 : REV A Standard Test Method for Cetane Number of Diesel Fuel Oil
ASTM D 1318 : 2016 Standard Test Method for Sodium in Residual Fuel Oil (Flame Photometric Method)
ASTM D 1266 : 2018 Standard Test Method for Sulfur in Petroleum Products (Lamp Method)
ASTM D 7875 : 2014 Standard Test Method for Determination of Butanol and Acetone Content of Butanol for Blending with Gasoline by Gas Chromatography
ASTM D 6890 : 2018 Standard Test Method for Determination of Ignition Delay and Derived Cetane Number (DCN) of Diesel Fuel Oils by Combustion in a Constant Volume Chamber
ASTM D 808 : 2016 Standard Test Method for Chlorine in New and Used Petroleum Products (High Pressure Decomposition Device Method) (Withdrawn 2021)
ASTM D 1018 : 2011 : R2016 Standard Test Method for Hydrogen In Petroleum Fractions (Withdrawn 2021)
ASTM D 6708 : 2019 Standard Practice for Statistical Assessment and Improvement of Expected Agreement Between Two Test Methods that Purport to Measure the Same Property of a Material
ASTM D 7757 : 2017 Standard Test Method for Silicon in Gasoline and Related Products by Monochromatic Wavelength Dispersive X-ray Fluorescence Spectrometry
ASTM D 8149 : 2017 Standard Practice for Optimization, Calibration, and Validation of Ion Chromatographic Determination of Heteroatoms and Anions in Petroleum Products and Lubricants
ASTM D 7328 : 2017 Standard Test Method for Determination of Existent and Potential Inorganic Sulfate and Total Inorganic Chloride in Fuel Ethanol by Ion Chromatography Using Aqueous Sample Injection
ASTM D 6667 : 2014 : R2019 Standard Test Method for Determination of Total Volatile Sulfur in Gaseous Hydrocarbons and Liquefied Petroleum Gases by Ultraviolet Fluorescence
ASTM D 6849 : 2013 Standard Practice for Storage and Use of Liquefied Petroleum Gases (LPG) in Sample Cylinders for LPG Test Methods
ASTM D 6895 : 2017 Standard Test Method for Rotational Viscosity of Heavy Duty Diesel Drain Oils at 100 °C
ASTM F 2617 : 2015 Standard Test Method for Identification and Quantification of Chromium, Bromine, Cadmium, Mercury, and Lead in Polymeric Material Using Energy Dispersive X-ray Spectrometry
ASTM D 6728 : 2016 Standard Test Method for Determination of Contaminants in Gas Turbine and Diesel Engine Fuel by Rotating Disc Electrode Atomic Emission Spectrometry
ASTM D 4323 : 2015 Standard Test Method for Hydrogen Sulfide in the Atmosphere by Rate of Change of Reflectance
ASTM D 3237 : 2017 Standard Test Method for Lead in Gasoline by Atomic Absorption Spectroscopy
ASTM D 7314 : 2010 : R2015 Standard Practice for Determination of the Heating Value of Gaseous Fuels using Calorimetry and On-line/At-line Sampling
ASTM D 7109 : 2018 Standard Test Method for Shear Stability of Polymer-Containing Fluids Using a European Diesel Injector Apparatus at 30 Cycles and 90 Cycles
ASTM D 6732 : 2004 : R2015 Standard Test Method for Determination of Copper in Jet Fuels by Graphite Furnace Atomic Absorption Spectrometry
ASTM D 7756 : 2019 Standard Test Method for Residues in Liquefied Petroleum (LP) Gases by Gas Chromatography with Liquid, On-Column Injection
ASTM E 1655 : 2017 Standard Practices for Infrared Multivariate Quantitative Analysis
ASTM D 1091 : 2011 : R2016 Standard Test Methods for Phosphorus in Lubricating Oils and Additives (Withdrawn 2021)
ASTM D 7235 : 2016 Standard Guide for Establishing a Linear Correlation Relationship Between Analyzer and Primary Test Method Results Using Relevant ASTM Standard Practices
