ISO 1133:2005

Foreword
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Apparatus
   5.1 Extrusion plastometer
   5.2 Accessory equipment
6 Test sample
   6.1 Sample form
   6.2 Conditioning
7 Temperature-calibration, cleaning and maintenance of
   the apparatus
   7.1 Calibration of the temperature-control system
   7.2 Cleaning the apparatus
8 Procedure A: mass-measurement method
   8.1 Selection of temperature and load
   8.2 Cleaning
   8.3 Selection of sample mass and charging cylinder
   8.4 Measurements
   8.5 Expression of results
9 Procedure B: displacement-measurement method
   9.1 Selection of temperature and load
   9.2 Minimum piston displacement distance
   9.3 Timer
   9.4 Preparation for the test
   9.5 Measurements
   9.6 Expression of results
10 Flow rate ratio (FRR)
11 Precision
12 Test report
Annex A (normative) Test conditions for MFR and MVR
                      determinations
Annex B (informative) Conditions specified in International
                      Standards for determination of the melt
                      flow rate of thermoplastic materials

ISO 1133:2005 specifies two procedures for the determination of the melt mass-flow rate (MFR) and the melt volume-flow rate (MVR) of thermoplastic materials under specified conditions of temperature and load. One is a mass-measurement method. The other is a displacement-measurement method. Normally, the test conditions for measurement of melt flow rate are specified in the material standard with a reference to ISO 1133. The test conditions normally used for thermoplastics are listed in annexes.

These methods are in principle also applicable to thermoplastics for which the rheological behaviour is affected during the measurement by phenomena such as hydrolysis, condensation or crosslinking, but only if the effect is limited in extent and only if the repeatability and reproducibility are within an acceptable range. For materials which show significantly affected rheological behaviour during testing, these methods are not appropriate. In such cases, the use of the viscosity number in dilute solution, determined in accordance with the relevant part of ISO 1628, is recommended for characterization purposes.