ASTM D 7220 : 2012 : R2017 Standard Test Method for Sulfur in Automotive, Heating, and Jet Fuels by Monochromatic Energy Dispersive X-ray Fluorescence Spectrometry
ASTM D 7260 : 2019 Standard Practice for Optimization, Calibration, and Validation of Inductively Coupled Plasma-Atomic Emission Spectrometry (ICP-AES) for Elemental Analysis of Petroleum Products and Lubricants
ASTM D 3341 : 2016 Standard Test Method for Lead in Gasoline—Iodine Monochloride Method (Withdrawn 2022)
ASTM D 7923 : 2019 Standard Test Method for Water in Ethanol and Hydrocarbon Blends by Karl Fischer Titration
ASTM D 5184 : 2012 : R2017 Standard Test Methods for Determination of Aluminum and Silicon in Fuel Oils by Ashing, Fusion, Inductively Coupled Plasma Atomic Emission Spectrometry, and Atomic Absorption Spectrometry
ASTM D 7620 : 2010 : R2015 Standard Test Method for Determination of Total Sulfur in Liquid Hydrocarbon Based Fuels by Continuous Injection, Air Oxidation and Ultraviolet Fluorescence Detection
ASTM D 3228 : 2008 : R2019 Standard Test Method for Total Nitrogen in Lubricating Oils and Fuel Oils by Modified Kjeldahl Method
ASTM D 7042 : 2016 : EDT 3 Standard Test Method for Dynamic Viscosity and Density of Liquids by Stabinger Viscometer (and the Calculation of Kinematic Viscosity)
ASTM D 4045 : 2015 Standard Test Method for Sulfur in Petroleum Products by Hydrogenolysis and Rateometric Colorimetry
ASTM D 8174 : 2018 Standard Test Method for Finite Flash Point Determination of Liquid Wastes by Small-Scale Closed Cup Tester
ASTM D 7343 : 2018 Standard Practice for Optimization, Sample Handling, Calibration, and Validation of X-ray Fluorescence Spectrometry Methods for Elemental Analysis of Petroleum Products and Lubricants
ASTM D 4629 : 2017 Standard Test Method for Trace Nitrogen in Liquid Hydrocarbons by Syringe/Inlet Oxidative Combustion and Chemiluminescence Detection
ASTM D 4628 : 2016 Standard Test Method for Analysis of Barium, Calcium, Magnesium, and Zinc in Unused Lubricating Oils by Atomic Absorption Spectrometry
ASTM D 1552 : 2016 : EDT 1 Standard Test Method for Sulfur in Petroleum Products by High Temperature Combustion and Infrared (IR) Detection or Thermal Conductivity Detection (TCD)
ASTM D 7808 : 2018 Standard Practice for Determining the Site Precision of a Process Stream Analyzer on Process Stream Material
ASTM D 7279 : 2018 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids by Automated Houillon Viscometer
ASTM D 7419 : 2018 Standard Test Method for Determination of Total Aromatics and Total Saturates in Lube Basestocks by High Performance Liquid Chromatography (HPLC) with Refractive Index Detection
ASTM D 8056 : 2018 Standard Guide for Elemental Analysis of Crude Oil
ASTM D 7845 : 2017 Standard Test Method for Determination of Chemical Species in Marine Fuel Oil by Multidimensional Gas Chromatography/Mass Spectrometry
ASTM D 909 : 2018 Standard Test Method for Supercharge Rating of Spark-Ignition Aviation Gasoline
ASTM D 94 : 2007 : R2017 Standard Test Methods for Saponification Number of Petroleum Products
ASTM D 8146 : 2018 Standard Guide for Evaluating Test Method Capability and Fitness for Use
ASTM D 2885 : 2019 : REV A Standard Test Method for Determination of Octane Number of Spark-Ignition Engine Fuels by On-Line Direct Comparison Technique
ASTM D 445 : 2019 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM D 7039 : 2015 : REV A Standard Test Method for Sulfur in Gasoline, Diesel Fuel, Jet Fuel, Kerosine, Biodiesel, Biodiesel Blends, and Gasoline-Ethanol Blends by Monochromatic Wavelength Dispersive X-ray Fluorescence Spectrometry
ASTM D 482 : 2013 Standard Test Method for Ash from Petroleum Products
ASTM D 7318 : 2019 Standard Test Method for Existent Inorganic Sulfate in Ethanol by Potentiometric Titration
ASTM D 7686 : 2011 Standard Test Method for Field-Based Condition Monitoring of Soot in In-Service Lubricants Using a Fixed-Filter Infrared (IR) Instrument
ASTM E 2193 : 2016 Standard Test Method for Ultraviolet Transmittance of Monoethylene Glycol (using Ultraviolet Spectrophotometry)
ASTM D 87 : 2009 : R2018 Standard Test Method for Melting Point of Petroleum Wax (Cooling Curve)
ASTM D 7171 : 2016 Standard Test Method for Hydrogen Content of Middle Distillate Petroleum Products by Low-Resolution Pulsed Nuclear Magnetic Resonance Spectroscopy
ASTM D 4951 : 2014 Standard Test Method for Determination of Additive Elements in Lubricating Oils by Inductively Coupled Plasma Atomic Emission Spectrometry
ASTM D 4927 : 2015 Standard Test Methods for Elemental Analysis of Lubricant and Additive Components—Barium, Calcium, Phosphorus, Sulfur, and Zinc by Wavelength-Dispersive X-Ray Fluorescence Spectroscopy
ASTM D 7720 : 2011 : R2017 Standard Guide for Statistically Evaluating Measurand Alarm Limits when Using Oil Analysis to Monitor Equipment and Oil for Fitness and Contamination
ASTM D 8175 : 2018 Standard Test Method for Finite Flash Point Determination of Liquid Wastes by Pensky-Martens Closed Cup Tester
ASTM D 5291 : 2016 Standard Test Methods for Instrumental Determination of Carbon, Hydrogen, and Nitrogen in Petroleum Products and Lubricants
ASTM D 7214 : 2007 : REV A : R2012 Standard Test Method for Determination of the Oxidation of Used Lubricants by FT-IR Using Peak Area Increase Calculation
ASTM D 8183 : 2018 Standard Test Method for Determination of Indicated Cetane Number (ICN) of Diesel Fuel Oils using a Constant Volume Combustion Chamber—Reference Fuels Calibration Method
ASTM D 3348 : 2012 : R2017 Standard Test Method for Rapid Field Test for Trace Lead in Unleaded Gasoline (Colorimetric Method) (Withdrawn 2022)
ASTM D 6624 : 2019 Standard Practice for Determining a Flow-Proportioned Average Property Value (FPAPV) for a Collected Batch of Process Stream Material Using Stream Analyzer Data
ASTM D 5191 : 2019 Standard Test Method for Vapor Pressure of Petroleum Products and Liquid Fuels (Mini Method)
ASTM D 5059 : 2014 : R2019 Standard Test Methods for Lead in Gasoline by X-Ray Spectroscopy
ASTM D 7112 : 2019 Standard Test Method for Determining Stability and Compatibility of Heavy Fuel Oils and Crude Oils by Heavy Fuel Oil Stability Analyzer (Optical Detection)
ASTM D 2272 : 2014 : REV A Standard Test Method for Oxidation Stability of Steam Turbine Oils by Rotating Pressure Vessel
ASTM D 7911 : 2014 Standard Guide for Using Reference Material to Characterize Measurement Bias Associated with Volatile Organic Compound Emission Chamber Test
ASTM D 7740 : 2011 : R2016 Standard Practice for Optimization, Calibration, and Validation of Atomic Absorption Spectrometry for Metal Analysis of Petroleum Products and Lubricants

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